Ripmeester et al. J. Chem. Soc., Chem. Commun., 0, 608-610 (1988) Figure 2 ##freq 1 ##col_ ppm Spectrum Model Si1/Si2/Si3 Si1/Si2/Si3 Si1/Si2/Si3 Si4 Si4 ----- -107.62 0.16188 0.01722 0.00121 0.00140 0.00143 0.00411 0.00905 -107.64 0.15755 0.01735 0.00122 0.00140 0.00143 0.00412 0.00915 -107.66 0.15253 0.01749 0.00122 0.00141 0.00144 0.00414 0.00926 -107.68 0.15266 0.01763 0.00122 0.00141 0.00144 0.00416 0.00936 -107.7 0.15401 0.01777 0.00123 0.00141 0.00145 0.00418 0.00947 -107.72 0.15099 0.01791 0.00123 0.00142 0.00145 0.00420 0.00958 -107.74 0.14535 0.01805 0.00124 0.00142 0.00146 0.00422 0.00969 -107.76 0.14499 0.01820 0.00124 0.00143 0.00146 0.00424 0.00981 -107.78 0.14565 0.01835 0.00124 0.00143 0.00147 0.00426 0.00992 -107.8 0.14534 0.01850 0.00125 0.00144 0.00147 0.00428 0.01004 -107.82 0.14536 0.01865 0.00125 0.00144 0.00148 0.00430 0.01016 -107.84 0.14581 0.01881 0.00125 0.00145 0.00149 0.00432 0.01028 -107.86 0.14410 0.01896 0.00126 0.00145 0.00149 0.00434 0.01040 -107.88 0.13675 0.01912 0.00126 0.00146 0.00150 0.00436 0.01053 -107.9 0.12488 0.01929 0.00126 0.00146 0.00150 0.00438 0.01066 -107.92 0.12130 0.01945 0.00127 0.00147 0.00151 0.00440 0.01079 -107.94 0.12294 0.01962 0.00127 0.00147 0.00151 0.00442 0.01092 -107.96 0.12263 0.01979 0.00128 0.00148 0.00152 0.00444 0.01106 -107.98 0.12252 0.01996 0.00128 0.00148 0.00152 0.00447 0.01119 -108. 0.12268 0.02014 0.00128 0.00149 0.00153 0.00449 0.01133 -108.02 0.12255 0.02032 0.00129 0.00149 0.00153 0.00451 0.01148 -108.04 0.12245 0.02050 0.00129 0.00150 0.00154 0.00453 0.01162 -108.06 0.12342 0.02068 0.00129 0.00150 0.00154 0.00455 0.01177 -108.08 0.12060 0.02087 0.00130 0.00151 0.00155 0.00457 0.01192 -108.1 0.11492 0.02106 0.00130 0.00151 0.00156 0.00460 0.01208 -108.12 0.11458 0.02125 0.00131 0.00152 0.00156 0.00462 0.01223 -108.14 0.11519 0.02145 0.00131 0.00152 0.00157 0.00464 0.01239 -108.16 0.11498 0.02165 0.00131 0.00153 0.00157 0.00466 0.01256 -108.18 0.11502 0.02186 0.00132 0.00153 0.00158 0.00469 0.01272 -108.2 0.11473 0.02206 0.00132 0.00154 0.00158 0.00471 0.01289 -108.22 0.11572 0.02227 0.00133 0.00154 0.00159 0.00473 0.01307 -108.24 0.11450 0.02249 0.00133 0.00155 0.00159 0.00476 0.01324 -108.26 0.10801 0.02271 0.00133 0.00155 0.00160 0.00478 0.01342 -108.28 0.11062 0.02293 0.00134 0.00156 0.00161 0.00480 0.01361 -108.3 0.11590 0.02316 0.00134 0.00156 0.00161 0.00483 0.01379 -108.32 0.11505 0.02339 0.00135 0.00157 0.00162 0.00485 0.01398 -108.34 0.11498 0.02362 0.00135 0.00157 0.00162 0.00487 0.01418 -108.36 0.11459 0.02386 0.00135 0.00158 0.00163 0.00490 0.01438 -108.38 0.11554 0.02410 0.00136 0.00158 0.00164 0.00492 0.01458 -108.4 0.12117 0.02435 0.00136 0.00159 0.00164 0.00495 0.01479 -108.42 0.12776 0.02460 0.00137 0.00159 0.00165 0.00497 0.01500 -108.44 0.13078 0.02486 0.00137 