Klinowski et al. Inorg. Chem., 22, 63-66 (1983) Figure 1b ##freq 1 ##col_ ppm Spectrum Model Si1 ----- -80.1 -0.00811 0.00015 0.00015 -80.2 -0.00811 0.00015 0.00015 -80.3 -0.00811 0.00015 0.00015 -80.4 -0.00813 0.00016 0.00016 -80.5 -0.00730 0.00016 0.00016 -80.6 -0.00581 0.00016 0.00016 -80.7 -0.00549 0.00016 0.00016 -80.8 -0.00708 0.00016 0.00016 -80.9 -0.00810 0.00016 0.00016 -81. -0.00670 0.00016 0.00016 -81.1 -0.00539 0.00016 0.00016 -81.2 -0.00618 0.00017 0.00017 -81.3 -0.00788 0.00017 0.00017 -81.4 -0.00922 0.00017 0.00017 -81.5 -0.00975 0.00017 0.00017 -81.6 -0.00976 0.00017 0.00017 -81.7 -0.00937 0.00017 0.00017 -81.8 -0.00809 0.00017 0.00017 -81.9 -0.00681 0.00018 0.00018 -82. -0.00576 0.00018 0.00018 -82.1 -0.00525 0.00018 0.00018 -82.2 -0.00603 0.00018 0.00018 -82.3 -0.00672 0.00018 0.00018 -82.4 -0.00663 0.00018 0.00018 -82.5 -0.00646 0.00018 0.00018 -82.6 -0.00646 0.00019 0.00019 -82.7 -0.00663 0.00019 0.00019 -82.8 -0.00706 0.00019 0.00019 -82.9 -0.00709 0.00019 0.00019 -83. -0.00667 0.00019 0.00019 -83.1 -0.00647 0.00019 0.00019 -83.2 -0.00694 0.00020 0.00020 -83.3 -0.00752 0.00020 0.00020 -83.4 -0.00719 0.00020 0.00020 -83.5 -0.00659 0.00020 0.00020 -83.6 -0.00648 0.00020 0.00020 -83.7 -0.00646 0.00020 0.00020 -83.8 -0.00554 0.00021 0.00021 -83.9 -0.00410 0.00021 0.00021 -84. -0.00449 0.00021 0.00021 -84.1 -0.00600 0.00021 0.00021 -84.2 -0.00667 0.00021 0.00021 -84.3 -0.00710 0.00021 0.00021 -84.4 -0.00774 0.00022 0.00022 -84.5 -0.00814 0.00022 0.00022 -84.6 -0.00805 0.00022 0.00022 -84.7 -0.00736 0.00022 0.00022 -84.8 -0.00716 0.00022 0.00022 -84.9 -0.00780 0.00023 0.00023 -85. -0.00812 0.00023 0.00023 -85.1 -0.00812 0.00023 0.00023 -85.2 -0.00811 0.00023 0.00023 -85.3 -0.00811 0.00023 0.00023 -85.4 -0.00811 0.00024 0.00024 -85.5 -0.00811 0.00024 0.00024 -85.6 -0.00811 0.00024 0.00024 -85.7 -0.00813 0.00024 0.00024 -85.8 -0.00863 0.00025 0.00025 -85.9 -0.00946 0.00025 0.00025 -86. -0.00977 0.00025 0.00025 -86.1 -0.00976 0.00025 0.00025 -86.2 -0.01012 0.00026 0.00026 -86.3 -0.01103 0.00026 0.00026 -86.4 -0.01230 0.00026 0.00026 -86.5 -0.01320 0.00026 0.00026 -86.6 -0.01365 0.00027 0.00027 -86.7 -0.01387 0.00027 0.00027 -86.8 -0.01364 0.00027 0.00027 -86.9 -0.01229 0.00027 0.00027 -87. -0.01040 0.00028 0.00028 -87.1 -0.00949 0.00028 0.00028 -87.2 -0.00967 0.00028 0.00028 -87.3 -0.01127 0.00028 0.00028 -87.4 -0.01361 0.00029 0.00029 -87.5 -0.01489 0.00029 0.00029 -87.6 -0.01509 0.00029 0.00029 -87.7 -0.01483 0.00030 0.00030 -87.8 -0.01220 