Klinowski and Anderson. J. Chem. Soc., Faraday Trans., 82, 569-584 (1986) Figure 2c ##freq 1 ##col_ ppm Spectrum Model Si1 Si2 ----- -70.16 0.00744 0.00100 0.00021 0.00078 -70.2 0.00748 0.00100 0.00022 0.00078 -70.24 0.00770 0.00100 0.00022 0.00078 -70.28 0.00791 0.00100 0.00022 0.00078 -70.32 0.00792 0.00101 0.00022 0.00078 -70.36 0.00788 0.00101 0.00022 0.00079 -70.4 0.00789 0.00101 0.00022 0.00079 -70.44 0.00789 0.00101 0.00022 0.00079 -70.48 0.00789 0.00101 0.00022 0.00079 -70.52 0.00789 0.00102 0.00022 0.00079 -70.56 0.00789 0.00102 0.00022 0.00080 -70.6 0.00788 0.00102 0.00022 0.00080 -70.64 0.00792 0.00102 0.00022 0.00080 -70.68 0.00791 0.00103 0.00022 0.00080 -70.72 0.00771 0.00103 0.00022 0.00080 -70.76 0.00749 0.00103 0.00022 0.00080 -70.8 0.00745 0.00103 0.00022 0.00081 -70.84 0.00755 0.00103 0.00022 0.00081 -70.88 0.00757 0.00104 0.00022 0.00081 -70.92 0.00721 0.00104 0.00022 0.00081 -70.96 0.00674 0.00104 0.00022 0.00081 -71. 0.00666 0.00104 0.00022 0.00082 -71.04 0.00674 0.00105 0.00022 0.00082 -71.08 0.00674 0.00105 0.00022 0.00082 -71.12 0.00672 0.00105 0.00022 0.00082 -71.16 0.00673 0.00105 0.00023 0.00082 -71.2 0.00674 0.00106 0.00023 0.00083 -71.24 0.00673 0.00106 0.00023 0.00083 -71.28 0.00660 0.00106 0.00023 0.00083 -71.32 0.00610 0.00106 0.00023 0.00083 -71.36 0.00535 0.00107 0.00023 0.00083 -71.4 0.00509 0.00107 0.00023 0.00083 -71.44 0.00518 0.00107 0.00023 0.00084 -71.48 0.00500 0.00107 0.00023 0.00084 -71.52 0.00476 0.00107 0.00023 0.00084 -71.56 0.00474 0.00108 0.00023 0.00084 -71.6 0.00484 0.00108 0.00023 0.00084 -71.64 0.00484 0.00108 0.00023 0.00085 -71.68 0.00449 0.00108 0.00023 0.00085 -71.72 0.00399 0.00109 0.00023 0.00085 -71.76 0.00368 0.00109 0.00023 0.00085 -71.8 0.00365 0.00109 0.00023 0.00086 -71.84 0.00369 0.00109 0.00023 0.00086 -71.88 0.00337 0.00110 0.00023 0.00086 -71.92 0.00288 0.00110 0.00023 0.00086 -71.96 0.00278 0.00110 0.00023 0.00086 -72. 0.00286 0.00110 0.00023 0.00087 -72.04 0.00286 0.00111 0.00023 0.00087 -72.08 0.00287 0.00111 0.00024 0.00087 -72.12 0.00288 0.00111 0.00024 0.00087 -72.16 0.00269 0.00111 0.00024 0.00087 -72.2 0.00246 0.00112 0.00024 0.00088 -72.24 0.00242 0.00112 0.00024 0.00088 -72.28 0.00249 0.00112 0.00024 0.00088 -72.32 0.00251 0.00113 0.00024 0.00088 -72.36 0.00233 0.00113 0.00024 0.00088 -72.4 0.00209 0.00113 0.00024 0.00089 -72.44 0.00208 0.00113 0.00024 0.00089 -72.48 0.00206 0.00114 0.00024 0.00089 -72.52 0.00181 0.00114 0.00024 0.00089 -72.56 0.00165 0.00114 0.00024 0.00090 -72.6 0.00168 0.00114 0.00024 0.00090 -72.64 0.00170 0.00115 0.00024 0.00090 -72.68 0.00169 0.00115 0.00024 0.00090 -72.72 0.00172 0.00115 0.00024 0.00090 -72.76 0.00165 0.00115 0.00024 0.00091 -72.8 0.00142 0.00116 0.00024 0.00091 -72.84 0.00114 0.00116 0.00024 0.00091 -72.88 0.00093 0.00116 0.00024 0.00091 -72.92 0.00088 0.00117 0.00025 0.00092 -72.96 0.00093 0.00117 0.00025 0.00092 -73. 