0.00160 0.00165 0.00500 0.01522 -108.46 0.13019 0.02512 0.00137 0.00161 0.00166 0.00502 0.01544 -108.48 0.13013 0.02539 0.00138 0.00161 0.00167 0.00505 0.01567 -108.5 0.13025 0.02566 0.00138 0.00162 0.00167 0.00507 0.01590 -108.52 0.13020 0.02594 0.00139 0.00162 0.00168 0.00510 0.01613 -108.54 0.13021 0.02623 0.00139 0.00163 0.00169 0.00513 0.01638 -108.56 0.13021 0.02652 0.00140 0.00163 0.00169 0.00515 0.01662 -108.58 0.13021 0.02681 0.00140 0.00164 0.00170 0.00518 0.01687 -108.6 0.13021 0.02711 0.00140 0.00164 0.00170 0.00521 0.01713 -108.62 0.13021 0.02742 0.00141 0.00165 0.00171 0.00523 0.01740 -108.64 0.13019 0.02773 0.00141 0.00166 0.00172 0.00526 0.01767 -108.66 0.13024 0.02805 0.00142 0.00166 0.00172 0.00529 0.01794 -108.68 0.13022 0.02838 0.00142 0.00167 0.00173 0.00532 0.01823 -108.7 0.12999 0.02871 0.00143 0.00167 0.00174 0.00534 0.01852 -108.72 0.13090 0.02906 0.00143 0.00168 0.00174 0.00537 0.01881 -108.74 0.12941 0.02940 0.00143 0.00168 0.00175 0.00540 0.01912 -108.76 0.12338 0.02976 0.00144 0.00169 0.00176 0.00543 0.01943 -108.78 0.12244 0.03013 0.00144 0.00170 0.00176 0.00546 0.01975 -108.8 0.12144 0.03050 0.00145 0.00170 0.00177 0.00548 0.02007 -108.82 0.11476 0.03088 0.00145 0.00171 0.00178 0.00551 0.02041 -108.84 0.10769 0.03127 0.00146 0.00171 0.00178 0.00554 0.02075 -108.86 0.11105 0.03167 0.00146 0.00172 0.00179 0.00557 0.02111 -108.88 0.11459 0.03208 0.00147 0.00173 0.00180 0.00560 0.02147 -108.9 0.10805 0.03250 0.00147 0.00173 0.00180 0.00563 0.02184 -108.92 0.10660 0.03293 0.00148 0.00174 0.00181 0.00566 0.02222 -108.94 0.10768 0.03337 0.00148 0.00175 0.00182 0.00569 0.02262 -108.96 0.10736 0.03383 0.00149 0.00175 0.00183 0.00572 0.02302 -108.98 0.10736 0.03429 0.00149 0.00176 0.00183 0.00576 0.02344 -109. 0.10743 0.03477 0.00149 0.00176 0.00184 0.00579 0.02387 -109.02 0.10736 0.03526 0.00150 0.00177 0.00185 0.00582 0.02431 -109.04 0.10738 0.03577 0.00150 0.00178 0.00185 0.00585 0.02476 -109.06 0.10763 0.03629 0.00151 0.00178 0.00186 0.00588 0.02523 -109.08 0.10667 0.03682 0.00151 0.00179 0.00187 0.00591 0.02572 -109.1 0.10824 0.03737 0.00152 0.00180 0.00188 0.00595 0.02622 -109.12 0.11432 0.03794 0.00152 0.00180 0.00188 0.00598 0.02673 -109.14 0.11465 0.03853 0.00153 0.00181 0.00189 0.00601 0.02727 -109.16 0.11733 0.03914 0.00153 0.00182 0.00190 0.00605 0.02782 -109.18 0.12260 0.03976 0.00154 0.00182 0.00191 0.00608 0.02840 -109.2 0.11712 0.04041 0.00154 0.00183 0.00191 0.00611 0.02899 -109.22 0.11401 0.04108 0.00155 0.00184 0.00192 0.00615 0.02961 -109.24 0.11517 0.04178 0.00155 0.00184 0.00193 0.00618 0.03025 -109.26 0.11499 0.04250 0.00156 0.00185 0.00194 0.00622 0.03092 -109.28 0.11538 0.04325 0.00156 0.00186 0.00194 0.00625 0.03162 -109.3 0.11386 0.04403 0.00157 0.00186 0.00195 0.00629 0.03234 -109.32 0.11585 0.04485 0.00157 