##TITLE=              31P MAS NMR spectrum of calcined EMM-3
##JCAMP-DX=           5.01
##DATA TYPE=          NMR SPECTRUM
##DATA CLASS=         XYDATA
##ORIGIN=             Afeworki et al. Chem. Mater., 18, 1697-1704 (2006) Figure 2a
##OWNER=              Digitized and processed by Brouwer Lab, Redeemer University
##LONG DATE=          2020/07/21 15:06:23
##SOURCE REFERENCE=   EZT-31P-Afeworki-2006-calcined
##DATA PROCESSING=    Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook

$$Sample information 
##NAMES=              EZT
##NAMES=              EMM-3
##SAMPLE DESCRIPTION= EMM-3, calcined

$$Bibliographic information 
##$AUTHORS=           Afeworki, M., Dorset, D.L., Kennedy, G.J., Strohmaier, K.G.
##$TITLE=             Synthesis and characterization of a new microporous material. 1. Structure of aluminophosphate EMM-3
##$JOURNAL=           Chemistry of Materials
##$VOLUME=            18
##$PAGES=             1697-1704
##$YEAR=              2006
##$DOI=               10.1021/cm052174r
##$FIGURE=            Figure 2a

$$Peak information    (Positions in ppm, Relative peak areas, Peak widths in ppm, Lorentzian/Gaussian shape parameter)
##$NUM PEAKS=         5
##$PEAK LABELS=        P7/P8/P9   P7/P8/P9   P7/P8/P9   P6         P10       
##$PEAK TSITES=        T3/T4/T2   T3/T4/T2   T3/T4/T2   T1         T5        
##$PEAK POSITIONS=    -30.5261   -30.0759   -29.491    -26.3218   -21.5691   
##$PEAK AREAS=         1.         1.         1.         2.         1.        
##$PEAK WIDTHS=        1.19556    1.19556    1.19556    1.67464    1.40799   
##$PEAK SHAPES=        0.54526    0.54526    0.54526    0.54526    0.54526   
##$NUMBERING REF=     Afeworki et al. Chem. Mater., 18, 1697-1704 (2006)
##$ASSIGN REF=        Afeworki et al. Chem. Mater., 18, 1697-1704 (2006) Figure 6
##$ASSIGN METHOD=     2D 27Al/31P correlation NMR, relative intensities
##$COMMENT=           Tentative partial peak assignments are based on a 2D 27Al/31P correlaton spectrum and relative peak areas

$$Spectrum acquisition information 
##.OBSERVE NUCLEUS=   ^31P
##.OBSERVE FREQUENCY= 202.1
##.PULSE SEQUENCE=    single pulse
##.MAS FREQUENCY=     10000-16000

$$Spectrum data information 
##XUNITS=             PPM
##YUNITS=             ARBITRARY UNITS
##FIRSTX=              20.13                
##LASTX=              -49.87                
##XFACTOR=            1
##YFACTOR=            1
##NPOINTS=            1001
##FIRSTY=              0.02316              

$$Spectrum data
##XYDATA=             (X++(Y..Y))
  20.13               0.02316              
  20.06               0.02434              
  19.99               0.02437              
  19.92               0.02469              
  19.85               0.02616              
  19.78               0.02480              
  19.71               0.02283              
  19.64               0.02538              
  19.57               0.03077              
  19.5                0.03433              
  19.43               0.03191              
  19.36               0.02778              
  19.29               0.02481              
  19.22               0.02202              
  19.15               0.02141              
  19.08               0.02384              
  19.01               0.02681              
  18.94               0.02764              
  18.87               0.02540              
  18.8                0.02248              
  18.73               0.02118              
  18.66               0.02158              
  18.59               0.01924              
  18.52               0.01432              
  18.45               0.00942              
  18.38               0.00244              
  18.31              -0.00337              
  18.24              -0.00141              
  18.17               0.00340              
  18.1                0.00625              
  18.03               0.00669              
  17.96               0.00636              
  17.89               0.00641              
  17.82               0.00636              
  17.75               0.00651              
  17.68               0.00668              
  17.61               0.00505              
  17.54               0.00292              
  17.47               0.00136              
  17.4               -0.00387              
  17.33              -0.00838              
  17.26              -0.00518              
  17.19              -0.00337              
  17.12              -0.00805              
  17.05              -0.01618              
  16.98              -0.02101              
  16.91              -0.02017              
  16.84              -0.01712              
  16.77              -0.01073              
  16.7               -0.00182              
  16.63               0.00343              
  16.56               0.00496              
  16.49               0.00501              
  16.42               0.00400              
  16.35               0.00308              
  16.28               0.00313              
  16.21               0.00292              
  16.14               0.00318              
  16.07               0.00536              
  16.                 0.00692              
  15.93               0.00648              
  15.86               0.00507              
  15.79               0.00514              
  15.72               0.00760              
  15.65               0.01088              
  15.58               0.01378              
  15.51               0.01586              
  15.44               0.01741              
  15.37               0.01787              
  15.3                0.01681              
  15.23               0.01509              