0.00096 0.00117 0.00025 0.00092 -73.04 0.00083 0.00117 0.00025 0.00092 -73.08 0.00058 0.00118 0.00025 0.00092 -73.12 0.00049 0.00118 0.00025 0.00093 -73.16 0.00053 0.00118 0.00025 0.00093 -73.2 0.00054 0.00118 0.00025 0.00093 -73.24 0.00053 0.00119 0.00025 0.00093 -73.28 0.00053 0.00119 0.00025 0.00094 -73.32 0.00052 0.00119 0.00025 0.00094 -73.36 0.00052 0.00120 0.00025 0.00094 -73.4 0.00057 0.00120 0.00025 0.00094 -73.44 0.00051 0.00120 0.00025 0.00095 -73.48 0.00027 0.00120 0.00025 0.00095 -73.52 0.00011 0.00121 0.00025 0.00095 -73.56 0.00013 0.00121 0.00025 0.00095 -73.6 0.00014 0.00121 0.00025 0.00095 -73.64 0.00014 0.00122 0.00025 0.00096 -73.68 0.00018 0.00122 0.00025 0.00096 -73.72 0.00010 0.00122 0.00026 0.00096 -73.76 -0.00014 0.00123 0.00026 0.00096 -73.8 -0.00028 0.00123 0.00026 0.00097 -73.84 -0.00025 0.00123 0.00026 0.00097 -73.88 -0.00022 0.00123 0.00026 0.00097 -73.92 -0.00024 0.00124 0.00026 0.00097 -73.96 -0.00028 0.00124 0.00026 0.00098 -74. -0.00016 0.00124 0.00026 0.00098 -74.04 0.00008 0.00125 0.00026 0.00098 -74.08 0.00018 0.00125 0.00026 0.00098 -74.12 0.00014 0.00125 0.00026 0.00099 -74.16 0.00013 0.00126 0.00026 0.00099 -74.2 0.00014 0.00126 0.00026 0.00099 -74.24 0.00014 0.00126 0.00026 0.00099 -74.28 0.00014 0.00126 0.00026 0.00100 -74.32 0.00014 0.00127 0.00026 0.00100 -74.36 0.00014 0.00127 0.00026 0.00100 -74.4 0.00014 0.00127 0.00026 0.00100 -74.44 0.00014 0.00128 0.00026 0.00101 -74.48 0.00014 0.00128 0.00027 0.00101 -74.52 0.00014 0.00128 0.00027 0.00101 -74.56 0.00014 0.00129 0.00027 0.00102 -74.6 0.00014 0.00129 0.00027 0.00102 -74.64 0.00014 0.00129 0.00027 0.00102 -74.68 0.00014 0.00130 0.00027 0.00102 -74.72 0.00014 0.00130 0.00027 0.00103 -74.76 0.00014 0.00130 0.00027 0.00103 -74.8 0.00014 0.00131 0.00027 0.00103 -74.84 0.00014 0.00131 0.00027 0.00103 -74.88 0.00014 0.00131 0.00027 0.00104 -74.92 0.00014 0.00132 0.00027 0.00104 -74.96 0.00014 0.00132 0.00027 0.00104 -75. 0.00014 0.00132 0.00027 0.00104 -75.04 0.00014 0.00133 0.00027 0.00105 -75.08 0.00014 0.00133 0.00027 0.00105 -75.12 0.00014 0.00133 0.00027 0.00105 -75.16 0.00014 0.00134 0.00027 0.00106 -75.2 0.00014 0.00134 0.00028 0.00106 -75.24 0.00014 0.00134 0.00028 0.00106 -75.28 0.00014 0.00135 0.00028 0.00106 -75.32 0.00014 0.00135 0.00028 0.00107 -75.36 0.00014 0.00135 0.00028 0.00107 -75.4 0.00013 