0.00187 0.00196 0.00632 0.03310 -109.34 0.12768 0.04569 0.00158 0.00188 0.00197 0.00636 0.03389 -109.36 0.13184 0.04658 0.00158 0.00188 0.00198 0.00640 0.03472 -109.38 0.12953 0.04750 0.00159 0.00189 0.00198 0.00643 0.03559 -109.4 0.13008 0.04847 0.00159 0.00190 0.00199 0.00647 0.03649 -109.42 0.13491 0.04948 0.00160 0.00191 0.00200 0.00651 0.03745 -109.44 0.14179 0.05053 0.00160 0.00191 0.00201 0.00654 0.03845 -109.46 0.14561 0.05164 0.00161 0.00192 0.00202 0.00658 0.03950 -109.48 0.14509 0.05281 0.00162 0.00193 0.00202 0.00662 0.04060 -109.5 0.14958 0.05404 0.00162 0.00193 0.00203 0.00666 0.04177 -109.52 0.15436 0.05532 0.00163 0.00194 0.00204 0.00670 0.04300 -109.54 0.15287 0.05668 0.00163 0.00195 0.00205 0.00674 0.04430 -109.56 0.14694 0.05811 0.00164 0.00196 0.00206 0.00678 0.04567 -109.58 0.14480 0.05962 0.00164 0.00196 0.00207 0.00682 0.04711 -109.6 0.14541 0.06121 0.00165 0.00197 0.00207 0.00686 0.04864 -109.62 0.14526 0.06289 0.00165 0.00198 0.00208 0.00690 0.05026 -109.64 0.14706 0.06467 0.00166 0.00199 0.00209 0.00694 0.05198 -109.66 0.14023 0.06655 0.00166 0.00199 0.00210 0.00698 0.05380 -109.68 0.12962 0.06854 0.00167 0.00200 0.00211 0.00702 0.05572 -109.7 0.13006 0.07064 0.00168 0.00201 0.00212 0.00706 0.05776 -109.72 0.12736 0.07287 0.00168 0.00202 0.00213 0.00711 0.05992 -109.74 0.12014 0.07523 0.00169 0.00202 0.00214 0.00715 0.06221 -109.76 0.11510 0.07772 0.00169 0.00203 0.00214 0.00719 0.06464 -109.78 0.11464 0.08037 0.00170 0.00204 0.00215 0.00723 0.06722 -109.8 0.11515 0.08317 0.00170 0.00205 0.00216 0.00728 0.06995 -109.82 0.11497 0.08613 0.00171 0.00206 0.00217 0.00732 0.07285 -109.84 0.11498 0.08927 0.00172 0.00206 0.00218 0.00737 0.07592 -109.86 0.11506 0.09259 0.00172 0.00207 0.00219 0.00741 0.07917 -109.88 0.11486 0.09610 0.00173 0.00208 0.00220 0.00746 0.08262 -109.9 0.11503 0.09982 0.00173 0.00209 0.00221 0.00751 0.08626 -109.92 0.11574 0.10375 0.00174 0.00210 0.00222 0.00755 0.09012 -109.94 0.11146 0.10790 0.00175 0.00210 0.00223 0.00760 0.09420 -109.96 0.10675 0.11228 0.00175 0.00211 0.00224 0.00765 0.09851 -109.98 0.10727 0.11690 0.00176 0.00212 0.00225 0.00769 0.10306 -110. 0.10755 0.12178 0.00176 0.00213 0.00226 0.00774 0.10787 -110.02 0.10733 0.12691 0.00177 0.00214 0.00227 0.00779 0.11293 -110.04 0.10740 0.13232 0.00178 0.00215 0.00228 0.00784 0.11826 -110.06 0.10740 0.13801 0.00178 0.00215 0.00229 0.00789 0.12387 -110.08 0.10738 0.14398 0.00179 0.00216 0.00230 0.00794 0.12978 -110.1 0.10741 0.15026 0.00179 0.00217 0.00231 0.00799 0.13597 -110.12 0.10740 0.15684 0.00180 0.00218 0.00232 0.00804 0.14248 -110.14 0.10727 0.16373 0.00181 0.00219 0.00233 0.00809 0.1493 -110.16 0.10777 0.17094 0.00181 0.00220 0.00234 0.00815 0.15643 -110.18 0.10694 0.17848 0.00182 0.00221 0.00235 0.00820 0.16389 -110.2 0.10630 0.18636 0.00183 0.00222 