29Si MAS NMR spectrum of Na-EMT ##freq 1 ##ppm spectr model Q4(4Al) Q4(3Al) Q4(2Al) ----- -70.15 3.1841 3.3928 0.3451 0.0178 0 -70.16 3.1373 3.3948 0.3451 0.0178 0 -70.17 3.1088 3.3958 0.3461 0.0178 0 -70.18 3.0976 3.3979 0.3461 0.0178 0 -70.19 3.1057 3.3999 0.3471 0.0178 0 -70.2 3.1332 3.4019 0.3471 0.0179 0 -70.21 3.1811 3.403 0.3481 0.0179 0 -70.22 3.234 3.405 0.3481 0.0179 0 -70.23 3.2727 3.407 0.3492 0.0179 0 -70.24 3.3164 3.408 0.3492 0.0179 0 -70.25 3.3633 3.4101 0.3502 0.018 0 -70.26 3.4121 3.4121 0.3502 0.018 0 -70.27 3.463 3.4142 0.3512 0.018 0 -70.28 3.5149 3.4152 0.3512 0.018 0 -70.29 3.5668 3.4172 0.3522 0.018 0 -70.3 3.6177 3.4192 0.3522 0.0181 0 -70.31 3.6676 3.4213 0.3532 0.0181 0 -70.32 3.7144 3.4223 0.3532 0.0181 0 -70.33 3.7582 3.4243 0.3542 0.0181 0 -70.34 3.7979 3.4264 0.3542 0.0181 0 -70.35 3.8335 3.4284 0.3553 0.0182 0 -70.36 3.8631 3.4294 0.3553 0.0182 0 -70.37 3.9038 3.4315 0.3563 0.0182 0 -70.38 3.9241 3.4335 0.3563 0.0182 0 -70.39 3.9282 3.4355 0.3573 0.0183 0 -70.4 3.9201 3.4366 0.3573 0.0183 0 -70.41 3.9038 3.4386 0.3583 0.0183 0 -70.42 3.8844 3.4406 0.3583 0.0183 0 -70.43 3.8671 3.4427 0.3593 0.0183 0 -70.44 3.8549 3.4437 0.3593 0.0184 0 -70.45 3.8478 3.4457 0.3603 0.0184 0 -70.46 3.8458 3.4477 0.3603 0.0184 0 -70.47 3.8478 3.4498 0.3614 0.0184 0 -70.48 3.8519 3.4508 0.3614 0.0184 0 -70.49 3.857 3.4528 0.3624 0.0185 0 -70.5 3.862 3.4549 0.3624 0.0185 0 -70.51 3.8651 3.4569 0.3634 0.0185 0 -70.52 3.8671 3.4579 0.3634 0.0185 0 -70.53 3.8682 3.46 0.3644 0.0185 0 -70.54 3.8682 3.462 0.3644 0.0186 0 -70.55 3.8671 3.464 0.3654 0.0186 0 -70.56 3.8661 3.4651 0.3654 0.0186 0 -70.57 3.8641 3.4671 0.3665 0.0186 0 -70.58 3.8631 3.4691 0.3665 0.0187 0 -70.59 3.8631 3.4712 0.3675 0.0187 0 -70.6 3.862 3.4732 0.3675 0.0187 0 -70.61 3.862 3.4742 0.3685 0.0187 0 -70.62 3.8631 3.4763 0.3685 0.0187 0 -70.63 3.8631 3.4783 0.3695 0.0188 0 -70.64 3.8631 3.4803 0.3695 0.0188 0 -70.65 3.8641 3.4813 0.3705 0.0188 0 -70.66 3.8641 3.4834 0.3705 0.0188 0 -70.67 3.8641 3.4854 0.3715 0.0188 0 -70.68 3.8641 3.4874 0.3715 0.0189 0 -70.69 3.8641 3.4895 0.3726 0.0189 0 -70.7 3.8641 3.4905 0.3736 0.0189 0 -70.71 3.8641 3.4925 0.3736 0.0189 