0.00030 0.00030 -87.9 -0.00957 0.00030 0.00030 -88. -0.00935 0.00031 0.00031 -88.1 -0.00983 0.00031 0.00031 -88.2 -0.01185 0.00031 0.00031 -88.3 -0.01386 0.00031 0.00031 -88.4 -0.01455 0.00032 0.00032 -88.5 -0.01436 0.00032 0.00032 -88.6 -0.01353 0.00033 0.00033 -88.7 -0.01304 0.00033 0.00033 -88.8 -0.01303 0.00033 0.00033 -88.9 -0.01339 0.00034 0.00034 -89. -0.01422 0.00034 0.00034 -89.1 -0.01488 0.00034 0.00034 -89.2 -0.01531 0.00035 0.00035 -89.3 -0.01508 0.00035 0.00035 -89.4 -0.01467 0.00035 0.00035 -89.5 -0.01473 0.00036 0.00036 -89.6 -0.01548 0.00036 0.00036 -89.7 -0.01612 0.00037 0.00037 -89.8 -0.01551 0.00037 0.00037 -89.9 -0.01431 0.00038 0.00038 -90. -0.01281 0.00038 0.00038 -90.1 -0.01239 0.00038 0.00038 -90.2 -0.01265 0.00039 0.00039 -90.3 -0.01188 0.00039 0.00039 -90.4 -0.01018 0.00040 0.00040 -90.5 -0.00871 0.00040 0.00040 -90.6 -0.00902 0.00041 0.00041 -90.7 -0.01055 0.00041 0.00041 -90.8 -0.01138 0.00042 0.00042 -90.9 -0.01036 0.00042 0.00042 -91. -0.00971 0.00043 0.00043 -91.1 -0.00994 0.00043 0.00043 -91.2 -0.01061 0.00044 0.00044 -91.3 -0.01067 0.00044 0.00044 -91.4 -0.00926 0.00045 0.00045 -91.5 -0.00926 0.00045 0.00045 -91.6 -0.01136 0.00046 0.00046 -91.7 -0.01286 0.00047 0.00047 -91.8 -0.01305 0.00047 0.00047 -91.9 -0.01305 0.00048 0.00048 -92. -0.01304 0.00048 0.00048 -92.1 -0.01340 0.00049 0.00049 -92.2 -0.01375 0.00050 0.00050 -92.3 -0.01220 0.00050 0.00050 -92.4 -0.00966 0.00051 0.00051 -92.5 -0.00822 0.00052 0.00052 -92.6 -0.00809 0.00052 0.00052 -92.7 -0.00811 0.00053 0.00053 -92.8 -0.00812 0.00054 0.00054 -92.9 -0.00728 0.00055 0.00055 -93. -0.00518 0.00055 0.00055 -93.1 -0.00533 0.00056 0.00056 -93.2 -0.00711 0.00057 0.00057 -93.3 -0.00936 0.00058 0.00058 -93.4 -0.01205 0.00059 0.00059 -93.5 -0.01275 0.00059 0.00059 -93.6 -0.01150 0.00060 0.00060 -93.7 -0.01023 0.00061 0.00061 -93.8 -0.01083 0.00062 0.00062 -93.9 -0.01253 0.00063 0.00063 -94. -0.01304 0.00064 0.00064 -94.1 -0.01305 0.00065 0.00065 -94.2 -0.01197 0.00066 0.00066 -94.3 -0.01028 0.00067 0.00067 -94.4 -0.00925 0.00068 0.00068 -94.5 -0.00843 0.00069 0.00069 -94.6 -0.00878 0.00070 0.00070 -94.7 -0.01103 0.00071 0.00071 -94.8 -0.01240 0.00072 0.00072 -94.9 -0.01146 0.00073 0.00073 -95. -0.00938 0.00074 0.00074 -95.1 -0.00832 0.00076 0.00076 -95.2 -0.00869 0.00077 0.00077 -95.3 -0.00914 0.00078 0.00078 -95.4 -0.00851 0.00079 0.00079 -95.5 -0.00703 0.00081 0.00081 -95.6 -0.00720 0.00082 0.00082 -95.7 -0.00895 0.00084 0.00084 -95.8 -0.00978 0.00085 0.00085 -95.9 -0.00918 