0.00236 0.00825 0.17169 -110.22 0.11684 0.19457 0.00183 0.00222 0.00237 0.00830 0.17982 -110.24 0.12340 0.20312 0.00184 0.00223 0.00238 0.00836 0.18829 -110.26 0.12276 0.21201 0.00184 0.00224 0.00239 0.00841 0.19711 -110.28 0.13315 0.22125 0.00185 0.00225 0.00240 0.00847 0.20626 -110.3 0.14548 0.23084 0.00186 0.00226 0.00241 0.00852 0.21577 -110.32 0.15585 0.24077 0.00186 0.00227 0.00242 0.00858 0.22561 -110.34 0.16692 0.25104 0.00187 0.00228 0.00243 0.00864 0.23580 -110.36 0.17841 0.26165 0.00188 0.00229 0.00244 0.00870 0.24633 -110.38 0.18748 0.27259 0.00188 0.00230 0.00245 0.00875 0.25718 -110.4 0.19113 0.28386 0.00189 0.00231 0.00246 0.00881 0.26836 -110.42 0.19056 0.29544 0.00190 0.00232 0.00247 0.00887 0.27986 -110.44 0.19627 0.30733 0.00190 0.00233 0.00249 0.00893 0.29167 -110.46 0.21371 0.31952 0.00191 0.00234 0.00250 0.00899 0.30376 -110.48 0.23603 0.33198 0.00192 0.00235 0.00251 0.00905 0.31613 -110.5 0.24846 0.34470 0.00193 0.00236 0.00252 0.00911 0.32877 -110.52 0.25711 0.35767 0.00193 0.00236 0.00253 0.00918 0.34164 -110.54 0.27025 0.37085 0.00194 0.00237 0.00254 0.00924 0.35473 -110.56 0.28730 0.38423 0.00195 0.00238 0.00255 0.00930 0.36802 -110.58 0.29818 0.39777 0.00195 0.00239 0.00257 0.00937 0.38147 -110.6 0.31332 0.41146 0.00196 0.00240 0.00258 0.00943 0.39506 -110.62 0.34485 0.42524 0.00197 0.00241 0.00259 0.00950 0.40875 -110.64 0.38961 0.43910 0.00197 0.00242 0.00260 0.00956 0.42251 -110.66 0.42584 0.45298 0.00198 0.00244 0.00261 0.00963 0.4363 -110.68 0.44659 0.46684 0.00199 0.00245 0.00263 0.00970 0.45006 -110.7 0.47429 0.48064 0.00200 0.00246 0.00264 0.00977 0.46376 -110.72 0.54459 0.49433 0.00200 0.00247 0.00265 0.00984 0.47735 -110.74 0.60143 0.50785 0.00201 0.00248 0.00266 0.00990 0.49077 -110.76 0.63788 0.52114 0.00202 0.00249 0.00268 0.00998 0.50396 -110.78 0.69533 0.53415 0.00203 0.00250 0.00269 0.01005 0.51687 -110.8 0.72948 0.54680 0.00203 0.00251 0.00270 0.01012 0.52942 -110.82 0.74370 0.55904 0.00204 0.00252 0.00271 0.01019 0.54155 -110.84 0.76790 0.57079 0.00205 0.00253 0.00273 0.01027 0.55320 -110.86 0.81187 0.58199 0.00206 0.00254 0.00274 0.01034 0.56429 -110.88 0.84919 0.59255 0.00206 0.00255 0.00275 0.01041 0.57475 -110.9 0.87206 0.60242 0.00207 0.00256 0.00277 0.01049 0.58451 -110.92 0.88885 0.61152 0.00208 0.00257 0.00278 0.01057 0.59350 -110.94 0.89519 0.61977 0.00209 0.00259 0.00279 0.01065 0.60164 -110.96 0.90305 0.62713 0.00210 0.00260 0.00281 0.01072 0.60888 -110.98 0.91389 0.63352 0.00210 0.00261 0.00282 0.01080 0.61516 -111. 