29Si MAS NMR spectrum of as-synthesized MCM-61 ##freq 1.0002 ##ppm spectr model Q4(0Al) Q4(0Al) Q4(1Al) ----- -70.4000 -0.0317 0.0011 0.0003 0.0004 0.0004 -70.6000 -0.0275 0.0011 0.0003 0.0004 0.0004 -70.8000 -0.0317 0.0011 0.0003 0.0004 0.0004 -71.0000 -0.0348 0.0011 0.0003 0.0004 0.0004 -71.2000 -0.0380 0.0011 0.0003 0.0005 0.0004 -71.4000 -0.0380 0.0011 0.0003 0.0005 0.0004 -71.6000 -0.0380 0.0012 0.0003 0.0005 0.0004 -71.8000 -0.0359 0.0012 0.0003 0.0005 0.0004 -72.0000 -0.0296 0.0012 0.0003 0.0005 0.0004 -72.2000 -0.0264 0.0012 0.0003 0.0005 0.0004 -72.4000 -0.0264 0.0012 0.0003 0.0005 0.0004 -72.6000 -0.0264 0.0012 0.0003 0.0005 0.0005 -72.8000 -0.0264 0.0012 0.0003 0.0005 0.0005 -73.0000 -0.0264 0.0012 0.0003 0.0005 0.0005 -73.2000 -0.0264 0.0013 0.0003 0.0005 0.0005 -73.4000 -0.0264 0.0013 0.0003 0.0005 0.0005 -73.6000 -0.0275 0.0013 0.0003 0.0005 0.0005 -73.8000 -0.0212 0.0013 0.0003 0.0005 0.0005 -74.0000 -0.0212 0.0013 0.0003 0.0005 0.0005 -74.2000 -0.0212 0.0013 0.0003 0.0005 0.0005 -74.4000 -0.0212 0.0013 0.0003 0.0005 0.0005 -74.6000 -0.0254 0.0014 0.0003 0.0005 0.0005 -74.8000 -0.0327 0.0014 0.0003 0.0005 0.0005 -75.0000 -0.0317 0.0014 0.0003 0.0005 0.0005 -75.2000 -0.0275 0.0014 0.0003 0.0006 0.0005 -75.4000 -0.0201 0.0014 0.0003 0.0006 0.0005 -75.6000 -0.0138 0.0014 0.0003 0.0006 0.0005 -75.8000 -0.0096 0.0014 0.0003 0.0006 0.0005 -76.0000 -0.0033 0.0015 0.0003 0.0006 0.0006 -76.2000 0.0009 0.0015 0.0003 0.0006 0.0006 -76.4000 0.0009 0.0015 0.0003 0.0006 0.0006 -76.6000 -0.0044 0.0015 0.0003 0.0006 0.0006 -76.8000 -0.0075 0.0015 0.0003 0.0006 0.0006 -77.0000 -0.0138 0.0016 0.0003 0.0006 0.0006 -77.2000 -0.0159 0.0016 0.0003 0.0006 0.0006 -77.4000 -0.0159 0.0016 0.0004 0.0006 0.0006 -77.6000 -0.0159 0.0016 0.0004 0.0006 0.0006 -77.8000 -0.0159 0.0016 0.0004 0.0006 0.0006 -78.0000 -0.0159 0.0016 0.0004 0.0006 0.0006 -78.2000 -0.0149 0.0017 0.0004 0.0007 0.0006 -78.4000 -0.0107 0.0017 0.0004 0.0007 0.0007 -78.6000 -0.0044 0.0017 0.0004 0.0007 0.0007 -78.8000 0.0009 0.0017 0.0004 0.0007 0.0007 -79.0000 -0.0002 0.0018 0.0004 0.0007 0.0007 -79.2000 -0.0044 0.0018 0.0004 0.0007 0.0007 -79.4000 -0.0044 0.0018 0.0004 0.0007 0.0007 -79.6000 -0.0075 0.0018 0.0004 0.0007 0.0007 -79.8000 -0.0044 0.0018 0.0004 0.0007 0.0007 -80.0000 -0.0075 0.0019 0.0004 0.0007 0.0007 -80.2000 -0.0107 0.0019 