0 -70.72 3.8641 3.4946 0.3746 0.019 0 -70.73 3.8641 3.4966 0.3746 0.019 0 -70.74 3.8641 3.4976 0.3756 0.019 0 -70.75 3.8641 3.4997 0.3756 0.019 0 -70.76 3.8641 3.5017 0.3766 0.019 0 -70.77 3.8641 3.5037 0.3766 0.0191 0 -70.78 3.8641 3.5058 0.3777 0.0191 0 -70.79 3.8641 3.5068 0.3777 0.0191 0 -70.8 3.8631 3.5088 0.3787 0.0191 0 -70.81 3.862 3.5109 0.3787 0.0192 0 -70.82 3.862 3.5129 0.3797 0.0192 0 -70.83 3.861 3.5149 0.3807 0.0192 0 -70.84 3.861 3.516 0.3807 0.0192 0 -70.85 3.862 3.518 0.3817 0.0192 0 -70.86 3.8631 3.52 0.3817 0.0193 0 -70.87 3.8651 3.5221 0.3827 0.0193 0 -70.88 3.8671 3.5241 0.3827 0.0193 0 -70.89 3.8702 3.5251 0.3838 0.0193 0 -70.9 3.8722 3.5271 0.3838 0.0194 0 -70.91 3.8732 3.5292 0.3848 0.0194 0 -70.92 3.8712 3.5312 0.3858 0.0194 0 -70.93 3.8682 3.5333 0.3858 0.0194 0 -70.94 3.861 3.5343 0.3868 0.0195 0 -70.95 3.8509 3.5363 0.3868 0.0195 0 -70.96 3.8407 3.5383 0.3878 0.0195 0 -70.97 3.8325 3.5404 0.3878 0.0195 0 -70.98 3.8295 3.5424 0.3889 0.0195 0 -70.99 3.8325 3.5445 0.3889 0.0196 0 -71 3.8447 3.5455 0.3899 0.0196 0 -71.01 3.8682 3.5475 0.3909 0.0196 0 -71.02 3.9048 3.5495 0.3909 0.0196 0 -71.03 3.9496 3.5516 0.3919 0.0197 0 -71.04 4.0005 3.5536 0.3919 0.0197 0 -71.05 4.0534 3.5546 0.3929 0.0197 0 -71.06 4.1033 3.5567 0.3929 0.0197 0 -71.07 4.1491 3.5587 0.3939 0.0198 0 -71.08 4.1847 3.5607 0.395 0.0198 0 -71.09 4.2071 3.5628 0.395 0.0198 0 -71.1 4.2193 3.5648 0.396 0.0198 0 -71.11 4.2224 3.5658 0.396 0.0199 0 -71.12 4.2183 3.5679 0.397 0.0199 0 -71.13 4.2102 3.5699 0.398 0.0199 0 -71.14 4.199 3.5719 0.398 0.0199 0 -71.15 4.1878 3.574 0.399 0.0199 0 -71.16 4.1796 3.576 0.399 0.02 0 -71.17 4.1725 3.578 0.4 0.02 0 -71.18 4.1695 3.5791 0.4 0.02 0 -71.19 4.1684 3.5811 0.4011 0.02 0 -71.2 4.1705 3.5831 0.4021 0.0201 0 -71.21 4.1746 3.5852 0.4021 0.0201 0 -71.22 4.1817 3.5872 0.4031 0.0201 0 -71.23 4.1908 3.5892 0.4031 0.0201 0 -71.24 4.202 3.5903 0.4041 0.0202 0 -71.25 4.2122 3.5923 0.4051 0.0202 0 -71.26 4.2204 3.5943 0.4051 0.0202 0 -71.27 4.2224 3.5964 0.4062 0.0202 0 -71.28 4.2173 3.5984 0.4062 0.0203 0 -71.29 4.202 3.6004 0.4072 0.0203 0 -71.3 4.1746 3.6025 0.4082 0.0203 0 -71.31 4.1359 3.6035 0.4082 0.0203 0 -71.32 4.089 3.6055 0.4092 0.0204 0 -71.33 4.0371 3.6076 0.4102 0.0204 0 -71.34 3.9852 3.6096 0.4102 0.0204 0 -71.35 3.9353 3.6116 0.4112 0.0204 0 -71.36 3.8926 3.6137 0.4112 0.0205 0 -71.37 3.86 3.6157 0.4123 0.0205 0 -71.38 3.8397 3.6177 0.4133 0.0205 0 -71.39 3.8305 3.6188 0.4133 0.0205 0 -71.4 3.8295 3.6208 0.4143 0.0206 0 -71.41 3.8356 3.6228 0.4143 0.0206 0 -71.42 3.8437 3.6249 0.4153 0.0206 0 -71.43 3.8539 3.6269 0.4163 0.0206 0 -71.44 3.8631 3.6289 0.4163 0.0207 0 -71.45 3.8692 3.631 0.4174 0.0207 0 -71.46 3.8712 3.633 0.4184 0.0207 0 -71.47 3.8722 3.634 0.4184 0.0207 0 -71.48 3.8702 3.6361 0.4194 0.0208 0 -71.49 3.8682 3.6381 0.4204 0.0208 0 -71.5 3.8661 3.6401 0.4204 0.0208 0 -71.51 3.8641 3.6422 0.4214 0.0208 0 -71.52 3.8631 3.6442 0.4214 0.0209 0 -71.53 3.8641 3.6462 0.4224 0.0209 0 -71.54 3.8651 3.6483 0.4235 0.0209 0 -71.55 3.8661 3.6503 0.4235 0.0209 0 -71.56 3.8671 3.6513 0.4245 0.021 0 -71.57 3.8671 3.6534 0.4255 0.021 0 -71.58 3.8651 3.6554 0.4255 0.021 0 -71.59 3.861 3.6574 0.4265 0.021 0 -71.6 3.857 3.6595 0.4275 0.0211 0 -71.61 3.8509 3.6615 0.4275 0.0211 0 -71.62 3.8468 3.6636 0.4286 0.0211 0 -71.63 3.8458 3.6656 0.4296 0.0211 0 -71.64 3.8478 3.6676 0.4296 0.0212 0 -71.65 3.8549 3.6697 0.4306 0.0212 0 -71.66 3.8692 3.6717 0.4316 0.0212 0 -71.67 3.8885 3.6727 0.4316 0.0212 0 -71.68 3.9089 3.6747 0.4326 0.0213 0 -71.69 3.9252 3.6768 0.4336 0.0213 0 -71.7 3.9333 3.6788 0.4336 0.0213 0 -71.71 3.9272 3.6809 0.4347 0.0213 0 -71.72 3.9038 3.6829 0.4357 0.0214 0 -71.73 3.86 3.6849 0.4357 0.0214 0 -71.74 3.8274 3.687 0.4367 0.0214 0 -71.75 3.7898 3.689 0.4377 0.0215 0 -71.76 3.747 3.691 0.4377 0.0215 0 -71.77 3.7002 3.6931 0.4387 0.0215 0 -71.78 3.6503 3.6951 0.4397 0.0215 0 -71.79 3.5984 3.6971 0.4397 0.0216 0 -71.8 3.5465 3.6992 0.4408 0.0216 0 -71.81 3.4936 3.7002 0.4418 0.0216 0 -71.82 3.4416 3.7022 0.4418 0.0216 0 -71.83 3.3918 3.7043 0.4428 0.0217 0 -71.84 3.3439 3.7063 0.4438 0.0217 0 -71.85 3.3001 3.7083 0.4438 0.0217 0 -71.86 3.2615 3.7104 0.4448 0.0217 0 -71.87 3.2279 3.7124 0.4459 0.0218 0 -71.88 3.1861 3.7144 0.4459 0.0218 0 -71.89 3.1587 3.7165 0.4469 0.0218 0 -71.9 3.1495 3.7185 0.4479 0.0219 0 -71.91 3.1556 