0.00086 0.00086 -96. -0.00844 0.00088 0.00088 -96.1 -0.00865 0.00089 0.00089 -96.2 -0.00983 0.00091 0.00091 -96.3 -0.01018 0.00093 0.00093 -96.4 -0.01034 0.00094 0.00094 -96.5 -0.01097 0.00096 0.00096 -96.6 -0.01140 0.00098 0.00098 -96.7 -0.01249 0.00100 0.00100 -96.8 -0.01345 0.00102 0.00102 -96.9 -0.01167 0.00103 0.00103 -97. -0.00824 0.00105 0.00105 -97.1 -0.00627 0.00107 0.00107 -97.2 -0.00605 0.00110 0.00110 -97.3 -0.00579 0.00112 0.00112 -97.4 -0.00439 0.00114 0.00114 -97.5 -0.00292 0.00116 0.00116 -97.6 -0.00216 0.00118 0.00118 -97.7 -0.00252 0.00121 0.00121 -97.8 -0.00317 0.00123 0.00123 -97.9 -0.00318 0.00126 0.00126 -98. -0.00316 0.00129 0.00129 -98.1 -0.00221 0.00131 0.00131 -98.2 -0.00074 0.00134 0.00134 -98.3 -0.00002 0.00137 0.00137 -98.4 0.00011 0.00140 0.00140 -98.5 0.00010 0.00143 0.00143 -98.6 -0.00045 0.00146 0.00146 -98.7 -0.00241 0.00150 0.00150 -98.8 -0.00506 0.00153 0.00153 -98.9 -0.00548 0.00157 0.00157 -99. -0.00445 0.00160 0.00160 -99.1 -0.00275 0.00164 0.00164 -99.2 -0.00063 0.00168 0.00168 -99.3 0.00012 0.00172 0.00172 -99.4 0.00009 0.00176 0.00176 -99.5 0.00013 0.00181 0.00181 -99.6 -0.00000 0.00185 0.00185 -99.7 -0.00088 0.00190 0.00190 -99.8 -0.00119 0.00195 0.00195 -99.9 -0.00028 0.00200 0.00200 -100. 0.00100 0.00205 0.00205 -100.1 0.00173 0.00211 0.00211 -100.2 0.00173 0.00216 0.00216 -100.3 0.00297 0.00222 0.00222 -100.4 0.00465 0.00229 0.00229 -100.5 0.00412 0.00235 0.00235 -100.6 0.00286 0.00242 0.00242 -100.7 0.00268 0.00249 0.00249 -100.8 0.00442 0.00256 0.00256 -100.9 0.00637 0.00264 0.00264 -101. 0.00718 0.00272 0.00272 -101.1 0.00659 0.00280 0.00280 -101.2 0.00496 0.00289 0.00289 -101.3 0.00529 0.00298 0.00298 -101.4 0.00701 0.00308 0.00308 -101.5 0.00790 0.00318 0.00318 -101.6 0.00812 0.00329 0.00329 -101.7 0.00767 0.00340 0.00340 -101.8 0.00703 0.00352 0.00352 -101.9 0.00668 0.00364 0.00364 -102. 0.00660 0.00377 0.00377 -102.1 0.00533 0.00391 0.00391 -102.2 0.00421 0.00406 0.00406 -102.3 0.00618 0.00421 0.00421 -102.4 0.00942 0.00437 0.00437 -102.5 0.01040 0.00455 0.00455 -102.6 0.01022 0.00473 0.00473 -102.7 0.00919 0.00492 0.00492 -102.8 0.00832 0.00513 0.00513 -102.9 0.00833 0.00535 0.00535 -103. 0.00833 0.00558 0.00558 -103.1 0.00859 0.00583 0.00583 -103.2 0.00895 0.00609 0.00609 -103.3 0.00867 0.00638 0.00638 -103.4 0.00888 0.00668 0.00668 -103.5 0.00967 0.00701 0.00701 -103.6 0.00959 0.00736 0.00736 -103.7 0.00849 0.00774 0.00774 -103.8 0.00715 0.00815 0.00815 -103.9 0.00743 0.00859 0.00859 -104. 