0.91418 0.63889 0.00211 0.00262 0.00283 0.01088 0.62042 -111.02 0.91402 0.64320 0.00212 0.00263 0.00285 0.01096 0.62462 -111.04 0.91240 0.64640 0.00213 0.00264 0.00286 0.01105 0.62771 -111.06 0.90639 0.64848 0.00214 0.00265 0.00287 0.01113 0.62967 -111.08 0.90612 0.64941 0.00214 0.00267 0.00289 0.01121 0.63048 -111.1 0.90359 0.64918 0.00215 0.00268 0.00290 0.01130 0.63013 -111.12 0.88799 0.64780 0.00216 0.00269 0.00292 0.01138 0.62863 -111.14 0.85982 0.64528 0.00217 0.00270 0.00293 0.01147 0.62599 -111.16 0.83672 0.64164 0.00218 0.00271 0.00295 0.01156 0.62223 -111.18 0.81258 0.63693 0.00218 0.00273 0.00296 0.01165 0.61739 -111.2 0.78499 0.63118 0.00219 0.00274 0.00297 0.01174 0.61151 -111.22 0.7693 0.62444 0.00220 0.00275 0.00299 0.01183 0.60465 -111.24 0.74460 0.61678 0.00221 0.00276 0.00300 0.01192 0.59686 -111.26 0.70885 0.60825 0.00222 0.00277 0.00302 0.01201 0.58820 -111.28 0.67610 0.59892 0.00223 0.00279 0.00303 0.01211 0.57874 -111.3 0.64387 0.58886 0.00224 0.00280 0.00305 0.01220 0.56855 -111.32 0.60968 0.57815 0.00224 0.00281 0.00306 0.01230 0.55771 -111.34 0.58613 0.56685 0.00225 0.00282 0.00308 0.01240 0.54628 -111.36 0.58383 0.55504 0.00226 0.00284 0.00310 0.01250 0.53433 -111.38 0.55425 0.54278 0.00227 0.00285 0.00311 0.01260 0.52193 -111.4 0.50577 0.53015 0.00228 0.00286 0.00313 0.01270 0.50916 -111.42 0.47459 0.51720 0.00229 0.00288 0.00314 0.01280 0.49608 -111.44 0.46152 0.50401 0.00230 0.00289 0.00316 0.01290 0.48274 -111.46 0.45129 0.49063 0.00231 0.00290 0.00317 0.01301 0.46922 -111.48 0.43121 0.47711 0.00232 0.00292 0.00319 0.01311 0.45555 -111.5 0.40266 0.46351 0.00232 0.00293 0.00321 0.01322 0.44181 -111.52 0.38401 0.44988 0.00233 0.00294 0.00322 0.01333 0.42802 -111.54 0.36566 0.43625 0.00234 0.00296 0.00324 0.01344 0.41425 -111.56 0.34359 0.42268 0.00235 0.00297 0.00326 0.01355 0.40053 -111.58 0.33724 0.40920 0.00236 0.00298 0.00327 0.01366 0.38689 -111.6 0.33001 0.39584 0.00237 0.00300 0.00329 0.01378 0.37338 -111.62 0.31837 0.38264 0.00238 0.00301 0.00331 0.01389 0.36003 -111.64 0.31300 0.36963 0.00239 0.00303 0.00333 0.01401 0.34685 -111.66 0.31320 0.35682 0.00240 0.00304 0.00334 0.01413 0.33389 -111.68 0.31083 0.34425 0.00241 0.00306 0.00336 0.01425 0.32116 -111.7 0.30493 0.33194 0.00242 0.00307 0.00338 0.01437 0.30868 -111.72 0.30401 0.3199 0.00243 0.00308 0.00340 0.01450 0.29647 -111.74 0.30899 0.30814 0.00244 0.00310 0.00341 0.01462 0.28455 -111.76 0.31336 0.29669 0.00245 0.00311 0.00343 0.01475 0.27293 -111.78 0.31285 0.28555 0.00246 0.00313 0.00345 0.01487 0.26162 -111.8 0.31268 0.27473 0.00247 0.00314 0.00347 0.01500 0.25063 -111.82 0.31263 0.26425 0.00248 0.00316 0.00349 0.01514 0.23997 -111.84 0.31290 0.25410 0.00249 0.00317 0.00351 0.01527 0.22965 -111.86 0.31345 0.24430 0.00250 0.00319 0.00353 0.01540 0.21966 -111.88 0.30831 0.23484 0.00251 0.00320 0.00354 0.01554 0.21002 -111.9 0.30503 0.22573 0.00252 0.00322 0.00356 0.01568 0.20073 -111.92 0.30525 0.21696 0.00253 0.00324 0.00358 0.01582 0.19178 -111.94 0.29561 0.20854 0.00254 0.00325 0.00360 0.01596 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