0.00136 0.00028 0.00107 -75.44 0.00015 0.00136 0.00028 0.00108 -75.48 0.00017 0.00136 0.00028 0.00108 -75.52 0.00003 0.00137 0.00028 0.00108 -75.56 -0.00021 0.00137 0.00028 0.00108 -75.6 -0.00031 0.00137 0.00028 0.00109 -75.64 -0.00021 0.00138 0.00028 0.00109 -75.68 0.00003 0.00138 0.00028 0.00109 -75.72 0.00018 0.00138 0.00028 0.00110 -75.76 0.00015 0.00139 0.00028 0.00110 -75.8 0.00013 0.00139 0.00028 0.00110 -75.84 0.00014 0.00139 0.00028 0.00111 -75.88 0.00014 0.00140 0.00029 0.00111 -75.92 0.00014 0.00140 0.00029 0.00111 -75.96 0.00014 0.00141 0.00029 0.00111 -76. 0.00014 0.00141 0.00029 0.00112 -76.04 0.00014 0.00141 0.00029 0.00112 -76.08 0.00014 0.00142 0.00029 0.00112 -76.12 0.00014 0.00142 0.00029 0.00113 -76.16 0.00014 0.00142 0.00029 0.00113 -76.2 0.00014 0.00143 0.00029 0.00113 -76.24 0.00014 0.00143 0.00029 0.00114 -76.28 0.00015 0.00144 0.00029 0.00114 -76.32 0.00014 0.00144 0.00029 0.00114 -76.36 0.00010 0.00144 0.00029 0.00115 -76.4 0.00019 0.00145 0.00029 0.00115 -76.44 0.00043 0.00145 0.00029 0.00115 -76.48 0.00058 0.00145 0.00029 0.00115 -76.52 0.00054 0.00146 0.00030 0.00116 -76.56 0.00048 0.00146 0.00030 0.00116 -76.6 0.00055 0.00147 0.00030 0.00116 -76.64 0.00079 0.00147 0.00030 0.00117 -76.68 0.00094 0.00147 0.00030 0.00117 -76.72 0.00092 0.00148 0.00030 0.00117 -76.76 0.00098 0.00148 0.00030 0.00118 -76.8 0.00128 0.00149 0.00030 0.00118 -76.84 0.00179 0.00149 0.00030 0.00118 -76.88 0.00211 0.00149 0.00030 0.00119 -76.92 0.00209 0.00150 0.00030 0.00119 -76.96 0.00215 0.00150 0.00030 0.00119 -77. 0.00241 0.00151 0.00030 0.00120 -77.04 0.00265 0.00151 0.00030 0.00120 -77.08 0.00287 0.00151 0.00030 0.00120 -77.12 0.00314 0.00152 0.00031 0.00121 -77.16 0.00326 0.00152 0.00031 0.00121 -77.2 0.00323 0.00153 0.00031 0.00121 -77.24 0.00334 0.00153 0.00031 0.00122 -77.28 0.00361 0.00153 0.00031 0.00122 -77.32 0.00386 0.00154 0.00031 0.00122 -77.36 0.00405 0.00154 0.00031 0.00123 -77.4 0.00424 0.00155 0.00031 0.00123 -77.44 0.00463 0.00155 0.00031 0.00124 -77.48 0.00511 0.00156 0.00031 0.00124 -77.52 0.00525 0.00156 0.00031 0.00124 -77.56 0.00518 0.00156 0.00031 0.00125 -77.6 0.00517 0.00157 0.00031 0.00125 -77.64 0.00517 0.00157 0.00031 0.00125 -77.68 0.00515 0.00158 0.00031 0.00126 -77.72 0.00530 0.00158 0.00032 0.00126 -77.76 0.00555 0.00159 0.00032 0.00126 -77.8 0.00564 0.00159 0.00032 0.00127 -77.84 0.00553 0.00159 0.00032 0.00127 -77.88 0.00528 0.00160 0.00032 0.00128 -77.92 0.00514 0.00160 0.00032 0.00128 -77.96 0.00517 0.00161 0.00032 0.00128 -78. 