3.7206 0.4489 0.0219 0 -71.92 3.1709 3.7226 0.4489 0.0219 0 -71.93 3.1912 3.7246 0.4499 0.0219 0 -71.94 3.2116 3.7267 0.4509 0.022 0 -71.95 3.2269 3.7287 0.4509 0.022 0 -71.96 3.236 3.7307 0.452 0.022 0 -71.97 3.2391 3.7328 0.453 0.022 0 -71.98 3.2391 3.7348 0.454 0.0221 0 -71.99 3.235 3.7368 0.454 0.0221 0 -72 3.2299 3.7389 0.455 0.0221 0 -72.01 3.2238 3.7409 0.456 0.0222 0 -72.02 3.2177 3.743 0.456 0.0222 0 -72.03 3.2136 3.745 0.4571 0.0222 0 -72.04 3.2106 3.747 0.4581 0.0222 0 -72.05 3.2085 3.7491 0.4591 0.0223 0 -72.06 3.2085 3.7511 0.4591 0.0223 0 -72.07 3.2106 3.7531 0.4601 0.0223 0 -72.08 3.2146 3.7552 0.4611 0.0224 0 -72.09 3.2207 3.7572 0.4611 0.0224 0 -72.1 3.2279 3.7582 0.4621 0.0224 0 -72.11 3.236 3.7603 0.4632 0.0224 0 -72.12 3.2421 3.7623 0.4642 0.0225 0 -72.13 3.2462 3.7643 0.4642 0.0225 0 -72.14 3.2452 3.7664 0.4652 0.0225 0 -72.15 3.237 3.7684 0.4662 0.0226 0 -72.16 3.2218 3.7704 0.4672 0.0226 0 -72.17 3.1973 3.7725 0.4672 0.0226 0 -72.18 3.1637 3.7745 0.4683 0.0226 0 -72.19 3.123 3.7765 0.4693 0.0227 0 -72.2 3.0762 3.7786 0.4703 0.0227 0 -72.21 3.0253 3.7816 0.4703 0.0227 0 -72.22 2.9703 3.7837 0.4713 0.0228 0 -72.23 2.9144 3.7857 0.4723 0.0228 0 -72.24 2.8584 3.7877 0.4733 0.0228 0 -72.25 2.8024 3.7898 0.4733 0.0228 0 -72.26 2.7494 3.7918 0.4744 0.0229 0 -72.27 2.6996 3.7938 0.4754 0.0229 0 -72.28 2.6558 3.7959 0.4764 0.0229 0 -72.29 2.6171 3.7979 0.4764 0.023 0 -72.3 2.5876 3.8 0.4774 0.023 0 -72.31 2.5662 3.802 0.4784 0.023 0 -72.32 2.555 3.804 0.4794 0.0231 0 -72.33 2.5509 3.8061 0.4805 0.0231 0 -72.34 2.552 3.8081 0.4805 0.0231 0 -72.35 2.5571 3.8101 0.4815 0.0231 0 -72.36 2.5642 3.8122 0.4825 0.0232 0 -72.37 2.5713 3.8142 0.4835 0.0232 0 -72.38 2.5774 3.8162 0.4835 0.0232 0 -72.39 2.5805 3.8183 0.4845 0.0233 0 -72.4 2.5825 3.8203 0.4856 0.0233 0 -72.41 2.5825 3.8223 0.4866 0.0233 0 -72.42 2.5815 3.8244 0.4876 0.0233 0 -72.43 2.5794 3.8264 0.4876 0.0234 0 -72.44 2.5774 3.8285 0.4886 0.0234 0 -72.45 2.5754 3.8305 0.4896 0.0234 0 -72.46 2.5744 3.8325 0.4906 0.0235 0 -72.47 2.5744 3.8346 0.4917 0.0235 0 -72.48 2.5744 3.8376 0.4917 0.0235 0 -72.49 2.5744 3.8397 0.4927 0.0236 0 -72.5 2.5744 3.8417 0.4937 0.0236 0 -72.51 