Camblor et al. Chem. Commun., 749-750 (1997) Figure 2a ##freq 1 ##col_ ppm Spectrum Model Si2 Si1 Si3 Si4 ----- -100. 0.00917 0.00316 0.00029 0.00080 0.00083 0.00124 -100.02 0.01796 0.00318 0.00029 0.00080 0.00083 0.00124 -100.04 0.01678 0.00319 0.00029 0.00080 0.00083 0.00125 -100.06 0.02239 0.00320 0.00029 0.00081 0.00084 0.00126 -100.08 0.02187 0.00322 0.00029 0.00081 0.00084 0.00126 -100.1 0.02176 0.00323 0.00029 0.00081 0.00084 0.00127 -100.12 0.02191 0.00325 0.00029 0.00082 0.00085 0.00128 -100.14 0.01669 0.00326 0.00029 0.00082 0.00085 0.00128 -100.16 0.01711 0.00327 0.00029 0.00082 0.00086 0.00129 -100.18 0.01174 0.00329 0.00029 0.00083 0.00086 0.00130 -100.2 0.01023 0.00330 0.00030 0.00083 0.00086 0.00130 -100.22 0.00849 0.00332 0.00030 0.00083 0.00087 0.00131 -100.24 0.00810 0.00333 0.00030 0.00083 0.00087 0.00132 -100.26 0.01198 0.00335 0.00030 0.00084 0.00087 0.00132 -100.28 0.01185 0.00336 0.00030 0.00084 0.00088 0.00133 -100.3 0.02042 0.00338 0.00030 0.00084 0.00088 0.00134 -100.32 0.02130 0.00339 0.00030 0.00085 0.00089 0.00134 -100.34 0.02610 0.00341 0.00030 0.00085 0.00089 0.00135 -100.36 0.03004 0.00342 0.00030 0.00085 0.00089 0.00136 -100.38 0.03133 0.00344 0.00030 0.00086 0.00090 0.00137 -100.4 0.03087 0.00345 0.00031 0.00086 0.00090 0.00137 -100.42 0.03610 0.00347 0.00031 0.00086 0.00090 0.00138 -100.44 0.03592 0.00349 0.00031 0.00087 0.00091 0.00139 -100.46 0.03603 0.00350 0.00031 0.00087 0.00091 0.00139 -100.48 0.03603 0.00352 0.00031 0.00087 0.00092 0.00140 -100.5 0.03603 0.00353 0.00031 0.00088 0.00092 0.00141 -100.52 0.03607 0.00355 0.00031 0.00088 0.00092 0.00142 -100.54 0.03627 0.00357 0.00031 0.00088 0.00093 0.00143 -100.56 0.03222 0.00358 0.00031 0.00089 0.00093 0.00143 -100.58 0.03147 0.00360 0.00031 0.00089 0.00094 0.00144 -100.6 0.03122 0.00362 0.00032 0.00089 0.00094 0.00145 -100.62 0.02965 0.00363 0.00032 0.00090 0.00095 0.00146 -100.64 0.02647 0.00365 0.00032 0.00090 0.00095 0.00146 -100.66 0.02448 0.00367 0.00032 0.00091 0.00095 0.00147 -100.68 0.02188 0.00368 0.00032 0.00091 0.00096 0.00148 -100.7 0.02183 0.00370 0.00032 0.00091 0.00096 0.00149 -100.72 0.02185 0.00372 0.00032 0.00092 0.00097 0.00150 -100.74 0.02426 0.00373 0.00032 0.00092 0.00097 0.00151 -100.76 0.03154 0.00375 0.00032 0.00092 0.00098 0.00151 -100.78 0.03125 0.00377 0.00033 0.00093 0.00098 0.00152 -100.8 0.03131 0.00379 0.00033 0.00093 0.00098 0.00153 -100.82 0.03133 0.00381 0.00033 0.00093 0.00099 0.00154 -100.84 0.03139 0.00382 0.00033 0.00094 0.00099 0.00155 -100.86 0.03093 0.00384 0.00033 0.00094 0.00100 0.00156 -100.88 0.03663 0.00386 0.00033 0.00095 0.00100 0.00157 -100.9 0.03572 0.00388 0.00033 0.00095 0.00101 0.00157 -100.92 0.04136 0.00390 0.00033 0.00095 0.00101 0.00158 -100.94 0.04060 0.00392 0.00034 0.00096 0.00102 0.00159 -100.96 0.04581 0.00394 0.00034 0.00096 0.00102 0.00160 -100.98 0.04540 0.00395 0.00034 0.00097 0.00103 0.00161 -101. 