##TITLE=              29Si MAS NMR spectrum of calcined pure silica HPM-1
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Rojas and Camblor. Angew. Chem. Int. Ed., 51, 3854-3856 (2012) Figure 1
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University College
##LONG DATE=          2019/08/08 15:31:38
##SOURCE REFERENCE=   STW-29Si-Rojas-2012
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              STW
##NAMES=              HPM-1
##SAMPLE DESCRIPTION= HPM-1, calcined

$$Bibliographic information 
##$AUTHORS=           Rojas, A., Camblor, M.A.
##$TITLE=             A pure silica chiral polymorph with helical pores
##$JOURNAL=           Angewandte Chemie, International Edition
##$VOLUME=            51
##$PAGES=             3854-3856
##$YEAR=              2012
##$DOI=               10.1002/anie.201108753
##$FIGURE=            Figure 1

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         5
##$PEAK LABELS=        A          B          C          D          E         
##$PEAK TSITES=       
##$PEAK POSITIONS=    -115.067   -109.395   -108.688   -108.579   -107.742   
##$PEAK AREAS=         1.         1.         1.         1.         1.        
##$PEAK WIDTHS=        0.54507    0.49941    0.51478    0.51478    0.43335   
##$PEAK SHAPES=        1          1          1          1          1         
##$NUMBERING REF=     
##$ASSIGN REF=        
##$ASSIGN METHOD=     
##$COMMENT=           

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^29Si
##.OBSERVE FREQUENCY= 
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=             -96.                  
##LASTX=              -122.98               
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1350
##FIRSTY=             -0.06420              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
 -96.                -0.06420              
 -96.02              -0.06656              
 -96.04              -0.07129              
 -96.06              -0.07378              
 -96.08              -0.06912              
 -96.1               -0.05317              
 -96.12              -0.03099              
 -96.14              -0.02001              
 -96.16              -0.01617              
 -96.18              -0.00772              
 -96.2                0.00388              
 -96.22               0.01583              
 -96.24               0.02601              
 -96.26               0.03220              
 -96.28               0.03476              
 -96.3                0.03733              
 -96.32               0.04062              
 -96.34               0.04375              
 -96.36               0.04585              
 -96.38               0.04958              
 -96.4                0.05818              
 -96.42               0.06734              
 -96.44               0.07275              
 -96.46               0.07316              
 -96.48               0.07360              
 -96.5                0.07698              
 -96.52               0.07833              
 -96.54               0.07781              
 -96.56               0.07642              
 -96.58               0.06683              
 -96.6                0.05069              
 -96.62               0.03791              
 -96.64               0.02658              
 -96.66               0.01442              
 -96.68               0.00436              
 -96.7               -0.00393              
 -96.72              -0.01260              
 -96.74              -0.02315              
 -96.76              -0.03556              
 -96.78              -0.04823              
 -96.8               -0.05804              
 -96.82              -0.06040              
 -96.84              -0.05108              
 -96.86              -0.03805              
 -96.88              -0.02923              
 -96.9               -0.02100              
 -96.92              -0.01172              
 -96.94              -0.00239              
 -96.96               0.00524              
 -96.98               0.01087              
 -97.                 0.01528              
 -97.02               0.01580              
 -97.04               0.00989              
 -97.06              -0.00273              
 -97.08              -0.02453              
 -97.1               -0.05502              
 -97.12              -0.08173              
 -97.14              -0.10508              
 -97.16              -0.13442              
 -97.18              -0.15359              
 -97.2               -0.15197              
 -97.22              -0.13834              
 -97.24              -0.11683              
 -97.26              -0.08985              
 -97.28              -0.06322              
 -97.3               -0.04059              
 -97.32              -0.02119              
 -97.34               0.00449              
 -97.36               0.03201              
 -97.38               0.04154              
 -97.4                0.04710              
 -97.42               0.06296              
 -97.44               0.07542              
 -97.46               0.08308              
 -97.48               0.09370              
 -97.5                0.10999              
 -97.52               0.12818              
 -97.54               0.13928              
 -97.56               0.13708              
 -97.58               0.12406              
 -97.6                0.11392              
 -97.62               0.10475              
 -97.64               0.08813              
 -97.66               0.06418              
 -97.68               0.04081              
 -97.7                0.02769              
 -97.72               0.01629              
 -97.74               0.00671              
 -97.76               0.01557              