0.0004 0.0007 0.0007 -80.4000 -0.0107 0.0019 0.0004 0.0007 0.0008 -80.6000 -0.0044 0.0019 0.0004 0.0008 0.0008 -80.8000 -0.0012 0.0020 0.0004 0.0008 0.0008 -81.0000 0.0040 0.0020 0.0004 0.0008 0.0008 -81.2000 0.0072 0.0020 0.0004 0.0008 0.0008 -81.4000 0.0061 0.0021 0.0004 0.0008 0.0008 -81.6000 0.0061 0.0021 0.0004 0.0008 0.0008 -81.8000 0.0061 0.0021 0.0005 0.0008 0.0008 -82.0000 0.0061 0.0021 0.0005 0.0008 0.0009 -82.2000 0.0051 0.0022 0.0005 0.0008 0.0009 -82.4000 -0.0044 0.0022 0.0005 0.0009 0.0009 -82.6000 -0.0107 0.0022 0.0005 0.0009 0.0009 -82.8000 -0.0170 0.0023 0.0005 0.0009 0.0009 -83.0000 -0.0128 0.0023 0.0005 0.0009 0.0009 -83.2000 -0.0075 0.0023 0.0005 0.0009 0.0009 -83.4000 -0.0044 0.0024 0.0005 0.0009 0.0010 -83.6000 -0.0054 0.0024 0.0005 0.0009 0.0010 -83.8000 -0.0086 0.0024 0.0005 0.0009 0.0010 -84.0000 -0.0117 0.0025 0.0005 0.0010 0.0010 -84.2000 -0.0149 0.0025 0.0005 0.0010 0.0010 -84.4000 -0.0159 0.0026 0.0005 0.0010 0.0010 -84.6000 -0.0170 0.0026 0.0005 0.0010 0.0011 -84.8000 -0.0254 0.0026 0.0005 0.0010 0.0011 -85.0000 -0.0338 0.0027 0.0006 0.0010 0.0011 -85.2000 -0.0380 0.0027 0.0006 0.0010 0.0011 -85.4000 -0.0380 0.0028 0.0006 0.0011 0.0011 -85.6000 -0.0380 0.0028 0.0006 0.0011 0.0012 -85.8000 -0.0306 0.0029 0.0006 0.0011 0.0012 -86.0000 -0.0201 0.0029 0.0006 0.0011 0.0012 -86.2000 -0.0159 0.0030 0.0006 0.0011 0.0012 -86.4000 -0.0159 0.0030 0.0006 0.0011 0.0013 -86.6000 -0.0191 0.0031 0.0006 0.0012 0.0013 -86.8000 -0.0233 0.0031 0.0006 0.0012 0.0013 -87.0000 -0.0264 0.0032 0.0006 0.0012 0.0013 -87.2000 -0.0212 0.0032 0.0006 0.0012 0.0014 -87.4000 -0.0212 0.0033 0.0006 0.0012 0.0014 -87.6000 -0.0149 0.0033 0.0007 0.0013 0.0014 -87.8000 -0.0191 0.0034 0.0007 0.0013 0.0015 -88.0000 -0.0212 0.0035 0.0007 0.0013 0.0015 -88.2000 -0.0212 0.0035 0.0007 0.0013 0.0015 -88.4000 -0.0201 0.0036 0.0007 0.0013 0.0015 -88.6000 -0.0159 0.0036 0.0007 0.0014 0.0016 -88.8000 -0.0149 0.0037 0.0007 0.0014 0.0016 -89.0000 -0.0159 0.0038 0.0007 0.0014 0.0016 -89.2000 -0.0159 0.0039 0.0007 0.0014 0.0017 -89.4000 -0.0222 0.0039 0.0008 0.0015 0.0017 -89.6000 -0.0201 0.0040 0.0008 0.0015 0.0018 -89.8000 -0.0159 0.0041 0.0008 0.0015 0.0018 -90.0000 -0.0033 0.0042 0.0008 0.0015 0.0018 -90.2000 0.0040 0.0043 0.0008 0.0016 0.0019 -90.4000 0.0093 0.0043 0.0008 0.0016 0.0019 -90.6000 0.0114 0.0044 0.0008 