0.04021 0.00397 0.00034 0.00097 0.00103 0.00162 -101.02 0.04050 0.00399 0.00034 0.00097 0.00103 0.00163 -101.04 0.03251 0.00401 0.00034 0.00098 0.00104 0.00164 -101.06 0.03095 0.00403 0.00034 0.00098 0.00104 0.00165 -101.08 0.02272 0.00405 0.00034 0.00099 0.00105 0.00166 -101.1 0.02109 0.00407 0.00034 0.00099 0.00105 0.00167 -101.12 0.01547 0.00409 0.00035 0.00099 0.00106 0.00168 -101.14 0.00962 0.00411 0.00035 0.00100 0.00106 0.00169 -101.16 0.01022 0.00413 0.00035 0.00100 0.00107 0.00170 -101.18 0.01160 0.00415 0.00035 0.00101 0.00107 0.00171 -101.2 0.01887 0.00417 0.00035 0.00101 0.00108 0.00172 -101.22 0.03050 0.00420 0.00035 0.00101 0.00108 0.00173 -101.24 0.03596 0.00422 0.00035 0.00102 0.00109 0.00174 -101.26 0.03908 0.00424 0.00035 0.00102 0.00110 0.00175 -101.28 0.03366 0.00426 0.00036 0.00103 0.00110 0.00176 -101.3 0.02562 0.00428 0.00036 0.00103 0.00111 0.00177 -101.32 0.00773 0.00430 0.00036 0.00104 0.00111 0.00178 -101.34 -0.01254 0.00432 0.00036 0.00104 0.00112 0.00179 -101.36 -0.02309 0.00435 0.00036 0.00105 0.00112 0.00180 -101.38 -0.04545 0.00437 0.00036 0.00105 0.00113 0.00181 -101.4 -0.04402 0.00439 0.00036 0.00105 0.00113 0.00183 -101.42 -0.03756 0.00441 0.00037 0.00106 0.00114 0.00184 -101.44 -0.03553 0.00444 0.00037 0.00106 0.00114 0.00185 -101.46 -0.03268 0.00446 0.00037 0.00107 0.00115 0.00186 -101.48 -0.02514 0.00448 0.00037 0.00107 0.00115 0.00187 -101.5 -0.01638 0.00451 0.00037 0.00108 0.00116 0.00188 -101.52 -0.00602 0.00453 0.00037 0.00108 0.00117 0.00189 -101.54 -0.00403 0.00455 0.00037 0.00109 0.00117 0.00191 -101.56 0.00117 0.00458 0.00037 0.00109 0.00118 0.00192 -101.58 0.00291 0.00460 0.00038 0.00110 0.00118 0.00193 -101.6 0.00583 0.00462 0.00038 0.00110 0.00119 0.00194 -101.62 0.01018 0.00465 0.00038 0.00111 0.00120 0.00195 -101.64 0.01016 0.00467 0.00038 0.00111 0.00120 0.00197 -101.66 0.01062 0.00470 0.00038 0.00112 0.00121 0.00198 -101.68 0.01213 0.00472 0.00038 0.00112 0.00121 0.00199 -101.7 0.01768 0.00475 0.00038 0.00112 0.00122 0.00201 -101.72 0.01713 0.00477 0.00039 0.00113 0.00123 0.00202 -101.74 0.01716 0.00480 0.00039 0.00113 0.00123 0.00203 -101.76 0.01719 0.00483 0.00039 0.00114 0.00124 0.00204 -101.78 0.01761 0.00485 0.00039 0.00114 0.00124 0.00206 -101.8 0.01253 0.00488 0.00039 0.00115 0.00125 0.00207 -101.82 0.01271 0.00491 0.00039 0.00116 0.00126 0.00208 -101.84 0.01262 0.00493 0.00040 0.00116 0.00126 0.00210 -101.86 0.01772 0.00496 0.00040 0.00117 0.00127 0.00211 -101.88 0.01762 0.00499 0.00040 0.00117 0.00128 0.00213 -101.9 0.02238 0.00501 0.00040 0.00118 0.00128 0.00214 -101.92 0.02271 0.00504 0.00040 0.00118 0.00129 0.00215 -101.94 0.02642 0.00507 0.00040 0.00119 0.00130 0.00217 -101.96 0.03193 0.00510 0.00040 0.00119 0.00130 0.00218 -101.98 0.02942 0.00513 0.00041 0.00120 0.00131 0.00220 -102. 