 -97.78               0.03361              
 -97.8                0.04588              
 -97.82               0.05399              
 -97.84               0.05894              
 -97.86               0.05989              
 -97.88               0.05759              
 -97.9                0.05446              
 -97.92               0.05375              
 -97.94               0.05422              
 -97.96               0.05415              
 -97.98               0.05431              
 -98.                 0.05408              
 -98.02               0.05330              
 -98.04               0.05648              
 -98.06               0.06307              
 -98.08               0.06646              
 -98.1                0.06031              
 -98.12               0.04725              
 -98.14               0.04138              
 -98.16               0.03296              
 -98.18               0.01273              
 -98.2                0.00645              
 -98.22               0.01598              
 -98.24               0.02366              
 -98.26               0.03710              
 -98.28               0.05613              
 -98.3                0.06219              
 -98.32               0.05027              
 -98.34               0.02593              
 -98.36               0.00240              
 -98.38              -0.01248              
 -98.4               -0.01849              
 -98.42              -0.02544              
 -98.44              -0.03135              
 -98.46              -0.02230              
 -98.48              -0.00932              
 -98.5               -0.00133              
 -98.52               0.01300              
 -98.54               0.03231              
 -98.56               0.04824              
 -98.58               0.05893              
 -98.6                0.06355              
 -98.62               0.06277              
 -98.64               0.06567              
 -98.66               0.07544              
 -98.68               0.08368              
 -98.7                0.09441              
 -98.72               0.11267              
 -98.74               0.12918              
 -98.76               0.13932              
 -98.78               0.14395              
 -98.8                0.14322              
 -98.82               0.13982              
 -98.84               0.13775              
 -98.86               0.12527              
 -98.88               0.09930              
 -98.9                0.08620              
 -98.92               0.08213              
 -98.94               0.06931              
 -98.96               0.06219              
 -98.98               0.06735              
 -99.                 0.07531              
 -99.02               0.07739              
 -99.04               0.07095              
 -99.06               0.06221              
 -99.08               0.05301              
 -99.1                0.04346              
 -99.12               0.03716              
 -99.14               0.03102              
 -99.16               0.01761              
 -99.18               0.00099              
 -99.2               -0.01094              
 -99.22              -0.01139              
 -99.24              -0.00675              
 -99.26              -0.00428              
 -99.28               0.00145              
 -99.3                0.01161              
 -99.32               0.02202              
 -99.34               0.02663              
 -99.36               0.02580              
 -99.38               0.02724              
 -99.4                0.03174              
 -99.42               0.03767              
 -99.44               0.04446              
 -99.46               0.04965              
 -99.48               0.05198              
 -99.5                0.05768              
 -99.52               0.06358              
 -99.54               0.05888              
 -99.56               0.05325              
 -99.58               0.05393              
 -99.6                0.05314              
 -99.62               0.04865              
 -99.64               0.04249              
 -99.66               0.03733              
 -99.68               0.03084              
 -99.7                0.01879              
 -99.72               0.00847              
 -99.74               0.00316              
 -99.76              -0.00288              
 -99.78              -0.00815              
 -99.8               -0.01072              
 -99.82              -0.01571              
 -99.84              -0.02172              
 -99.86              -0.02315              
 -99.88              -0.01938              
 -99.9               -0.01301              
 -99.92              -0.00852              
 -99.94              -0.00747              
 -99.96              -0.00793              
 -99.98              -0.00434              
 -100.                0.00271              
 -100.02              0.00920              
 -100.04              0.01311              
 -100.06              0.01593              
 -100.08              0.02127              
 -100.1               0.02788              
 -100.12              0.03383              
 -100.14              0.03852              
 -100.16              0.03981              
 -100.18              0.03861              
 -100.2               0.04480              
 -100.22              0.05405              
 -100.24              0.05316              
 -100.26              0.04688              
 -100.28              0.04098              
 -100.3               0.03574              
 -100.32              0.02857              
 -100.34              0.01907              