0.00519 0.00161 0.00032 0.00129 -78.04 0.00518 0.00162 0.00032 0.00129 -78.08 0.00518 0.00162 0.00032 0.00129 -78.12 0.00518 0.00163 0.00032 0.00130 -78.16 0.00518 0.00163 0.00032 0.00130 -78.2 0.00518 0.00163 0.00032 0.00131 -78.24 0.00518 0.00164 0.00032 0.00131 -78.28 0.00516 0.00164 0.00033 0.00131 -78.32 0.00519 0.00165 0.00033 0.00132 -78.36 0.00537 0.00165 0.00033 0.00132 -78.4 0.00579 0.00166 0.00033 0.00132 -78.44 0.00627 0.00166 0.00033 0.00133 -78.48 0.00638 0.00167 0.00033 0.00133 -78.52 0.00634 0.00167 0.00033 0.00134 -78.56 0.00656 0.00168 0.00033 0.00134 -78.6 0.00676 0.00168 0.00033 0.00134 -78.64 0.00675 0.00169 0.00033 0.00135 -78.68 0.00672 0.00169 0.00033 0.00135 -78.72 0.00673 0.00170 0.00033 0.00136 -78.76 0.00674 0.00170 0.00033 0.00136 -78.8 0.00673 0.00171 0.00034 0.00136 -78.84 0.00671 0.00171 0.00034 0.00137 -78.88 0.00677 0.00171 0.00034 0.00137 -78.92 0.00679 0.00172 0.00034 0.00138 -78.96 0.00642 0.00172 0.00034 0.00138 -79. 0.00596 0.00173 0.00034 0.00139 -79.04 0.00589 0.00173 0.00034 0.00139 -79.08 0.00596 0.00174 0.00034 0.00139 -79.12 0.00593 0.00174 0.00034 0.00140 -79.16 0.00605 0.00175 0.00034 0.00140 -79.2 0.00631 0.00175 0.00034 0.00141 -79.24 0.00643 0.00176 0.00034 0.00141 -79.28 0.00632 0.00177 0.00034 0.00142 -79.32 0.00605 0.00177 0.00035 0.00142 -79.36 0.00596 0.00178 0.00035 0.00142 -79.4 0.00600 0.00178 0.00035 0.00143 -79.44 0.00567 0.00179 0.00035 0.00143 -79.48 0.00519 0.00179 0.00035 0.00144 -79.52 0.00510 0.00180 0.00035 0.00144 -79.56 0.00520 0.00180 0.00035 0.00145 -79.6 0.00522 0.00181 0.00035 0.00145 -79.64 0.00509 0.00181 0.00035 0.00145 -79.68 0.00484 0.00182 0.00035 0.00146 -79.72 0.00456 0.00182 0.00035 0.00146 -79.76 0.00440 0.00183 0.00035 0.00147 -79.8 0.00442 0.00183 0.00036 0.00147 -79.84 0.00434 0.00184 0.00036 0.00148 -79.88 0.00408 0.00184 0.00036 0.00148 -79.92 0.00400 0.00185 0.00036 0.00149 -79.96 0.00402 0.00186 0.00036 0.00149 -80. 0.00385 0.00186 0.00036 0.00150 -80.04 0.00357 0.00187 0.00036 0.00150 -80.08 0.00333 0.00187 0.00036 0.00151 -80.12 0.00316 0.00188 0.00036 0.00151 -80.16 0.00293 0.00188 0.00036 0.00152 -80.2 0.00247 0.00189 0.00036 0.00152 -80.24 0.00206 0.00190 0.00037 0.00153 -80.28 0.00202 0.00190 0.00037 0.00153 -80.32 0.00210 0.00191 0.00037 0.00153 -80.36 0.00210 0.00191 0.00037 0.00154 -80.4 0.00200 0.00192 0.00037 0.00154 -80.44 0.00172 0.00192 0.00037 0.00155 -80.48 0.00124 0.00193 0.00037 0.00155 -80.52 0.00088 0.00194 0.00037 0.00156 -80.56 0.00087 0.00194 0.00037 0.00156 -80.6 0.00093 0.00195 0.00037 0.00157 -80.64 0.00092 0.00195 0.00037 0.00157 -80.68 0.00091 0.00196 0.00037 0.00158 -80.72 0.00092 0.00197 0.00038 0.00158 -80.76 0.00092 0.00197 0.00038 0.00159 -80.8 0.00091 0.00198 0.00038 0.00160 -80.84 0.00091 0.00198 0.00038 0.00160 -80.88 0.00092 0.00199 0.00038 0.00161 -80.92 0.00092 0.00200 0.00038 0.00161 -80.96 0.00090 0.00200 0.00038 0.00162 -81. 