0.00954 0.00907 0.00907 -104.1 0.01168 0.00959 0.00959 -104.2 0.01380 0.01015 0.01015 -104.3 0.01496 0.01077 0.01077 -104.4 0.01516 0.01144 0.01144 -104.5 0.01588 0.01217 0.01217 -104.6 0.01670 0.01298 0.01298 -104.7 0.01721 0.01388 0.01388 -104.8 0.01701 0.01487 0.01487 -104.9 0.01640 0.01596 0.01596 -105. 0.01677 0.01718 0.01718 -105.1 0.01981 0.01855 0.01855 -105.2 0.02288 0.02008 0.02008 -105.3 0.02333 0.02181 0.02181 -105.4 0.02314 0.02377 0.02377 -105.5 0.02383 0.02600 0.02600 -105.6 0.02462 0.02856 0.02856 -105.7 0.02386 0.03150 0.03150 -105.8 0.02312 0.03492 0.03492 -105.9 0.02612 0.03892 0.03892 -106. 0.03247 0.04363 0.04363 -106.1 0.03950 0.04923 0.04923 -106.2 0.04752 0.05595 0.05595 -106.3 0.05502 0.06413 0.06413 -106.4 0.06345 0.07423 0.07423 -106.5 0.07617 0.08694 0.08694 -106.6 0.09644 0.1033 0.1033 -106.7 0.12484 0.12480 0.12480 -106.8 0.16619 0.15366 0.15366 -106.9 0.21865 0.19283 0.19283 -107. 0.26815 0.24608 0.24608 -107.1 0.33701 0.31766 0.31766 -107.2 0.42931 0.41127 0.41127 -107.3 0.52507 0.52709 0.52709 -107.4 0.63415 0.65501 0.65501 -107.5 0.73634 0.76505 0.76505 -107.6 0.79340 0.81137 0.81137 -107.7 0.79197 0.76842 0.76842 -107.8 0.70299 0.66003 0.66003 -107.9 0.56642 0.53210 0.53210 -108. 0.40799 0.41549 0.41549 -108.1 0.27117 0.32096 0.32096 -108.2 0.19241 0.24856 0.24856 -108.3 0.14935 0.19466 0.19466 -108.4 0.12494 0.15500 0.15500 -108.5 0.10609 0.12580 0.12580 -108.6 0.09095 0.10404 0.10404 -108.7 0.08030 0.08752 0.08752 -108.8 0.07255 0.07468 0.07468 -108.9 0.06625 0.06449 0.06449 -109. 0.06216 0.05625 0.05625 -109.1 0.06050 0.04947 0.04947 -109.2 0.05986 0.04383 0.04383 -109.3 0.05843 0.03909 0.03909 -109.4 0.05607 0.03507 0.03507 -109.5 0.05364 0.03163 0.03163 -109.6 0.05075 0.02867 0.02867 -109.7 0.04820 0.02610 0.02610 -109.8 0.04542 0.02385 0.02385 -109.9 0.04192 0.02188 0.02188 -110. 0.04130 0.02015 0.02015 -110.1 0.04378 0.01861 0.01861 -110.2 0.04574 0.01723 0.01723 -110.3 0.04681 0.01601 0.01601 -110.4 0.04806 0.01491 0.01491 -110.5 0.04818 0.01391 0.01391 -110.6 0.04836 0.01302 0.01302 -110.7 0.05030 0.01221 0.01221 -110.8 0.05217 0.01147 0.01147 -110.9 0.05274 0.01079 0.01079 -111. 0.05273 0.01017 0.01017 -111.1 0.05273 0.00961 0.00961 -111.2 0.05274 0.00909 0.00909 -111.3 0.05256 0.00861 0.00861 -111.4 0.05134 0.00817 0.00817 -111.5 0.04856 0.00776 0.00776 -111.6 0.04604 0.00738 0.00738 -111.7 0.04484 0.00702 0.00702 -111.8 0.04393 0.00670 0.00670 -111.9 0.04207 0.00639 0.00639 -112. 