 -100.36              0.01311              
 -100.38              0.00631              
 -100.4              -0.00728              
 -100.42             -0.01211              
 -100.44             -0.00037              
 -100.46              0.02086              
 -100.48              0.03944              
 -100.5               0.05059              
 -100.52              0.06432              
 -100.54              0.07922              
 -100.56              0.08887              
 -100.58              0.09480              
 -100.6               0.09685              
 -100.62              0.09268              
 -100.64              0.08391              
 -100.66              0.07186              
 -100.68              0.05572              
 -100.7               0.03650              
 -100.72              0.01573              
 -100.74             -0.00594              
 -100.76             -0.02631              
 -100.78             -0.04133              
 -100.8              -0.04528              
 -100.82             -0.04108              
 -100.84             -0.04063              
 -100.86             -0.03972              
 -100.88             -0.03110              
 -100.9              -0.01567              
 -100.92              0.00326              
 -100.94              0.02180              
 -100.96              0.03735              
 -100.98              0.04847              
 -101.                0.05517              
 -101.02              0.06065              
 -101.04              0.06678              
 -101.06              0.07143              
 -101.08              0.07312              
 -101.1               0.07262              
 -101.12              0.07490              
 -101.14              0.07783              
 -101.16              0.07504              
 -101.18              0.07302              
 -101.2               0.07361              
 -101.22              0.06844              
 -101.24              0.06320              
 -101.26              0.06579              
 -101.28              0.07312              
 -101.3               0.08274              
 -101.32              0.09286              
 -101.34              0.09804              
 -101.36              0.09714              
 -101.38              0.09466              
 -101.4               0.09086              
 -101.42              0.08492              
 -101.44              0.07734              
 -101.46              0.06744              
 -101.48              0.05513              
 -101.5               0.04501              
 -101.52              0.04012              
 -101.54              0.04000              
 -101.56              0.03924              
 -101.58              0.03582              
 -101.6               0.03456              
 -101.62              0.02889              
 -101.64              0.01330              
 -101.66              0.00149              
 -101.68             -0.00259              
 -101.7              -0.00529              
 -101.72             -0.00900              
 -101.74             -0.01209              
 -101.76             -0.01069              
 -101.78             -0.01390              
 -101.8              -0.02689              
 -101.82             -0.03496              
 -101.84             -0.04601              
 -101.86             -0.07445              
 -101.88             -0.09292              
 -101.9              -0.09282              
 -101.92             -0.09454              
 -101.94             -0.09803              
 -101.96             -0.09562              
 -101.98             -0.08243              
 -102.               -0.06800              
 -102.02             -0.06104              
 -102.04             -0.04316              
 -102.06             -0.01821              
 -102.08             -0.00946              
 -102.1              -0.00505              
 -102.12              0.00752              
 -102.14              0.02403              
 -102.16              0.03663              
 -102.18              0.04019              
 -102.2               0.03885              
 -102.22              0.03526              
 -102.24              0.02974              
 -102.26              0.02289              
 -102.28              0.01694              
 -102.3               0.01599              
 -102.32              0.02364              
 -102.34              0.03686              
 -102.36              0.04101              
 -102.38              0.04005              
 -102.4               0.04735              
 -102.42              0.06068              
 -102.44              0.06862              
 -102.46              0.05775              
 -102.48              0.03994              
 -102.5               0.02564              
 -102.52              0.00809              
 -102.54             -0.00904              
 -102.56             -0.01710              
 -102.58             -0.01337              
 -102.6               0.00099              
 -102.62              0.02173              
 -102.64              0.04191              
 -102.66              0.06226              
 -102.68              0.09279              
 -102.7               0.11895              
 -102.72              0.12744              
 -102.74              0.13579              
 -102.76              0.14415              
 -102.78              0.14032              
 -102.8               0.13041              
 -102.82              0.12161              
 -102.84              0.11585              
 -102.86              0.10878              
 -102.88              0.09906              
 -102.9               0.09534              
 -102.92              0.09689              
 -102.94              0.09890              