0.02534 0.00516 0.00041 0.00120 0.00132 0.00221 -102.02 0.01740 0.00518 0.00041 0.00121 0.00132 0.00223 -102.04 0.01429 0.00521 0.00041 0.00121 0.00133 0.00224 -102.06 0.01036 0.00524 0.00041 0.00122 0.00134 0.00226 -102.08 0.00056 0.00527 0.00041 0.00123 0.00135 0.00227 -102.1 -0.00882 0.00530 0.00042 0.00123 0.00135 0.00229 -102.12 -0.00882 0.00533 0.00042 0.00124 0.00136 0.00231 -102.14 -0.02094 0.00536 0.00042 0.00124 0.00137 0.00232 -102.16 -0.01998 0.00539 0.00042 0.00125 0.00137 0.00234 -102.18 -0.02618 0.00543 0.00042 0.00125 0.00138 0.00235 -102.2 -0.02995 0.00546 0.00042 0.00126 0.00139 0.00237 -102.22 -0.03253 0.00549 0.00043 0.00127 0.00140 0.00239 -102.24 -0.03255 0.00552 0.00043 0.00127 0.00140 0.00240 -102.26 -0.02523 0.00555 0.00043 0.00128 0.00141 0.00242 -102.28 -0.02035 0.00559 0.00043 0.00128 0.00142 0.00244 -102.3 -0.01517 0.00562 0.00043 0.00129 0.00143 0.00245 -102.32 -0.01165 0.00565 0.00043 0.00130 0.00143 0.00247 -102.34 0.00065 0.00568 0.00044 0.00130 0.00144 0.00249 -102.36 0.01675 0.00572 0.00044 0.00131 0.00145 0.00251 -102.38 0.02962 0.00575 0.00044 0.00131 0.00146 0.00253 -102.4 0.03144 0.00579 0.00044 0.00132 0.00147 0.00254 -102.42 0.03661 0.00582 0.00044 0.00133 0.00147 0.00256 -102.44 0.03647 0.00586 0.00044 0.00133 0.00148 0.00258 -102.46 0.04110 0.00589 0.00045 0.00134 0.00149 0.00260 -102.48 0.04079 0.00593 0.00045 0.00135 0.00150 0.00262 -102.5 0.04061 0.00596 0.00045 0.00135 0.00151 0.00264 -102.52 0.03969 0.00600 0.00045 0.00136 0.00152 0.00266 -102.54 0.03583 0.00604 0.00045 0.00137 0.00152 0.00268 -102.56 0.03597 0.00607 0.00046 0.00137 0.00153 0.00270 -102.58 0.03612 0.00611 0.00046 0.00138 0.00154 0.00272 -102.6 0.03782 0.00615 0.00046 0.00139 0.00155 0.00274 -102.62 0.04085 0.00619 0.00046 0.00139 0.00156 0.00276 -102.64 0.04285 0.00622 0.00046 0.00140 0.00157 0.00278 -102.66 0.04543 0.00626 0.00046 0.00141 0.00158 0.00280 -102.68 0.04086 0.00630 0.00047 0.00141 0.00159 0.00282 -102.7 0.03589 0.00634 0.00047 0.00142 0.00160 0.00284 -102.72 0.03310 0.00638 0.00047 0.00143 0.00160 0.00287 -102.74 0.03118 0.00642 0.00047 0.00143 0.00161 0.00289 -102.76 0.02745 0.00646 0.00047 0.00144 0.00162 0.00291 -102.78 0.02062 0.00651 0.00048 0.00145 0.00163 0.00293 -102.8 0.01695 0.00655 0.00048 0.00146 0.00164 0.00295 -102.82 0.01683 0.00659 0.00048 0.00146 0.00165 0.00298 -102.84 0.02135 0.00663 0.00048 0.00147 0.00166 0.00300 -102.86 0.02343 0.00667 0.00048 0.00148 0.00167 0.00303 -102.88 0.02652 0.00672 0.00049 0.00149 0.00168 0.00305 -102.9 0.03384 0.00676 0.00049 0.00149 0.00169 0.00307 -102.92 0.03606 0.00681 0.00049 0.00150 0.00170 0.00310 -102.94 0.03657 0.00685 0.00049 0.00151 0.00171 0.00312 -102.96 0.03124 0.00690 0.00050 0.00152 0.00172 0.00315 -102.98 0.02865 0.00694 0.00050 0.00152 0.00173 0.00317 -103. 