  15.16               0.01263              
  15.09               0.00868              
  15.02               0.00283              
  14.95              -0.00359              
  14.88              -0.00837              
  14.81              -0.01098              
  14.74              -0.01165              
  14.67              -0.01095              
  14.6               -0.00922              
  14.53              -0.00703              
  14.46              -0.00540              
  14.39              -0.00519              
  14.32              -0.00541              
  14.25              -0.00255              
  14.18               0.00254              
  14.11               0.00625              
  14.04               0.00477              
  13.97               0.00124              
  13.9                0.00038              
  13.83              -0.00174              
  13.76              -0.00511              
  13.69              -0.00591              
  13.62              -0.00367              
  13.55               0.00104              
  13.48               0.00701              
  13.41               0.01043              
  13.34               0.00996              
  13.27               0.00804              
  13.2                0.00275              
  13.13              -0.00430              
  13.06              -0.00331              
  12.99               0.00246              
  12.92               0.00649              
  12.85               0.01162              
  12.78               0.01661              
  12.71               0.01810              
  12.64               0.01730              
  12.57               0.01462              
  12.5                0.00955              
  12.43               0.00391              
  12.36              -0.00131              
  12.29              -0.00631              
  12.22              -0.00878              
  12.15              -0.00732              
  12.08              -0.00325              
  12.01               0.00075              
  11.94               0.00282              
  11.87               0.00353              
  11.8                0.00291              
  11.73               0.00086              
  11.66              -0.00195              
  11.59              -0.00343              
  11.52              -0.00165              
  11.45               0.00175              
  11.38               0.00476              
  11.31               0.00606              
  11.24               0.00674              
  11.17               0.00790              
  11.1                0.00985              
  11.03               0.01211              
  10.96               0.01207              
  10.89               0.00571              
  10.82              -0.00160              
  10.75              -0.00373              
  10.68              -0.00126              
  10.61               0.00415              
  10.54               0.00995              
  10.47               0.01204              
  10.4                0.01130              
  10.33               0.01122              
  10.26               0.01141              
  10.19               0.01135              
  10.12               0.01123              
  10.05               0.01160              
  9.98                0.01280              
  9.91                0.01444              
  9.84                0.01413              
  9.77                0.01066              
  9.7                 0.00570              
  9.63                0.00008              
  9.56               -0.00451              
  9.49               -0.00439              
  9.42               -0.00133              
  9.35                0.00159              
  9.28                0.00618              
  9.21                0.00977              
  9.14                0.00809              
  9.07                0.00490              
  9.                  0.00316              
  8.93                0.00344              
  8.86                0.00633              
  8.79                0.01081              
  8.72                0.01405              
  8.65                0.01433              
  8.58                0.01196              
  8.51                0.00925              
  8.44                0.00524              
  8.37               -0.00036              
  8.3                -0.00354              
  8.23               -0.00321              
  8.16               -0.00095              
  8.09                0.00041              
  8.02               -0.00021              
  7.95               -0.00225              
  7.88               -0.00446              
  7.81               -0.00511              
  7.74               -0.00306              
  7.67               -0.00143              
  7.6                -0.00293              
  7.53               -0.00746              
  7.46               -0.01039              
  7.39               -0.00898              
  7.32               -0.00630              
  7.25               -0.00501              
  7.18               -0.00529              
  7.11               -0.00345              
  7.04                0.00035              
  6.97                0.00436              
  6.9                 0.00979              
  6.83                0.01474              
  6.76                0.01609              
  6.69                0.01673              
  6.62                0.01787              
  6.55                0.01804              
  6.48                0.01790              
  6.41                0.01793              
  6.34                0.01775              
  6.27                0.01816              
  6.2                 0.01740              
