Villaescusa et al. Chem. Mater., 10, 3966-3973 (1998) Figure 4 ##freq 1 ##col_ ppm Spectrum Model Si2 Si1 ----- -95.01 -0.04023 0.00146 0.00052 0.00094 -95.02 -0.04020 0.00147 0.00052 0.00094 -95.03 -0.04064 0.00147 0.00052 0.00094 -95.04 -0.04104 0.00147 0.00052 0.00094 -95.05 -0.04014 0.00147 0.00052 0.00095 -95.06 -0.03754 0.00147 0.00052 0.00095 -95.07 -0.03510 0.00147 0.00052 0.00095 -95.08 -0.03447 0.00148 0.00052 0.00095 -95.09 -0.03493 0.00148 0.00052 0.00095 -95.1 -0.03527 0.00148 0.00052 0.00095 -95.11 -0.03518 0.00148 0.00052 0.00095 -95.12 -0.03484 0.00148 0.00052 0.00095 -95.13 -0.03471 0.00148 0.00052 0.00095 -95.14 -0.03550 0.00149 0.00052 0.00096 -95.15 -0.03720 0.00149 0.00053 0.00096 -95.16 -0.03890 0.00149 0.00053 0.00096 -95.17 -0.03994 0.00149 0.00053 0.00096 -95.18 -0.04043 0.00149 0.00053 0.00096 -95.19 -0.04058 0.00149 0.00053 0.00096 -95.2 -0.04048 0.00150 0.00053 0.00096 -95.21 -0.04021 0.00150 0.00053 0.00096 -95.22 -0.04021 0.00150 0.00053 0.00097 -95.23 -0.04107 0.00150 0.00053 0.00097 -95.24 -0.04278 0.00150 0.00053 0.00097 -95.25 -0.04482 0.00150 0.00053 0.00097 -95.26 -0.04578 0.00151 0.00053 0.00097 -95.27 -0.04307 0.00151 0.00053 0.00097 -95.28 -0.03650 0.00151 0.00053 0.00097 -95.29 -0.03146 0.00151 0.00053 0.00097 -95.3 -0.03178 0.00151 0.00053 0.00097 -95.31 -0.03207 0.00151 0.00053 0.00098 -95.32 -0.02598 0.00152 0.00053 0.00098 -95.33 -0.01657 0.00152 0.00054 0.00098 -95.34 -0.01071 0.00152 0.00054 0.00098 -95.35 -0.01027 0.00152 0.00054 0.00098 -95.36 -0.01320 0.00152 0.00054 0.00098 -95.37 -0.01526 0.00153 0.00054 0.00098 -95.38 -0.00953 0.00153 0.00054 0.00098 -95.39 0.00541 0.00153 0.00054 0.00099 -95.4 0.01887 0.00153 0.00054 0.00099 -95.41 0.02204 0.00153 0.00054 0.00099 -95.42 0.01927 0.00153 0.00054 0.00099 -95.43 0.01742 0.00154 0.00054 0.00099 -95.44 0.01894 0.00154 0.00054 0.00099 -95.45 0.02422 0.00154 0.00054 0.00099 -95.46 0.03067 0.00154 0.00054 0.00099 -95.47 0.03367 0.00154 0.00054 0.00100 -95.48 0.03297 0.00154 0.00054 0.00100 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0.00056 0.00103 -95.75 -0.01171 0.00159 0.00056 0.00103 -95.76 -0.01064 0.00160 0.00056 0.00103 -95.77 -0.01048 0.00160 0.00056 0.00103 -95.78 -0.01705 0.00160 0.00056 0.00103 -95.79 -0.02739 0.00160 0.00056 0.00104 -95.8 -0.03323 0.00160 0.00056 0.00104 -95.81 -0.03276 0.00161 0.00056 0.00104 -95.82 -0.03125 0.00161 0.00056 0.00104 -95.83 -0.03220 0.00161 0.00056 0.00104 -95.84 -0.03538 0.00161 0.00056 0.00104 -95.85 -0.03985 0.00161 0.00057 0.00104 -95.86 -0.04370 0.00162 0.00057 0.00104 -95.87 -0.04519 0.00162 0.00057 0.00105 -95.88 -0.04452 0.00162 0.00057 0.00105 -95.89 -0.04266 0.00162 0.00057 0.00105 -95.9 -0.04086 0.00162 0.00057 0.00105 -95.91 -0.04049 0.00163 0.00057 0.00105 -95.92 -0.04097 0.00163 0.00057 0.00105 -95.93 -0.03975 0.00163 0.00057 0.00105 -95.94 -0.03582 0.00163 0.00057 0.00106 -95.95 -0.03103 0.00163 0.00057 0.00106 -95.96 -0.02731 0.00163 0.00057 0.00106 -95.97 -0.02603 0.00164 0.00057 0.00106 -95.98 -0.02756 0.00164 0.00057 0.00106 -95.99 -0.02738 0.00164 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