0.0016 0.0020 -90.8000 0.0051 0.0045 0.0008 0.0017 0.0020 -91.0000 -0.0012 0.0046 0.0009 0.0017 0.0021 -91.2000 -0.0075 0.0047 0.0009 0.0017 0.0021 -91.4000 -0.0138 0.0048 0.0009 0.0017 0.0022 -91.6000 -0.0159 0.0049 0.0009 0.0018 0.0022 -91.8000 -0.0159 0.0050 0.0009 0.0018 0.0023 -92.0000 -0.0107 0.0051 0.0009 0.0019 0.0024 -92.2000 -0.0096 0.0053 0.0009 0.0019 0.0024 -92.4000 -0.0023 0.0054 0.0010 0.0019 0.0025 -92.6000 0.0040 0.0055 0.0010 0.0020 0.0026 -92.8000 0.0103 0.0056 0.0010 0.0020 0.0026 -93.0000 0.0177 0.0058 0.0010 0.0021 0.0027 -93.2000 0.0177 0.0059 0.0010 0.0021 0.0028 -93.4000 0.0156 0.0061 0.0010 0.0021 0.0029 -93.6000 0.0082 0.0062 0.0011 0.0022 0.0030 -93.8000 0.0019 0.0064 0.0011 0.0022 0.0030 -94.0000 -0.0044 0.0065 0.0011 0.0023 0.0031 -94.2000 -0.0138 0.0067 0.0011 0.0023 0.0032 -94.4000 -0.0159 0.0069 0.0012 0.0024 0.0033 -94.6000 -0.0138 0.0071 0.0012 0.0024 0.0034 -94.8000 -0.0086 0.0072 0.0012 0.0025 0.0036 -95.0000 -0.0012 0.0074 0.0012 0.0026 0.0037 -95.2000 0.0009 0.0076 0.0012 0.0026 0.0038 -95.4000 0.0009 0.0079 0.0013 0.0027 0.0039 -95.6000 0.0009 0.0081 0.0013 0.0027 0.0041 -95.8000 0.0009 0.0083 0.0013 0.0028 0.0042 -96.0000 0.0103 0.0086 0.0013 0.0029 0.0044 -96.2000 0.0198 0.0088 0.0014 0.0029 0.0045 -96.4000 0.0240 0.0091 0.0014 0.0030 0.0047 -96.6000 0.0187 0.0094 0.0014 0.0031 0.0049 -96.8000 0.0177 0.0097 0.0015 0.0032 0.0051 -97.0000 0.0177 0.0101 0.0015 0.0033 0.0053 -97.2000 0.0187 0.0105 0.0015 0.0033 0.0056 -97.4000 0.0240 0.0109 0.0016 0.0034 0.0059 -97.6000 0.0250 0.0113 0.0016 0.0035 0.0062 -97.8000 0.0271 0.0118 0.0016 0.0036 0.0065 -98.0000 0.0281 0.0123 0.0017 0.0037 0.0069 -98.2000 0.0302 0.0129 0.0017 0.0038 0.0074 -98.4000 0.0344 0.0136 0.0018 0.0039 0.0079 -98.6000 0.0439 0.0144 0.0018 0.0041 0.0085 -98.8000 0.0449 0.0153 0.0018 0.0042 0.0093 -99.0000 0.0512 0.0163 0.0019 0.0043 0.0101 -99.2000 0.0512 0.0174 0.0019 0.0044 0.0111 -99.4000 0.0491 0.0188 0.0020 0.0046 0.0122 -99.6000 0.0460 0.0203 0.0020 0.0047 0.0136 -99.8000 0.0449 0.0221 0.0021 0.0049 0.0152 -100.0000 0.0386 0.0242 0.0021 0.0050 0.0170 -100.2000 0.0407 0.0266 0.0022 0.0052 0.0192 -100.4000 0.0460 0.0293 0.0022 0.0054 0.0217 -100.6000 0.0512 0.0325 0.0023 0.0055 0.0247 -100.8000 0.0512 0.0362 0.0024 0.0057 0.0281 -101.0000 0.0512 0.0404 0.0024 0.0059 0.0320 -101.2000 0.0502 