  6.13                0.00980              
  6.06               -0.00039              
  5.99               -0.00690              
  5.92               -0.01030              
  5.85               -0.00963              
  5.78               -0.00490              
  5.71               -0.00322              
  5.64               -0.00511              
  5.57               -0.00519              
  5.5                -0.00050              
  5.43                0.00751              
  5.36                0.01363              
  5.29                0.01382              
  5.22                0.00890              
  5.15                0.00484              
  5.08                0.00259              
  5.01                0.00057              
  4.94               -0.00279              
  4.87               -0.00530              
  4.8                -0.00588              
  4.73               -0.00985              
  4.66               -0.01331              
  4.59               -0.01012              
  4.52               -0.00716              
  4.45               -0.00503              
  4.38                0.00055              
  4.31                0.00403              
  4.24                0.00188              
  4.17               -0.00411              
  4.1                -0.01054              
  4.03               -0.01344              
  3.96               -0.00976              
  3.89               -0.00344              
  3.82                0.00081              
  3.75                0.00231              
  3.68                0.00107              
  3.61               -0.00068              
  3.54                0.00320              
  3.47                0.01024              
  3.4                 0.01390              
  3.33                0.01510              
  3.26                0.01463              
  3.19                0.01249              
  3.12                0.01081              
  3.05                0.01119              
  2.98                0.01345              
  2.91                0.01479              
  2.84                0.01346              
  2.77                0.01052              
  2.7                 0.00722              
  2.63                0.00498              
  2.56                0.00525              
  2.49                0.00659              
  2.42                0.00674              
  2.35                0.00544              
  2.28                0.00290              
  2.21               -0.00034              
  2.14               -0.00318              
  2.07               -0.00505              
  2.                 -0.00570              
  1.93               -0.00391              
  1.86               -0.00046              
  1.79                0.00182              
  1.72                0.00401              
  1.65                0.00624              
  1.58                0.00590              
  1.51                0.00450              
  1.44                0.00360              
  1.37                0.00127              
  1.3                -0.00240              
  1.23               -0.00515              
  1.16               -0.00313              
  1.09                0.00178              
  1.02                0.00509              
  0.95                0.00790              
  0.88                0.00815              
  0.81                0.00165              
  0.74               -0.00688              
  0.67               -0.01155              
  0.6                -0.00938              
  0.53               -0.00591              
  0.46               -0.00620              
  0.39               -0.00965              
  0.32               -0.01444              
  0.25               -0.01795              
  0.18               -0.01696              
  0.11               -0.01256              
  0.04               -0.00803              
 -0.03               -0.00556              
 -0.1                -0.00507              
 -0.17               -0.00509              
 -0.24               -0.00498              
 -0.31               -0.00505              
 -0.38               -0.00564              
 -0.45               -0.00380              
 -0.52                0.00086              
 -0.59                0.00516              
 -0.66                0.00963              
 -0.73                0.01404              
 -0.8                 0.01490              
 -0.87                0.01212              
 -0.94                0.00691              
 -1.01               -0.00023              
 -1.08               -0.00545              
 -1.15               -0.00490              
 -1.22               -0.00071              
 -1.29                0.00324              
 -1.36                0.00377              
 -1.43                0.00228              
 -1.5                -0.00000              
 -1.57               -0.00304              
 -1.64               -0.00647              
 -1.71               -0.00962              
 -1.78               -0.01181              
 -1.85               -0.01408              
 -1.92               -0.01537              
 -1.99               -0.01112              
 -2.06               -0.00598              
 -2.13               -0.00350              
 -2.2                 0.00430              
 -2.27                0.01386              
 -2.34                0.01678              
 -2.41                0.01458              
 -2.48                0.01128              
 -2.55                0.01009              
 -2.62                0.00901              
 -2.69                0.00661              
 -2.76                0.00377              
 -2.83                0.00357              
