##TITLE=              31P MAS NMR spectrum of calcined AlPO-18
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             He and Klinowski. J. Phys. Chem., 97, 10385-10388 (1993) Figure 2b
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/13 11:18:53
##SOURCE REFERENCE=   AEI-31P-He-1993-calcined
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              AEI
##NAMES=              AlPO-18
##SAMPLE DESCRIPTION= AlPO-18, calcined

$$Bibliographic information 
##$AUTHORS=           He, H., Klinowski, J.
##$TITLE=             Solid state NMR studies of the aluminophosphate molecular sieve AlPO4-18
##$JOURNAL=           Journal of Physical Chemistry
##$VOLUME=            97
##$PAGES=             10385-10388
##$YEAR=              1993
##$DOI=               10.1021/j100142a020
##$FIGURE=            Figure 2b

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         3
##$PEAK LABELS=        A          B          C         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -31.3348   -30.958    -30.1766   
##$PEAK AREAS=         1.         1.         1.        
##$PEAK WIDTHS=        1.57001    1.57001    1.57001   
##$PEAK SHAPES=        0.28267    0.28267    0.28267   
##$NUMBERING REF=     Simmen et al. Zeolites, 11, 654-661 (1991)
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 162.0
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     8000-10000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -22.36                
##LASTX=              -38.84                
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            413
##FIRSTY=              0.00686              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -22.36               0.00686              
 -22.4                0.00929              
 -22.44               0.00769              
 -22.48               0.00625              
 -22.52               0.00663              
 -22.56               0.00658              
 -22.6                0.00684              
 -22.64               0.00511              
 -22.68               0.00355              
 -22.72               0.00388              
 -22.76               0.00386              
 -22.8                0.00384              
 -22.84               0.00381              
 -22.88               0.00391              
 -22.92               0.00384              
 -22.96               0.00334              
 -23.                 0.00698              
 -23.04               0.00991              
 -23.08               0.00923              
 -23.12               0.00930              
 -23.16               0.00935              
 -23.2                0.00931              
 -23.24               0.00933              
 -23.28               0.00932              
 -23.32               0.00932              
 -23.36               0.00932              
 -23.4                0.00932              
 -23.44               0.00932              
 -23.48               0.00932              
 -23.52               0.00932              
 -23.56               0.00934              
 -23.6                0.00928              
 -23.64               0.00935              
 -23.68               0.00955              
 -23.72               0.00750              
 -23.76               0.00652              
 -23.8                0.00625              
 -23.84               0.00392              
 -23.88               0.00368              
 -23.92               0.00392              
 -23.96               0.00381              
 -24.                 0.00386              
 -24.04               0.00389              
 -24.08               0.00357              
 -24.12               0.00491              
 -24.16               0.00694              
 -24.2                0.00661              
 -24.24               0.00435              
 -24.28               0.00360              
 -24.32               0.00392              
 -24.36               0.00382              
 -24.4                0.00382              
 -24.44               0.00400              
 -24.48               0.00332              
 -24.52               0.00493              
 -24.56               0.00937              
 -24.6                0.00956              
 -24.64               0.00919              
 -24.68               0.00937              
 -24.72               0.00932              
 -24.76               0.00932              
 -24.8                0.00933              
 -24.84               0.00932              
 -24.88               0.00932              
 -24.92               0.00932              
 -24.96               0.00932              
 -25.                 0.00932              
 -25.04               0.00932              
 -25.08               0.00932              
 -25.12               0.00932              
 -25.16               0.00932              
 -25.2                0.00932              
 -25.24               0.00932              
 -25.28               0.00932              
 -25.32               0.00932              
 -25.36               0.00932              
 -25.4                0.00932              
 -25.44               0.00932              
 -25.48               0.00932              
 -25.52               0.00932              
 -25.56               0.00932              
 -25.6                0.00932              
 -25.64               0.00932              
 -25.68               0.00932              
 -25.72               0.00932              
 -25.76               0.00933              
 -25.8                0.00932              
 -25.84               0.00932              
 -25.88               0.00934              
 -25.92               0.00925              
 -25.96               0.00953              
 -26.                 0.00907              
 -26.04               0.00678              
 -26.08               0.00638              
 -26.12               0.00673              
 -26.16               0.00642              
 -26.2                0.00664              
 -26.24               0.00890              
 -26.28               0.00956              
 -26.32               0.00925              
 -26.36               0.00934              
 -26.4                0.00933              
 -26.44               0.00932              
 -26.48               0.00932              
 -26.52               0.00933              
 -26.56               0.00932              
 -26.6                0.00931              
 -26.64               0.00940              
 -26.68               0.00909              
 -26.72               0.00972              
 -26.76               0.01199              
 -26.8                0.01220              