0.04012 0.00611 0.00611 -112.1 0.03906 0.00584 0.00584 -112.2 0.03680 0.00559 0.00559 -112.3 0.03391 0.00536 0.00536 -112.4 0.03329 0.00514 0.00514 -112.5 0.03490 0.00493 0.00493 -112.6 0.03704 0.00474 0.00474 -112.7 0.03855 0.00455 0.00455 -112.8 0.03916 0.00438 0.00438 -112.9 0.03819 0.00422 0.00422 -113. 0.03633 0.00406 0.00406 -113.1 0.03555 0.00392 0.00392 -113.2 0.03432 0.00378 0.00378 -113.3 0.03234 0.00365 0.00365 -113.4 0.03045 0.00352 0.00352 -113.5 0.02881 0.00341 0.00341 -113.6 0.02795 0.00329 0.00329 -113.7 0.02711 0.00319 0.00319 -113.8 0.02643 0.00308 0.00308 -113.9 0.02642 0.00299 0.00299 -114. 0.02642 0.00290 0.00290 -114.1 0.02642 0.00281 0.00281 -114.2 0.02642 0.00272 0.00272 -114.3 0.02642 0.00264 0.00264 -114.4 0.02642 0.00257 0.00257 -114.5 0.02639 0.00249 0.00249 -114.6 0.02625 0.00242 0.00242 -114.7 0.02626 0.00235 0.00235 -114.8 0.02642 0.00229 0.00229 -114.9 0.02592 0.00223 0.00223 -115. 0.02411 0.00217 0.00217 -115.1 0.02095 0.00211 0.00211 -115.2 0.01796 0.00205 0.00205 -115.3 0.01762 0.00200 0.00200 -115.4 0.01893 0.00195 0.00195 -115.5 0.01967 0.00190 0.00190 -115.6 0.01959 0.00185 0.00185 -115.7 0.01908 0.00181 0.00181 -115.8 0.01801 0.00176 0.00176 -115.9 0.01562 0.00172 0.00172 -116. 0.01359 0.00168 0.00168 -116.1 0.01400 0.00164 0.00164 -116.2 0.01358 0.00160 0.00160 -116.3 0.01170 0.00157 0.00157 -116.4 0.00935 0.00153 0.00153 -116.5 0.00723 0.00150 0.00150 -116.6 0.00576 0.00146 0.00146 -116.7 0.00502 0.00143 0.00143 -116.8 0.00591 0.00140 0.00140 -116.9 0.00853 0.00137 0.00137 -117. 0.01045 0.00134 0.00134 -117.1 0.00906 0.00131 0.00131 -117.2 0.00564 0.00129 0.00129 -117.3 0.00344 0.00126 0.00126 -117.4 0.00534 0.00123 0.00123 -117.5 0.00822 0.00121 0.00121 -117.6 0.00896 0.00119 0.00119 -117.7 0.00639 0.00116 0.00116 -117.8 0.00273 0.00114 0.00114 -117.9 -0.00105 0.00112 0.00112 -118. -0.00248 0.00110 0.00110 -118.1 -0.00058 0.00108 0.00108 -118.2 0.00008 0.00105 0.00105 -118.3 -0.00057 0.00104 0.00104 -118.4 -0.00194 0.00102 0.00102 -118.5 -0.00309 0.00100 0.00100 -118.6 -0.00303 0.00098 0.00098 -118.7 -0.00277 0.00096 0.00096 -118.8 -0.00296 0.00094 0.00094 -118.9 -0.00360 0.00093 0.00093 -119. -0.00423 0.00091 0.00091 -119.1 -0.00469 0.00090 0.00090 -119.2 -0.00579 0.00088 0.00088 -119.3 -0.00653 0.00087 0.00087 -119.4 -0.00637 0.00085 0.00085 -119.5 -0.00564 0.00084 0.00084 -119.6 -0.00445 0.00082 0.00082 -119.7 -0.00362 0.00081 0.00081 -119.8 -0.00438 0.00080 0.00080 -119.9 -0.00686 0.00078 0.00078 -120. -0.00928 0.00077 0.00077 -120.1 -0.01017 0.00076 0.00076