 -2.9                 0.00609              
 -2.97                0.00707              
 -3.04                0.00590              
 -3.11                0.00369              
 -3.18                0.00163              
 -3.25               -0.00070              
 -3.32               -0.00315              
 -3.39               -0.00264              
 -3.46                0.00017              
 -3.53                0.00253              
 -3.6                 0.00344              
 -3.67                0.00312              
 -3.74                0.00273              
 -3.81                0.00407              
 -3.88                0.00632              
 -3.95                0.00625              
 -4.02                0.00343              
 -4.09                0.00012              
 -4.16                0.00046              
 -4.23                0.00460              
 -4.3                 0.00920              
 -4.37                0.00863              
 -4.44                0.00369              
 -4.51               -0.00182              
 -4.58               -0.00552              
 -4.65               -0.00673              
 -4.72               -0.00648              
 -4.79               -0.00773              
 -4.86               -0.01001              
 -4.93               -0.01042              
 -5.                 -0.00948              
 -5.07               -0.00842              
 -5.14               -0.00846              
 -5.21               -0.01162              
 -5.28               -0.01617              
 -5.35               -0.01583              
 -5.42               -0.01228              
 -5.49               -0.00908              
 -5.56               -0.00674              
 -5.63               -0.00467              
 -5.7                -0.00172              
 -5.77                0.00305              
 -5.84                0.00454              
 -5.91               -0.00254              
 -5.98               -0.01069              
 -6.05               -0.01329              
 -6.12               -0.00868              
 -6.19               -0.00264              
 -6.26                0.00119              
 -6.33                0.00310              
 -6.4                -0.00087              
 -6.47               -0.01006              
 -6.54               -0.01606              
 -6.61               -0.01883              
 -6.68               -0.02010              
 -6.75               -0.01766              
 -6.82               -0.01229              
 -6.89               -0.00599              
 -6.96                0.00077              
 -7.03                0.00487              
 -7.1                 0.00266              
 -7.17               -0.00409              
 -7.24               -0.01153              
 -7.31               -0.01611              
 -7.38               -0.02001              
 -7.45               -0.02305              
 -7.52               -0.02145              
 -7.59               -0.01615              
 -7.66               -0.00964              
 -7.73               -0.00408              
 -7.8                -0.00154              
 -7.87               -0.00267              
 -7.94               -0.00522              
 -8.01               -0.00452              
 -8.08                0.00192              
 -8.15                0.00825              
 -8.22                0.00958              
 -8.29                0.00469              
 -8.36               -0.00158              
 -8.43               -0.00657              
 -8.5                -0.01046              
 -8.57               -0.01177              
 -8.64               -0.01028              
 -8.71               -0.00791              
 -8.78               -0.00639              
 -8.85               -0.00548              
 -8.92               -0.00264              
 -8.99                0.00039              
 -9.06                0.00226              
 -9.13                0.00588              
 -9.2                 0.00800              
 -9.27                0.00480              
 -9.34                0.00126              
 -9.41               -0.00200              
 -9.48               -0.00740              
 -9.55               -0.01201              
 -9.62               -0.01481              
 -9.69               -0.01729              
 -9.76               -0.01839              
 -9.83               -0.01697              
 -9.9                -0.01306              
 -9.97               -0.00877              
 -10.04              -0.00666              
 -10.11              -0.00846              
 -10.18              -0.01262              
 -10.25              -0.01609              
 -10.32              -0.01614              
 -10.39              -0.01269              
 -10.46              -0.00737              
 -10.53              -0.00218              
 -10.6               -0.00017              
 -10.67              -0.00272              
 -10.74              -0.00251              
 -10.81               0.00132              
 -10.88               0.00241              
 -10.95               0.00042              
 -11.02              -0.00412              
 -11.09              -0.01123              
 -11.16              -0.01552              
 -11.23              -0.01403              
 -11.3               -0.01091              
 -11.37              -0.00764              
 -11.44              -0.00436              
 -11.51              -0.00194              
 -11.58               0.00012              
 -11.65               0.00245              
 -11.72               0.00346              
 -11.79               0.00312              
 -11.86               0.00288              