0.0451 0.0025 0.0062 0.0365 -101.4000 0.0502 0.0505 0.0026 0.0064 0.0415 -101.6000 0.0565 0.0566 0.0026 0.0066 0.0473 -101.8000 0.0638 0.0634 0.0027 0.0069 0.0538 -102.0000 0.0764 0.0709 0.0028 0.0071 0.0610 -102.2000 0.0859 0.0793 0.0029 0.0074 0.0690 -102.4000 0.0964 0.0885 0.0030 0.0077 0.0778 -102.6000 0.1037 0.0985 0.0031 0.0080 0.0874 -102.8000 0.1069 0.1094 0.0032 0.0083 0.0979 -103.0000 0.1142 0.1211 0.0033 0.0087 0.1091 -103.2000 0.1205 0.1336 0.0034 0.0091 0.1211 -103.4000 0.1300 0.1468 0.0035 0.0095 0.1338 -103.6000 0.1425 0.1606 0.0036 0.0099 0.1471 -103.8000 0.1530 0.1750 0.0037 0.0104 0.1609 -104.0000 0.1656 0.1898 0.0039 0.0109 0.1751 -104.2000 0.1877 0.2049 0.0040 0.0114 0.1895 -104.4000 0.2118 0.2202 0.0041 0.0120 0.2041 -104.6000 0.2381 0.2354 0.0043 0.0127 0.2185 -104.8000 0.2548 0.2504 0.0044 0.0134 0.2326 -105.0000 0.2758 0.2650 0.0046 0.0142 0.2462 -105.2000 0.2947 0.2789 0.0048 0.0151 0.2591 -105.4000 0.3052 0.2920 0.0050 0.0162 0.2709 -105.6000 0.3210 0.3041 0.0052 0.0174 0.2815 -105.8000 0.3283 0.3149 0.0054 0.0189 0.2906 -106.0000 0.3378 0.3244 0.0056 0.0207 0.2981 -106.2000 0.3388 0.3324 0.0058 0.0229 0.3036 -106.4000 0.3409 0.3388 0.0061 0.0256 0.3071 -106.6000 0.3441 0.3438 0.0064 0.0289 0.3085 -106.8000 0.3451 0.3475 0.0067 0.0331 0.3077 -107.0000 0.3483 0.3500 0.0070 0.0383 0.3047 -107.2000 0.3504 0.3518 0.0073 0.0448 0.2997 -107.4000 0.3504 0.3532 0.0076 0.0528 0.2928 -107.6000 0.3472 0.3547 0.0080 0.0627 0.2841 -107.8000 0.3462 0.3570 0.0084 0.0747 0.2738 -108.0000 0.3483 0.3605 0.0089 0.0893 0.2623 -108.2000 0.3556 0.3659 0.0094 0.1068 0.2497 -108.4000 0.3650 0.3738 0.0099 0.1276 0.2363 -108.6000 0.3850 0.3848 0.0105 0.1520 0.2223 -108.8000 0.4007 0.3994 0.0112 0.1802 0.2079 -109.0000 0.4228 0.4179 0.0120 0.2125 0.1934 -109.2000 0.4522 0.4407 0.0130 0.2489 0.1789 -109.4000 0.4857 0.4680 0.0141 0.2893 0.1646 -109.6000 0.5214 0.4996 0.0155 0.3335 0.1507 -109.8000 0.5424 0.5354 0.0171 0.3810 0.1372 -110.0000 0.5760 0.5750 0.0192 0.4314 0.1244 -110.2000 0.6169 0.6178 0.0219 0.4837 0.1122 -110.4000 0.6621 0.6630 0.0252 0.5370 0.1008 -110.6000 0.7019 0.7096 0.0294 0.5901 0.0901 -110.8000 0.7471 0.7565 0.0348 0.6414 0.0803 -111.0000 0.7922 0.8025 0.0416 0.6897 0.0713 -111.2000 0.8426 0.8462 0.0501 0.7331 0.0630 -111.4000 0.8877 0.8862 0.0606 0.7700 0.0556 -111.6000 