 -102.96              0.10565              
 -102.98              0.11502              
 -103.                0.11877              
 -103.02              0.12190              
 -103.04              0.12830              
 -103.06              0.13283              
 -103.08              0.13487              
 -103.1               0.13548              
 -103.12              0.13236              
 -103.14              0.12550              
 -103.16              0.11697              
 -103.18              0.10713              
 -103.2               0.09507              
 -103.22              0.07915              
 -103.24              0.05944              
 -103.26              0.04016              
 -103.28              0.03202              
 -103.3               0.03537              
 -103.32              0.04346              
 -103.34              0.05475              
 -103.36              0.07026              
 -103.38              0.09050              
 -103.4               0.10325              
 -103.42              0.10474              
 -103.44              0.11442              
 -103.46              0.13134              
 -103.48              0.14405              
 -103.5               0.15324              
 -103.52              0.16221              
 -103.54              0.17184              
 -103.56              0.16956              
 -103.58              0.15302              
 -103.6               0.14073              
 -103.62              0.1335               
 -103.64              0.12284              
 -103.66              0.10380              
 -103.68              0.08291              
 -103.7               0.07198              
 -103.72              0.06609              
 -103.74              0.06005              
 -103.76              0.05484              
 -103.78              0.05489              
 -103.8               0.06132              
 -103.82              0.06572              
 -103.84              0.06336              
 -103.86              0.05468              
 -103.88              0.04572              
 -103.9               0.04037              
 -103.92              0.03795              
 -103.94              0.03331              
 -103.96              0.02400              
 -103.98              0.01476              
 -104.                0.00574              
 -104.02             -0.00557              
 -104.04             -0.02042              
 -104.06             -0.04329              
 -104.08             -0.07745              
 -104.1              -0.10452              
 -104.12             -0.11488              
 -104.14             -0.12040              
 -104.16             -0.12031              
 -104.18             -0.11133              
 -104.2              -0.10156              
 -104.22             -0.09738              
 -104.24             -0.10020              
 -104.26             -0.10232              
 -104.28             -0.09859              
 -104.3              -0.08965              
 -104.32             -0.07401              
 -104.34             -0.05045              
 -104.36             -0.02047              
 -104.38              0.01372              
 -104.4               0.04825              
 -104.42              0.07461              
 -104.44              0.09064              
 -104.46              0.10128              
 -104.48              0.10770              
 -104.5               0.10797              
 -104.52              0.09798              
 -104.54              0.08009              
 -104.56              0.06104              
 -104.58              0.04898              
 -104.6               0.04906              
 -104.62              0.06075              
 -104.64              0.07094              
 -104.66              0.07299              
 -104.68              0.07368              
 -104.7               0.07254              
 -104.72              0.06688              
 -104.74              0.05804              
 -104.76              0.04930              
 -104.78              0.04334              
 -104.8               0.03686              
 -104.82              0.03086              
 -104.84              0.03176              
 -104.86              0.03637              
 -104.88              0.04412              
 -104.9               0.06520              
 -104.92              0.08868              
 -104.94              0.09680              
 -104.96              0.09573              
 -104.98              0.09237              
 -105.                0.08916              
 -105.02              0.08649              
 -105.04              0.08359              
 -105.06              0.07892              
 -105.08              0.07195              
 -105.1               0.06309              
 -105.12              0.05362              
 -105.14              0.04492              
 -105.16              0.03706              
 -105.18              0.02504              
 -105.2               0.00950              
 -105.22             -0.00097              
 -105.24             -0.00940              
 -105.26             -0.01914              
 -105.28             -0.02295              
 -105.3              -0.02156              
 -105.32             -0.02112              
 -105.34             -0.02224              
 -105.36             -0.02205              
 -105.38             -0.01660              
 -105.4              -0.01113              
 -105.42             -0.01109              
 -105.44             -0.01577              
 -105.46             -0.02221              
 -105.48             -0.02641              
 -105.5              -0.02430              
 -105.52             -0.01740              
 -105.54             -0.01135              
