##TITLE=              31P MAS NMR spectrum of as-made STA-15 (with tetrapropylammonium hydroxide template)
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Han et al. Chem. Mater., 22, 338-346 (2010) Figure 4
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/22 11:08:02
##SOURCE REFERENCE=   SAF-31P-Han-2010-asmade
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              SAF
##NAMES=              STA-15
##SAMPLE DESCRIPTION= STA-15, as-made

$$Bibliographic information 
##$AUTHORS=           Han, Z., Lorena Picone, A., Slawin, A.M., Seymour, V.R., Ashbrook, S.E., Zhou, W., Thompson, S.P., Parker, J.E., Wright, P.A.
##$TITLE=             Novel large-pore aluminophosphate molecular sieve STA-15 prepared using the tetrapropylammonium cation as a structure directing agent
##$JOURNAL=           Chemistry of Materials
##$VOLUME=            22
##$PAGES=             338-346
##$YEAR=              2010
##$DOI=               10.1021/cm902528y
##$FIGURE=            Figure 4

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         4
##$PEAK LABELS=        A          B          C          D         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -32.5534   -32.3534   -31.2419   -28.3726   
##$PEAK AREAS=         1.         1.         1.         1.        
##$PEAK WIDTHS=        4.72551    4.72551    4.72551    4.72551   
##$PEAK SHAPES=        0          0          0          0         
##$NUMBERING REF=     Han et al. Chem. Mater., 22, 338-346 (2010)
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           Peak assignments are not available

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 243.0
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     10000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              4.6                  
##LASTX=              -54.5                 
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            198
##FIRSTY=              0.00965              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  4.6                 0.00965              
  4.3                 0.00820              
  4.                  0.00809              
  3.7                 0.00900              
  3.4                 0.00864              
  3.1                 0.00642              
  2.8                 0.00558              
  2.5                 0.00625              
  2.2                 0.00646              
  1.9                 0.00722              
  1.6                 0.00835              
  1.3                 0.00728              
  1.                  0.00551              
  0.7                 0.00512              
  0.4                 0.00487              
  0.1                 0.00302              
 -0.2                 0.00229              
 -0.5                 0.00477              
 -0.8                 0.00485              
 -1.1                 0.00321              
 -1.4                 0.00446              
 -1.7                 0.00691              
 -2.                  0.00604              
 -2.3                 0.00404              
 -2.6                 0.00688              
 -2.9                 0.00912              
 -3.2                 0.00693              
 -3.5                 0.00543              
 -3.8                 0.00651              
 -4.1                 0.00735              
 -4.4                 0.00625              
 -4.7                 0.00510              
 -5                   0.00567              
 -5.3                 0.00790              
 -5.6                 0.01023              
 -5.9                 0.00975              
 -6.2                 0.00947              
 -6.5                 0.01022              
 -6.8                 0.01049              
 -7.1                 0.01088              
 -7.4                 0.01260              
 -7.7                 0.01458              
 -8                   0.01573              
 -8.3                 0.01743              
 -8.6                 0.01856              
 -8.9                 0.01859              
 -9.2                 0.01957              
 -9.5                 0.02080              
 -9.8                 0.02125              
 -10.1                0.02124              
 -10.4                0.02102              
 -10.7                0.02015              
 -11                  0.02061              
 -11.3                0.02361              
 -11.6                0.02617              
 -11.9                0.02740              
 -12.2                0.02866              
 -12.5                0.02932              
 -12.8                0.02985              
 -13.1                0.03173              
 -13.4                0.03336              
 -13.7                0.03380              
 -14.                 0.03457              
 -14.3                0.03629              
 -14.6                0.03837              
 -14.9                0.04066              
 -15.2                0.04431              
 -15.5                0.04805              
 -15.8                0.05138              
 -16.1                0.05398              
 -16.4                0.05509              
 -16.7                0.05636              
 -17.                 0.05927              
 -17.3                0.06365              
 -17.6                0.06859              
 -17.9                0.07218              
 -18.2                0.07344              
 -18.5                0.07367              
 -18.8                0.07367              
 -19.1                0.07379              
 -19.4                0.07539              
 -19.7                0.07846              
 -20.                 0.08132              
 -20.3                0.08368              
 -20.6                0.08597              
 -20.9                0.08812              
 -21.2                0.08871              
 -21.5                0.08768              
 -21.8                0.08712              
 -22.1                0.08818              
 -22.4                0.09160              
 -22.7                0.09556              
 -23.                 0.09863              
 -23.3                0.10181              
 -23.6                0.10552              
 -23.9                0.10984              
 -24.2                0.11483              
 -24.5                0.12138              
 -24.8                0.12955              
 -25.1                0.13674              
 -25.4                0.14567              
 -25.7                0.15719              
 -26.                 0.17028              
 -26.3                0.18623              
 -26.6                0.20344              
 -26.9                0.22224              
 -27.2                0.24421              
 -27.5                0.27049              
 -27.8                0.29802              
 -28.1                0.32987              
 -28.4                0.36531              
 -28.7                0.39988              
 -29.                 0.43473              
 -29.3                0.47026              
 -29.6                0.50173              
 -29.9                0.52896              
 -30.2                0.55020              
 -30.5                0.56983              
 -30.8                0.58939              
 -31.1                0.60599              
 -31.4                0.62071              
 -31.7                0.63078              
 -32.                 0.63130              
 -32.3                0.62292              
 -32.6                0.60349              
 -32.9                0.57218              
 -33.2                0.53437              
 -33.5                0.48880              
 -33.8                0.43673              
 -34.1                0.38317              
 -34.4                0.32537              
 -34.7                0.27277              
 -35.                 0.22330              
 -35.3                0.17869              
 -35.6                0.14374              
 -35.9                0.11103              
 -36.2                0.08734              
 -36.5                0.06613              
 -36.8                0.04876              
 -37.1                0.03652              
 -37.4                0.02753              
 -37.7                0.02227              
 -38                  0.01950              
 -38.3                0.01590              
 -38.6                0.01211              
 -38.9                0.01069              
 -39.2                0.01049              
 -39.5                0.01049              
 -39.8                0.01049              
 -40.1                0.00977              
 -40.4                0.00707              
 -40.7                0.00533              
 -41.                 0.00597              
 -41.3                0.00594              
 -41.6                0.00534              
 -41.9                0.00660              
 -42.2                0.00855              
 -42.5                0.00803              
 -42.8                0.00669              
 -43.1                0.00646              
 -43.4                0.00724              
 -43.7                0.00864              
 -44.                 0.00730              
 -44.3                0.00457              
 -44.6                0.00405              
 -44.9                0.00466              
 -45.2                0.00358              
 -45.5                0.00326              
 -45.8                0.00648              
 -46.1                0.00734              
 -46.4                0.00484              
 -46.7                0.00473              
 -47.                 0.00571              
 -47.3                0.00566              
 -47.6                0.00537              
 -47.9                0.00719              
 -48.2                0.00834              
 -48.5                0.00732              
 -48.8                0.00667              
 -49.1                0.00570              
 -49.4                0.00466              
 -49.7                0.00526              
 -50.                 0.00771              
 -50.3                0.00825              
 -50.6                0.00811              
 -50.9                0.00886              
 -51.2                0.00782              
 -51.5                0.00586              
 -51.8                0.00515              
 -52.1                0.00565              
 -52.4                0.00789              
 -52.7                0.00919              
 -53.                 0.00910              
 -53.3                0.00859              
 -53.6                0.00776              
 -53.9                0.00791              
 -54.2                0.00888              
 -54.5                0.00915              
##END=