0.02668 0.00699 0.00050 0.00153 0.00174 0.00320 -103.02 0.02655 0.00703 0.00050 0.00154 0.00175 0.00322 -103.04 0.02647 0.00708 0.00050 0.00155 0.00176 0.00325 -103.06 0.02966 0.00713 0.00051 0.00156 0.00177 0.00328 -103.08 0.03635 0.00718 0.00051 0.00156 0.00178 0.00330 -103.1 0.03610 0.00722 0.00051 0.00157 0.00180 0.00333 -103.12 0.03743 0.00727 0.00051 0.00158 0.00181 0.00336 -103.14 0.04087 0.00732 0.00051 0.00159 0.00182 0.00339 -103.16 0.04067 0.00737 0.00052 0.00160 0.00183 0.00342 -103.18 0.04094 0.00742 0.00052 0.00160 0.00184 0.00344 -103.2 0.03594 0.00748 0.00052 0.00161 0.00185 0.00347 -103.22 0.03130 0.00753 0.00052 0.00162 0.00186 0.00350 -103.24 0.02092 0.00758 0.00053 0.00163 0.00187 0.00353 -103.26 0.01687 0.00763 0.00053 0.00164 0.00189 0.00356 -103.28 0.01010 0.00769 0.00053 0.00165 0.00190 0.00359 -103.3 0.00201 0.00774 0.00053 0.00166 0.00191 0.00363 -103.32 -0.00329 0.00779 0.00054 0.00167 0.00192 0.00366 -103.34 -0.00657 0.00785 0.00054 0.00167 0.00193 0.00369 -103.36 -0.00629 0.00791 0.00054 0.00168 0.00195 0.00372 -103.38 -0.00571 0.00796 0.00054 0.00169 0.00196 0.00375 -103.4 -0.00430 0.00802 0.00054 0.00170 0.00197 0.00379 -103.42 0.00161 0.00808 0.00055 0.00171 0.00198 0.00382 -103.44 0.00743 0.00814 0.00055 0.00172 0.00200 0.00385 -103.46 0.00873 0.00819 0.00055 0.00173 0.00201 0.00389 -103.48 0.02170 0.00825 0.00055 0.00174 0.00202 0.00392 -103.5 0.02167 0.00832 0.00056 0.00175 0.00204 0.00396 -103.52 0.02188 0.00838 0.00056 0.00176 0.00205 0.00399 -103.54 0.02193 0.00844 0.00056 0.00177 0.00206 0.00403 -103.56 0.02199 0.00850 0.00056 0.00178 0.00208 0.00407 -103.58 0.01862 0.00856 0.00057 0.00179 0.00209 0.00410 -103.6 0.01668 0.00863 0.00057 0.00180 0.00210 0.00414 -103.62 0.01039 0.00869 0.00057 0.00181 0.00212 0.00418 -103.64 0.01013 0.00876 0.00058 0.00182 0.00213 0.00422 -103.66 0.01010 0.00883 0.00058 0.00183 0.00215 0.00426 -103.68 0.01010 0.00889 0.00058 0.00184 0.00216 0.00430 -103.7 0.01010 0.00896 0.00058 0.00185 0.00217 0.00434 -103.72 0.01010 0.00903 0.00059 0.00186 0.00219 0.00438 -103.74 0.01010 0.00910 0.00059 0.00187 0.00220 0.00442 -103.76 0.01010 0.00917 0.00059 0.00188 0.00222 0.00446 -103.78 0.01010 0.00924 0.00059 0.00189 0.00223 0.00451 -103.8 0.01010 0.00931 0.00060 0.00190 0.00225 0.00455 -103.82 0.01010 0.00939 0.00060 0.00191 0.00226 0.00460 -103.84 0.01012 0.00946 0.00060 0.00192 0.00228 0.00464 -103.86 0.01016 0.00954 0.00061 0.00193 0.00230 0.00469 -103.88 0.00935 0.00961 0.00061 0.00195 0.00231 0.00473 -103.9 0.01781 0.00969 0.00061 0.00196 0.00233 0.00478 -103.92 0.01707 0.00977 0.00061 0.00197 0.00234 0.00483 -103.94 0.01716 0.00985 0.00062 0.00198 0.00236 0.00487 -103.96 0.01720 0.00993 0.00062 0.00199 0.00238 0.00492 -103.98 0.01744 0.01001 0.00062 0.00200 0.00239 0.00497 -104. 