2.5754 3.8437 0.4947 0.0236 0 -72.52 2.5754 3.8458 0.4957 0.0237 0 -72.53 2.5764 3.8478 0.4968 0.0237 0 -72.54 2.5764 3.8498 0.4968 0.0237 0 -72.55 2.5764 3.8519 0.4978 0.0237 0 -72.56 2.5764 3.8539 0.4988 0.0238 0 -72.57 2.5764 3.8559 0.4998 0.0238 0 -72.58 2.5764 3.858 0.5008 0.0238 0 -72.59 2.5754 3.86 0.5008 0.0239 0 -72.6 2.5754 3.862 0.5018 0.0239 0 -72.61 2.5754 3.8651 0.5029 0.0239 0 -72.62 2.5754 3.8671 0.5039 0.024 0 -72.63 2.5754 3.8692 0.5049 0.024 0 -72.64 2.5754 3.8712 0.5059 0.024 0 -72.65 2.5754 3.8732 0.5059 0.0241 0 -72.66 2.5754 3.8753 0.5069 0.0241 0 -72.67 2.5754 3.8773 0.508 0.0241 0 -72.68 2.5754 3.8794 0.509 0.0242 0 -72.69 2.5754 3.8814 0.51 0.0242 0 -72.7 2.5754 3.8834 0.511 0.0242 0 -72.71 2.5754 3.8865 0.512 0.0242 0 -72.72 2.5754 3.8885 0.512 0.0243 0 -72.73 2.5754 3.8906 0.513 0.0243 0 -72.74 2.5754 3.8926 0.5141 0.0243 0 -72.75 2.5754 3.8946 0.5151 0.0244 0 -72.76 2.5754 3.8967 0.5161 0.0244 0 -72.77 2.5754 3.8987 0.5171 0.0244 0 -72.78 2.5754 3.9007 0.5181 0.0245 0 -72.79 2.5754 3.9038 0.5181 0.0245 0 -72.8 2.5754 3.9058 0.5191 0.0245 0 -72.81 2.5754 3.9079 0.5202 0.0246 0 -72.82 2.5754 3.9099 0.5212 0.0246 0 -72.83 2.5754 3.9119 0.5222 0.0246 0 -72.84 2.5754 3.914 0.5232 0.0247 0 -72.85 2.5754 3.916 0.5242 0.0247 0 -72.86 2.5754 3.9191 0.5253 0.0247 0 -72.87 2.5754 3.9211 0.5253 0.0248 0 -72.88 2.5754 3.9231 0.5263 0.0248 0 -72.89 2.5754 3.9252 0.5273 0.0248 0 -72.9 2.5754 3.9272 0.5283 0.0249 0 -72.91 2.5754 3.9292 0.5293 0.0249 0 -72.92 2.5754 3.9313 0.5303 0.0249 0 -72.93 2.5754 3.9343 0.5314 0.025 0 -72.94 2.5754 3.9364 0.5324 0.025 0 -72.95 2.5754 3.9384 0.5334 0.025 0 -72.96 2.5754 3.9404 0.5344 0.0251 0 -72.97 2.5754 3.9425 0.5344 0.0251 0 -72.98 2.5754 3.9445 0.5354 0.0251 0 -72.99 2.5754 3.9476 0.5365 0.0252 0 -73 2.5754 3.9496 0.5375 0.0252 0 -73.01 2.5754 3.9516 0.5385 0.0252 0 -73.02 2.5754 3.9537 0.5395 0.0253 0 -73.03 2.5754 3.9557 0.5405 0.0253 0 -73.04 2.5754 3.9588 0.5415 0.0253 0 -73.05 2.5754 3.9608 0.5426 0.0254 0 -73.06 2.5754 3.9628 0.5436 0.0254 0 -73.07 2.5754 3.9649 0.5446 0.0254 0 -73.08 2.5754 3.9669 0.5456 0.0255 0 -73.09 2.5754 3.97 0.5466 0.0255 0 -73.1 2.5754 3.972 0.5476 