 -105.56             -0.00516              
 -105.58             -0.00171              
 -105.6              -0.01133              
 -105.62             -0.02932              
 -105.64             -0.04702              
 -105.66             -0.06554              
 -105.68             -0.07838              
 -105.7              -0.07442              
 -105.72             -0.05486              
 -105.74             -0.03009              
 -105.76             -0.01524              
 -105.78             -0.00461              
 -105.8               0.01263              
 -105.82              0.03831              
 -105.84              0.06482              
 -105.86              0.08334              
 -105.88              0.10045              
 -105.9               0.12581              
 -105.92              0.16483              
 -105.94              0.19983              
 -105.96              0.21965              
 -105.98              0.23753              
 -106.                0.25481              
 -106.02              0.26382              
 -106.04              0.25561              
 -106.06              0.23108              
 -106.08              0.19940              
 -106.1               0.16483              
 -106.12              0.12896              
 -106.14              0.09269              
 -106.16              0.06434              
 -106.18              0.04924              
 -106.2               0.03793              
 -106.22              0.03046              
 -106.24              0.03373              
 -106.26              0.04586              
 -106.28              0.06458              
 -106.3               0.08817              
 -106.32              0.10364              
 -106.34              0.10325              
 -106.36              0.09814              
 -106.38              0.09143              
 -106.4               0.08185              
 -106.42              0.07579              
 -106.44              0.07725              
 -106.46              0.08614              
 -106.48              0.10273              
 -106.5               0.1242               
 -106.52              0.14316              
 -106.54              0.16088              
 -106.56              0.17982              
 -106.58              0.19222              
 -106.6               0.19182              
 -106.62              0.17697              
 -106.64              0.15422              
 -106.66              0.13318              
 -106.68              0.12350              
 -106.7               0.12677              
 -106.72              0.14088              
 -106.74              0.16357              
 -106.76              0.18726              
 -106.78              0.20352              
 -106.8               0.21542              
 -106.82              0.22394              
 -106.84              0.22559              
 -106.86              0.22445              
 -106.88              0.22458              
 -106.9               0.22452              
 -106.92              0.22472              
 -106.94              0.22550              
 -106.96              0.22223              
 -106.98              0.21566              
 -107.                0.21076              
 -107.02              0.20183              
 -107.04              0.18896              
 -107.06              0.18553              
 -107.08              0.19317              
 -107.1               0.20929              
 -107.12              0.23740              
 -107.14              0.27133              
 -107.16              0.29940              
 -107.18              0.32440              
 -107.2               0.34518              
 -107.22              0.35301              
 -107.24              0.35958              
 -107.26              0.37308              
 -107.28              0.37672              
 -107.3               0.38160              
 -107.32              0.41084              
 -107.34              0.45241              
 -107.36              0.50124              
 -107.38              0.56597              
 -107.4               0.63773              
 -107.42              0.70145              
 -107.44              0.74668              
 -107.46              0.80062              
 -107.48              0.88855              
 -107.5               0.96755              
 -107.52              1.03408              
 -107.54              1.12206              
 -107.56              1.20878              
 -107.58              1.27557              
 -107.6               1.33508              
 -107.62              1.38876              
 -107.64              1.44155              
 -107.66              1.51983              
 -107.68              1.59317              
 -107.7               1.60931              
 -107.72              1.62096              
 -107.74              1.65115              
 -107.76              1.65766              
 -107.78              1.64004              
 -107.8               1.61315              
 -107.82              1.58266              
 -107.84              1.543                
 -107.86              1.48893              
 -107.88              1.43857              
 -107.9               1.40243              
 -107.92              1.37609              
 -107.94              1.34629              
 -107.96              1.30415              
 -107.98              1.2531               
 -108.                1.19798              
 -108.02              1.14518              
 -108.04              1.10449              
 -108.06              1.07382              
 -108.08              1.04401              
 -108.1               1.02485              
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##END=