 -11.93               0.00372              
 -12.                 0.00619              
 -12.07               0.00986              
 -12.14               0.01151              
 -12.21               0.01004              
 -12.28               0.00798              
 -12.35               0.00569              
 -12.42               0.00346              
 -12.49               0.00293              
 -12.56               0.00312              
 -12.63               0.00295              
 -12.7                0.00413              
 -12.77               0.00673              
 -12.84               0.00983              
 -12.91               0.01337              
 -12.98               0.01630              
 -13.05               0.01742              
 -13.12               0.01857              
 -13.19               0.01819              
 -13.26               0.01218              
 -13.33               0.00651              
 -13.4                0.00378              
 -13.47              -0.00135              
 -13.54              -0.00592              
 -13.61              -0.00582              
 -13.68              -0.00195              
 -13.75               0.00203              
 -13.82               0.00392              
 -13.89               0.00718              
 -13.96               0.01175              
 -14.03               0.01520              
 -14.1                0.01717              
 -14.17               0.01792              
 -14.24               0.01751              
 -14.31               0.01459              
 -14.38               0.01277              
 -14.45               0.01902              
 -14.52               0.02683              
 -14.59               0.02952              
 -14.66               0.02672              
 -14.73               0.01848              
 -14.8                0.00918              
 -14.87               0.00968              
 -14.94               0.01543              
 -15.01               0.01689              
 -15.08               0.01426              
 -15.15               0.01120              
 -15.22               0.01104              
 -15.29               0.01148              
 -15.36               0.01135              
 -15.43               0.01131              
 -15.5                0.01142              
 -15.57               0.01270              
 -15.64               0.01666              
 -15.71               0.02083              
 -15.78               0.02491              
 -15.85               0.03215              
 -15.92               0.03326              
 -15.99               0.02291              
 -16.06               0.01306              
 -16.13               0.00498              
 -16.2               -0.00335              
 -16.27              -0.00494              
 -16.34              -0.00159              
 -16.41               0.00027              
 -16.48               0.00379              
 -16.55               0.00957              
 -16.62               0.01444              
 -16.69               0.01713              
 -16.76               0.01789              
 -16.83               0.01799              
 -16.9                0.01784              
 -16.97               0.01678              
 -17.04               0.01355              
 -17.11               0.01105              
 -17.18               0.01127              
 -17.25               0.01103              
 -17.32               0.01167              
 -17.39               0.01510              
 -17.46               0.01701              
 -17.53               0.01619              
 -17.6                0.01526              
 -17.67               0.01900              
 -17.74               0.02592              
 -17.81               0.02981              
 -17.88               0.03190              
 -17.95               0.03281              
 -18.02               0.03040              
 -18.09               0.02658              
 -18.16               0.02345              
 -18.23               0.02094              
 -18.3                0.01927              
 -18.37               0.01912              
 -18.44               0.02140              
 -18.51               0.02497              
 -18.58               0.02815              
 -18.65               0.03114              
 -18.72               0.03089              
 -18.79               0.02500              
 -18.86               0.02292              
 -18.93               0.02749              
 -19.                 0.03310              
 -19.07               0.03767              
 -19.14               0.04185              
 -19.21               0.04720              
 -19.28               0.04883              
 -19.35               0.04506              
 -19.42               0.04298              
 -19.49               0.04495              
 -19.56               0.04862              
 -19.63               0.04824              
 -19.7                0.04562              
 -19.77               0.04544              
 -19.84               0.04655              
 -19.91               0.04926              
 -19.98               0.05417              
 -20.05               0.05563              
 -20.12               0.05407              
 -20.19               0.05610              
 -20.26               0.06119              
 -20.33               0.06890              
 -20.4                0.08156              
 -20.47               0.09926              
 -20.54               0.1207               
 -20.61               0.14449              
 -20.68               0.17436              
 -20.75               0.21111              
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##END=