0.9255 0.9214 0.0736 0.7989 0.0489 -111.8000 0.9633 0.9507 0.0893 0.8184 0.0430 -112.0000 0.9853 0.9734 0.1082 0.8275 0.0377 -112.2000 1.0000 0.9892 0.1305 0.8256 0.0331 -112.4000 1.0000 0.9986 0.1565 0.8131 0.0291 -112.6000 1.0000 1.0021 0.1862 0.7903 0.0255 -112.8000 0.9948 1.0008 0.2198 0.7586 0.0225 -113.0000 0.9885 0.9961 0.2569 0.7193 0.0198 -113.2000 0.9885 0.9890 0.2972 0.6742 0.0176 -113.4000 0.9853 0.9806 0.3402 0.6247 0.0156 -113.6000 0.9790 0.9717 0.3851 0.5726 0.0140 -113.8000 0.9654 0.9626 0.4307 0.5194 0.0126 -114.0000 0.9465 0.9535 0.4759 0.4663 0.0114 -114.2000 0.9328 0.9441 0.5193 0.4145 0.0103 -114.4000 0.9223 0.9336 0.5592 0.3649 0.0095 -114.6000 0.9108 0.9212 0.5940 0.3184 0.0087 -114.8000 0.8982 0.9056 0.6221 0.2755 0.0081 -115.0000 0.8814 0.8859 0.6420 0.2364 0.0075 -115.2000 0.8615 0.8609 0.6525 0.2014 0.0071 -115.4000 0.8363 0.8300 0.6529 0.1705 0.0066 -115.6000 0.8048 0.7932 0.6434 0.1435 0.0063 -115.8000 0.7670 0.7506 0.6243 0.1204 0.0059 -116.0000 0.7135 0.7033 0.5969 0.1007 0.0057 -116.2000 0.6694 0.6522 0.5626 0.0842 0.0054 -116.4000 0.6075 0.5987 0.5231 0.0705 0.0052 -116.6000 0.5277 0.5441 0.4800 0.0592 0.0050 -116.8000 0.4605 0.4896 0.4349 0.0499 0.0048 -117.0000 0.4091 0.4363 0.3893 0.0425 0.0046 -117.2000 0.3682 0.3852 0.3443 0.0365 0.0044 -117.4000 0.3220 0.3370 0.3011 0.0316 0.0042 -117.6000 0.2737 0.2924 0.2605 0.0278 0.0041 -117.8000 0.2276 0.2516 0.2230 0.0246 0.0040 -118.0000 0.2055 0.2151 0.1892 0.0221 0.0038 -118.2000 0.1845 0.1828 0.1591 0.0201 0.0037 -118.4000 0.1593 0.1547 0.1327 0.0184 0.0036 -118.6000 0.1404 0.1306 0.1101 0.0170 0.0035 -118.8000 0.1247 0.1101 0.0909 0.0158 0.0034 -119.0000 0.1142 0.0929 0.0749 0.0148 0.0033 -119.2000 0.1037 0.0788 0.0617 0.0139 0.0032 -119.4000 0.0922 0.0671 0.0509 0.0131 0.0031 -119.6000 0.0796 0.0577 0.0423 0.0124 0.0030 -119.8000 0.0649 0.0501 0.0354 0.0118 0.0029 -120.0000 0.0586 0.0439 0.0299 0.0112 0.0028 -120.2000 0.0523 0.0390 0.0255 0.0107 0.0027 -120.4000 0.0502 0.0350 0.0221 0.0102 0.0027 -120.6000 0.0460 0.0318 0.0194 0.0098 0.0026 -120.8000 0.0397 0.0292 0.0173 0.0093 0.0025 -121.0000 0.0397 0.0270 0.0156 0.0090 0.0024 -121.2000 0.0376 0.0252 0.0142 0.0086 0.0024 -121.4000 0.0365 0.0236 0.0131 0.0082 0.0023 -121.6000 0.0418 0.0223 0.0121 0.0079 0.0023 -121.8000 0.0449 0.0211 0.0113 0.0076 0.0022 -122.0000 