0.00092 0.00201 0.00038 0.00162 -81.04 0.00096 0.00201 0.00038 0.00163 -81.08 0.00082 0.00202 0.00038 0.00163 -81.12 0.00057 0.00203 0.00039 0.00164 -81.16 0.00049 0.00203 0.00039 0.00164 -81.2 0.00053 0.00204 0.00039 0.00165 -81.24 0.00054 0.00205 0.00039 0.00165 -81.28 0.00053 0.00205 0.00039 0.00166 -81.32 0.00053 0.00206 0.00039 0.00166 -81.36 0.00053 0.00207 0.00039 0.00167 -81.4 0.00053 0.00207 0.00039 0.00168 -81.44 0.00054 0.00208 0.00039 0.00168 -81.48 0.00052 0.00209 0.00039 0.00169 -81.52 0.00049 0.00209 0.00039 0.00169 -81.56 0.00061 0.00210 0.00040 0.00170 -81.6 0.00087 0.00211 0.00040 0.00170 -81.64 0.00096 0.00211 0.00040 0.00171 -81.68 0.00092 0.00212 0.00040 0.00172 -81.72 0.00091 0.00213 0.00040 0.00172 -81.76 0.00092 0.00213 0.00040 0.00173 -81.8 0.00091 0.00214 0.00040 0.00173 -81.84 0.00093 0.00215 0.00040 0.00174 -81.88 0.00093 0.00215 0.00040 0.00174 -81.92 0.00084 0.00216 0.00040 0.00175 -81.96 0.00096 0.00217 0.00041 0.00176 -82. 0.00145 0.00217 0.00041 0.00176 -82.04 0.00176 0.00218 0.00041 0.00177 -82.08 0.00172 0.00219 0.00041 0.00177 -82.12 0.00168 0.00220 0.00041 0.00178 -82.16 0.00169 0.00220 0.00041 0.00179 -82.2 0.00165 0.00221 0.00041 0.00179 -82.24 0.00174 0.00222 0.00041 0.00180 -82.28 0.00199 0.00222 0.00041 0.00181 -82.32 0.00212 0.00223 0.00042 0.00181 -82.36 0.00209 0.00224 0.00042 0.00182 -82.4 0.00207 0.00225 0.00042 0.00182 -82.44 0.00208 0.00225 0.00042 0.00183 -82.48 0.00208 0.00226 0.00042 0.00184 -82.52 0.00208 0.00227 0.00042 0.00184 -82.56 0.00208 0.00228 0.00042 0.00185 -82.6 0.00208 0.00228 0.00042 0.00186 -82.64 0.00208 0.00229 0.00042 0.00186 -82.68 0.00208 0.00230 0.00042 0.00187 -82.72 0.00208 0.00231 0.00043 0.00188 -82.76 0.00208 0.00231 0.00043 0.00188 -82.8 0.00208 0.00232 0.00043 0.00189 -82.84 0.00208 0.00233 0.00043 0.00190 -82.88 0.00208 0.00234 0.00043 0.00190 -82.92 0.00208 0.00235 0.00043 0.00191 -82.96 0.00206 0.00235 0.00043 0.00192 -83. 0.00211 0.00236 0.00043 0.00192 -83.04 0.00214 0.00237 0.00043 0.00193 -83.08 0.00181 0.00238 0.00044 0.00194 -83.12 0.00133 0.00239 0.00044 0.00194 -83.16 0.00121 0.00239 0.00044 0.00195 -83.2 0.00134 0.00240 0.00044 0.00196 -83.24 0.00140 0.00241 0.00044 0.00196 -83.28 0.00110 0.00242 0.00044 0.00197 -83.32 0.00060 0.00243 0.00044 0.00198 -83.36 0.00045 0.00243 0.00044 0.00199 -83.4 0.00053 0.00244 0.00045 0.00199 -83.44 0.00054 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