0.0255 0 -73.11 2.5754 3.974 0.5476 0.0256 0 -73.12 2.5754 3.9761 0.5487 0.0256 0 -73.13 2.5754 3.9781 0.5497 0.0256 0 -73.14 2.5754 3.9811 0.5507 0.0257 0 -73.15 2.5754 3.9832 0.5517 0.0257 0 -73.16 2.5754 3.9852 0.5527 0.0257 0 -73.17 2.5754 3.9873 0.5538 0.0258 0 -73.18 2.5754 3.9903 0.5548 0.0258 0 -73.19 2.5754 3.9923 0.5558 0.0259 0 -73.2 2.5754 3.9944 0.5568 0.0259 0 -73.21 2.5754 3.9964 0.5578 0.0259 0 -73.22 2.5754 3.9985 0.5588 0.026 0 -73.23 2.5754 4.0015 0.5599 0.026 0 -73.24 2.5754 4.0035 0.5609 0.026 0 -73.25 2.5754 4.0056 0.5619 0.0261 0 -73.26 2.5754 4.0076 0.5629 0.0261 0 -73.27 2.5754 4.0107 0.5639 0.0261 0 -73.28 2.5754 4.0127 0.565 0.0262 0 -73.29 2.5754 4.0147 0.566 0.0262 0 -73.3 2.5754 4.0168 0.567 0.0262 0 -73.31 2.5754 4.0198 0.568 0.0263 0 -73.32 2.5754 4.0219 0.569 0.0263 0 -73.33 2.5754 4.0239 0.57 0.0264 0 -73.34 2.5754 4.027 0.5711 0.0264 0 -73.35 2.5754 4.029 0.5721 0.0264 0 -73.36 2.5754 4.031 0.5731 0.0265 0 -73.37 2.5754 4.0331 0.5741 0.0265 0 -73.38 2.5754 4.0361 0.5751 0.0265 0 -73.39 2.5754 4.0382 0.5762 0.0266 0 -73.4 2.5754 4.0402 0.5772 0.0266 0 -73.41 2.5754 4.0422 0.5782 0.0266 0 -73.42 2.5754 4.0453 0.5792 0.0267 0 -73.43 2.5754 4.0473 0.5802 0.0267 0 -73.44 2.5754 4.0493 0.5812 0.0268 0 -73.45 2.5754 4.0524 0.5823 0.0268 0 -73.46 2.5754 4.0544 0.5833 0.0268 0 -73.47 2.5754 4.0565 0.5843 0.0269 0 -73.48 2.5754 4.0595 0.5853 0.0269 0 -73.49 2.5754 4.0616 0.5863 0.0269 0 -73.5 2.5754 4.0636 0.5873 0.027 0 -73.51 2.5754 4.0667 0.5884 0.027 0 -73.52 2.5754 4.0687 0.5894 0.0271 0 -73.53 2.5754 4.0707 0.5914 0.0271 0 -73.54 2.5764 4.0738 0.5924 0.0271 0 -73.55 2.5764 4.0758 0.5935 0.0272 0 -73.56 2.5764 4.0779 0.5945 0.0272 0 -73.57 2.5774 4.0809 0.5955 0.0272 0 -73.58 2.5774 4.0829 0.5965 0.0273 0 -73.59 2.5764 4.085 0.5975 0.0273 0 -73.6 2.5764 4.088 0.5985 0.0274 0 -73.61 2.5744 4.0901 0.5996 0.0274 0 -73.62 2.5733 4.0921 0.6006 0.0274 0 -73.63 2.5723 4.0952 0.6016 0.0275 0 -73.64 2.5713 4.0972 0.6026 0.0275 0 -73.65 2.5713 4.0992 0.6036 0.0275 0 -73.66 2.5723 4.1023 0.6057 0.0276 0 -73.67 2.5744 4.1043 0.6067 0.0276 0 -73.68 2.5784 4.1064 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