0.0449 0.0201 0.0106 0.0073 0.0022 -122.2000 0.0439 0.0191 0.0100 0.0070 0.0021 -122.4000 0.0355 0.0183 0.0094 0.0068 0.0020 -122.6000 0.0344 0.0175 0.0089 0.0065 0.0020 -122.8000 0.0344 0.0167 0.0085 0.0063 0.0019 -123.0000 0.0344 0.0161 0.0081 0.0061 0.0019 -123.2000 0.0386 0.0154 0.0077 0.0059 0.0019 -123.4000 0.0397 0.0148 0.0073 0.0057 0.0018 -123.6000 0.0376 0.0143 0.0070 0.0055 0.0018 -123.8000 0.0302 0.0137 0.0067 0.0053 0.0017 -124.0000 0.0219 0.0132 0.0064 0.0051 0.0017 -124.2000 0.0177 0.0128 0.0061 0.0050 0.0017 -124.4000 0.0208 0.0123 0.0059 0.0048 0.0016 -124.6000 0.0261 0.0119 0.0056 0.0047 0.0016 -124.8000 0.0323 0.0115 0.0054 0.0045 0.0016 -125.0000 0.0355 0.0111 0.0052 0.0044 0.0015 -125.2000 0.0365 0.0107 0.0050 0.0043 0.0015 -125.4000 0.0292 0.0104 0.0048 0.0041 0.0015 -125.6000 0.0292 0.0101 0.0046 0.0040 0.0014 -125.8000 0.0229 0.0098 0.0045 0.0039 0.0014 -126.0000 0.0250 0.0095 0.0043 0.0038 0.0014 -126.2000 0.0323 0.0092 0.0041 0.0037 0.0013 -126.4000 0.0344 0.0089 0.0040 0.0036 0.0013 -126.6000 0.0344 0.0087 0.0039 0.0035 0.0013 -126.8000 0.0302 0.0084 0.0037 0.0034 0.0013 -127.0000 0.0208 0.0082 0.0036 0.0033 0.0012 -127.2000 0.0103 0.0079 0.0035 0.0032 0.0012 -127.4000 0.0051 0.0077 0.0034 0.0031 0.0012 -127.6000 -0.0023 0.0075 0.0033 0.0031 0.0012 -127.8000 -0.0086 0.0073 0.0032 0.0030 0.0012 -128.0000 -0.0159 0.0071 0.0031 0.0029 0.0011 -128.2000 -0.0201 0.0069 0.0030 0.0028 0.0011 -128.4000 -0.0243 0.0068 0.0029 0.0028 0.0011 -128.6000 -0.0243 0.0066 0.0028 0.0027 0.0011 -128.8000 -0.0191 0.0064 0.0027 0.0027 0.0011 -129.0000 -0.0075 0.0063 0.0027 0.0026 0.0010 -129.2000 0.0040 0.0061 0.0026 0.0025 0.0010 -129.4000 0.0114 0.0060 0.0025 0.0025 0.0010 -129.6000 0.0124 0.0058 0.0024 0.0024 0.0010 -129.8000 0.0103 0.0057 0.0024 0.0024 0.0010 -130.0000 0.0030 0.0056 0.0023 0.0023 0.0009 -130.2000 -0.0033 0.0054 0.0022 0.0023 0.0009 -130.4000 -0.0096 0.0053 0.0022 0.0022 0.0009 -130.6000 -0.0107 0.0052 0.0021 0.0022 0.0009 -130.8000 -0.0107 0.0051 0.0021 0.0021 0.0009 -131.0000 -0.0096 0.0050 0.0020 0.0021 0.0009 -131.2000 -0.0128 0.0049 0.0020 0.0020 0.0009 -131.4000 -0.0159 0.0048 0.0019 0.0020 0.0008 -131.6000 -0.0159 0.0047 0.0019 0.0020 0.0008 -131.8000 -0.0138 0.0046 0.0018 0.0019 0.0008 -132.0000 -0.0054 0.0045 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