 -26.84               0.01207              
 -26.88               0.01191              
 -26.92               0.01223              
 -26.96               0.01452              
 -27.                 0.01502              
 -27.04               0.01473              
 -27.08               0.01482              
 -27.12               0.01481              
 -27.16               0.01481              
 -27.2                0.01479              
 -27.24               0.01486              
 -27.28               0.01475              
 -27.32               0.01465              
 -27.36               0.01672              
 -27.4                0.01784              
 -27.44               0.01746              
 -27.48               0.01755              
 -27.52               0.01767              
 -27.56               0.01703              
 -27.6                0.01917              
 -27.64               0.02368              
 -27.68               0.02568              
 -27.72               0.02602              
 -27.76               0.02516              
 -27.8                0.02711              
 -27.84               0.03135              
 -27.88               0.03102              
 -27.92               0.03449              
 -27.96               0.03749              
 -28.                 0.03642              
 -28.04               0.03654              
 -28.08               0.04099              
 -28.12               0.04250              
 -28.16               0.04269              
 -28.2                0.04514              
 -28.24               0.04707              
 -28.28               0.05148              
 -28.32               0.05357              
 -28.36               0.05333              
 -28.4                0.05580              
 -28.44               0.05995              
 -28.48               0.06454              
 -28.52               0.06817              
 -28.56               0.07335              
 -28.6                0.08235              
 -28.64               0.08529              
 -28.68               0.08882              
 -28.72               0.09665              
 -28.76               0.10527              
 -28.8                0.11393              
 -28.84               0.12198              
 -28.88               0.13213              
 -28.92               0.14203              
 -28.96               0.14804              
 -29.                 0.16051              
 -29.04               0.17395              
 -29.08               0.18597              
 -29.12               0.20191              
 -29.16               0.2222               
 -29.2                0.23265              
 -29.24               0.25125              
 -29.28               0.27572              
 -29.32               0.28738              
 -29.36               0.31469              
 -29.4                0.34764              
 -29.44               0.37409              
 -29.48               0.39766              
 -29.52               0.42906              
 -29.56               0.46868              
 -29.6                0.50004              
 -29.64               0.52139              
 -29.68               0.54769              
 -29.72               0.58079              
 -29.76               0.60531              
 -29.8                0.63416              
 -29.84               0.67372              
 -29.88               0.70528              
 -29.92               0.74169              
 -29.96               0.77711              
 -30.                 0.81096              
 -30.04               0.84750              
 -30.08               0.87657              
 -30.12               0.89968              
 -30.16               0.93182              
 -30.2                0.97071              
 -30.24               0.99608              
 -30.28               1.01462              
 -30.32               1.03883              
 -30.36               1.07283              
 -30.4                1.10618              
 -30.44               1.12518              
 -30.48               1.14739              
 -30.52               1.16965              
 -30.56               1.18485              
 -30.6                1.19972              
 -30.64               1.21986              
 -30.68               1.2323               
 -30.72               1.2409               
 -30.76               1.25438              
 -30.8                1.26522              
 -30.84               1.27447              
 -30.88               1.28119              
 -30.92               1.28419              
 -30.96               1.28397              
 -31.                 1.27943              
 -31.04               1.2648               
 -31.08               1.24866              
 -31.12               1.23923              
 -31.16               1.229                
 -31.2                1.2121               
 -31.24               1.19753              
 -31.28               1.17388              
 -31.32               1.1316               
 -31.36               1.10365              
 -31.4                1.08375              
 -31.44               1.0517               
 -31.48               1.00679              
 -31.52               0.97015              
 -31.56               0.94570              
 -31.6                0.90008              
 -31.64               0.85188              
 -31.68               0.82879              
 -31.72               0.79100              
 -31.76               0.7529               
 -31.8                0.7161               
 -31.84               0.6807               
 -31.88               0.65405              
 -31.92               0.62110              
 -31.96               0.57546              
 -32.                 0.53722              
 -32.04               0.51247              
 -32.08               0.47189              
 -32.12               0.43508              
 -32.16               0.41693              
 -32.2                0.39389              
 -32.24               0.34473              
 -32.28               0.31328              
 -32.32               0.29031              
 -32.36               0.25525              
 -32.4                0.21539              
 -32.44               0.19577              
 -32.48               0.18157              
 -32.52               0.16505              
 -32.56               0.14812              
 -32.6                0.13336              
 -32.64               0.12028              
 -32.68               0.10847              
 -32.72               0.09956              
 -32.76               0.09370              
 -32.8                0.08743              
 -32.84               0.07867              