0.01312 0.01009 0.00063 0.00202 0.00241 0.00502 -104.02 0.00743 0.01017 0.00063 0.00203 0.00243 0.00507 -104.04 0.00769 0.01026 0.00063 0.00204 0.00245 0.00513 -104.06 0.00320 0.01034 0.00063 0.00205 0.00246 0.00518 -104.08 -0.00152 0.01043 0.00064 0.00206 0.00248 0.00523 -104.1 0.00303 0.01052 0.00064 0.00208 0.00250 0.00529 -104.12 0.00838 0.01061 0.00064 0.00209 0.00252 0.00534 -104.14 0.01265 0.01070 0.00065 0.00210 0.00253 0.00540 -104.16 0.01214 0.01079 0.00065 0.00211 0.00255 0.00546 -104.18 0.01945 0.01088 0.00065 0.00213 0.00257 0.00551 -104.2 0.02160 0.01097 0.00066 0.00214 0.00259 0.00557 -104.22 0.02223 0.01107 0.00066 0.00215 0.00261 0.00563 -104.24 0.01530 0.01116 0.00066 0.00217 0.00263 0.00569 -104.26 0.01243 0.01126 0.00067 0.00218 0.00265 0.00576 -104.28 0.00808 0.01136 0.00067 0.00219 0.00267 0.00582 -104.3 0.00533 0.01146 0.00067 0.00221 0.00269 0.00588 -104.32 0.00544 0.01156 0.00068 0.00222 0.00271 0.00595 -104.34 0.00538 0.01167 0.00068 0.00223 0.00273 0.00601 -104.36 0.01383 0.01177 0.00068 0.00225 0.00275 0.00608 -104.38 0.02196 0.01188 0.00069 0.00226 0.00277 0.00615 -104.4 0.02423 0.01199 0.00069 0.00227 0.00279 0.00622 -104.42 0.03155 0.01210 0.00069 0.00229 0.00281 0.00629 -104.44 0.03124 0.01221 0.00070 0.00230 0.00283 0.00636 -104.46 0.03125 0.01232 0.00070 0.00232 0.00285 0.00643 -104.48 0.03182 0.01243 0.00070 0.00233 0.00288 0.00651 -104.5 0.02641 0.01255 0.00071 0.00235 0.00290 0.00658 -104.52 0.02264 0.01267 0.00071 0.00236 0.00292 0.00666 -104.54 0.02194 0.01279 0.00071 0.00238 0.00294 0.00674 -104.56 0.02216 0.01291 0.00072 0.00239 0.00297 0.00682 -104.58 0.01678 0.01303 0.00072 0.00241 0.00299 0.00690 -104.6 0.01706 0.01316 0.00073 0.00242 0.00301 0.00698 -104.62 0.02234 0.01329 0.00073 0.00244 0.00304 0.00706 -104.64 0.02187 0.01341 0.00073 0.00245 0.00306 0.00715 -104.66 0.02473 0.01355 0.00074 0.00247 0.00309 0.00724 -104.68 0.02688 0.01368 0.00074 0.00249 0.00311 0.00733 -104.7 0.03172 0.01381 0.00074 0.00250 0.00314 0.00742 -104.72 0.03135 0.01395 0.00075 0.00252 0.00316 0.00751 -104.74 0.03131 0.01409 0.00075 0.00254 0.00319 0.00760 -104.76 0.03132 0.01423 0.00076 0.00255 0.00321 0.00770 -104.78 0.03132 0.01438 0.00076 0.00257 0.00324 0.00779 -104.8 0.03132 0.01452 0.00076 0.00259 0.00327 0.00789 -104.82 0.03132 0.01467 0.00077 0.00260 0.00329 0.00799 -104.84 0.03132 0.01483 0.00077 0.00262 0.00332 0.00810 -104.86 0.03132 0.01498 0.00078 0.00264 0.00335 0.00820 -104.88 0.03132 0.01514 0.00078 0.00266 0.00338 0.00831 -104.9 0.03132 0.01530 0.00078 0.00268 0.00340 0.00842 -104.92 0.03136 0.01546 0.00079 0.00269 0.00343 0.00853 -104.94 0.02857 0.01562 0.00079 0.00271 0.00346 0.00864 -104.96 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