 -32.88               0.07226              
 -32.92               0.06859              
 -32.96               0.06421              
 -33.                 0.05997              
 -33.04               0.05540              
 -33.08               0.05211              
 -33.12               0.05009              
 -33.16               0.04780              
 -33.2                0.04810              
 -33.24               0.04536              
 -33.28               0.04161              
 -33.32               0.04224              
 -33.36               0.04275              
 -33.4                0.03896              
 -33.44               0.03609              
 -33.48               0.03691              
 -33.52               0.03688              
 -33.56               0.03463              
 -33.6                0.03399              
 -33.64               0.03343              
 -33.68               0.03118              
 -33.72               0.03116              
 -33.76               0.03124              
 -33.8                0.03145              
 -33.84               0.03089              
 -33.88               0.02861              
 -33.92               0.02834              
 -33.96               0.02860              
 -34.                 0.02844              
 -34.04               0.02855              
 -34.08               0.02871              
 -34.12               0.02671              
 -34.16               0.02549              
 -34.2                0.02581              
 -34.24               0.02576              
 -34.28               0.02596              
 -34.32               0.02455              
 -34.36               0.02201              
 -34.4                0.02012              
 -34.44               0.02003              
 -34.48               0.02249              
 -34.52               0.02215              
 -34.56               0.01994              
 -34.6                0.02029              
 -34.64               0.02060              
 -34.68               0.01861              
 -34.72               0.01747              
 -34.76               0.01733              
 -34.8                0.01500              
 -34.84               0.01463              
 -34.88               0.01482              
 -34.92               0.01493              
 -34.96               0.01475              
 -35.                 0.01251              
 -35.04               0.01175              
 -35.08               0.01236              
 -35.12               0.01172              
 -35.16               0.00945              
 -35.2                0.00916              
 -35.24               0.00940              
 -35.28               0.00930              
 -35.32               0.00933              
 -35.36               0.00934              
 -35.4                0.00924              
 -35.44               0.00957              
 -35.48               0.00890              
 -35.52               0.00664              
 -35.56               0.00670              
 -35.6                0.00521              
 -35.64               0.00354              
 -35.68               0.00388              
 -35.72               0.00386              
 -35.76               0.00382              
 -35.8                0.00387              
 -35.84               0.00381              
 -35.88               0.00384              
 -35.92               0.00410              
 -35.96               0.00231              
 -36.                 0.00081              
 -36.04               0.00115              
 -36.08               0.00113              
 -36.12               0.00101              
 -36.16               0.00137              
 -36.2                0.00055              
 -36.24              -0.00166              
 -36.28              -0.00175              
 -36.32              -0.00156              
 -36.36              -0.00165              
 -36.4               -0.00163              
 -36.44              -0.00163              
 -36.48              -0.00163              
 -36.52              -0.00164              
 -36.56              -0.00161              
 -36.6               -0.00164              
 -36.64              -0.00172              
 -36.68              -0.00118              
 -36.72              -0.00309              
 -36.76              -0.00385              
 -36.8                0.00088              
 -36.84               0.00147              
 -36.88               0.00094              
 -36.92               0.00115              
 -36.96               0.00110              
 -37.                 0.00110              
 -37.04               0.00110              
 -37.08               0.00110              
 -37.12               0.00110              
 -37.16               0.00110              
 -37.2                0.00110              
 -37.24               0.00110              
 -37.28               0.00110              
 -37.32               0.00110              
 -37.36               0.00110              
 -37.4                0.00110              
 -37.44               0.00110              
 -37.48               0.00110              
 -37.52               0.00110              
 -37.56               0.00110              
 -37.6                0.00110              
 -37.64               0.00110              
 -37.68               0.00110              
 -37.72               0.00110              
 -37.76               0.00110              
 -37.8                0.00110              
 -37.84               0.00110              
 -37.88               0.00110              
 -37.92               0.00110              
 -37.96               0.00110              
 -38.                 0.00110              
 -38.04               0.00110              
 -38.08               0.00110              
 -38.12               0.00110              
 -38.16               0.00110              
 -38.2                0.00110              
 -38.24               0.00110              
 -38.28               0.00110              
 -38.32               0.00110              
 -38.36               0.00110              
 -38.4                0.00110              
 -38.44               0.00110              
 -38.48               0.00110              
 -38.52               0.00110              
 -38.56               0.00110              
 -38.6                0.00110              
 -38.64               0.00110              
 -38.68               0.00112              
 -38.72               0.00105              
 -38.76               0.00119              
 -38.8                0.00112              
 -38.84              -0.00084              
##END=
