29Si MAS NMR spectrum of ZSM-5 (Si/Al=51) ##freq 71.5531 ##ppm,spectr,model,Q4(0Al),Q4(0Al),Q4(1Al),Q3(0Al),Q4(1Al) ----- -91.9703,0.0040,0.0023,0.0005,0.0008,0.0003,0.0005,0.0002 -92.1703,0.0037,0.0024,0.0005,0.0008,0.0003,0.0006,0.0003 -92.3701,0.0038,0.0024,0.0005,0.0008,0.0003,0.0006,0.0003 -92.5701,0.0034,0.0025,0.0005,0.0009,0.0003,0.0006,0.0003 -92.7700,0.0034,0.0026,0.0005,0.0009,0.0003,0.0006,0.0003 -92.9700,0.0037,0.0027,0.0005,0.0009,0.0003,0.0007,0.0003 -93.1700,0.0045,0.0028,0.0005,0.0009,0.0003,0.0007,0.0004 -93.3698,0.0041,0.0029,0.0005,0.0009,0.0003,0.0007,0.0004 -93.5698,0.0038,0.0030,0.0005,0.0010,0.0003,0.0007,0.0005 -93.7697,0.0042,0.0032,0.0005,0.0010,0.0004,0.0008,0.0005 -93.9697,0.0048,0.0033,0.0006,0.0010,0.0004,0.0008,0.0006 -94.1696,0.0058,0.0035,0.0006,0.0010,0.0004,0.0008,0.0007 -94.3695,0.0062,0.0037,0.0006,0.0010,0.0004,0.0009,0.0008 -94.5695,0.0064,0.0040,0.0006,0.0011,0.0004,0.0009,0.0010 -94.7693,0.0065,0.0044,0.0006,0.0011,0.0004,0.0010,0.0013 -94.9693,0.0079,0.0049,0.0006,0.0011,0.0004,0.0010,0.0017 -95.1693,0.0083,0.0057,0.0006,0.0012,0.0005,0.0011,0.0024 -95.3692,0.0090,0.0069,0.0006,0.0012,0.0005,0.0011,0.0035 -95.5692,0.0096,0.0084,0.0007,0.0012,0.0005,0.0012,0.0049 -95.7690,0.0110,0.0106,0.0007,0.0013,0.0005,0.0012,0.0069 -95.9690,0.0137,0.0133,0.0007,0.0013,0.0005,0.0013,0.0095 -96.1690,0.0161,0.0165,0.0007,0.0013,0.0005,0.0014,0.0126 -96.3689,0.0204,0.0203,0.0007,0.0014,0.0006,0.0015,0.0162 -96.5688,0.0240,0.0244,0.0007,0.0014,0.0006,0.0015,0.0201 -96.7687,0.0278,0.0283,0.0008,0.0014,0.0006,0.0016,0.0239 -96.9687,0.0319,0.0319,0.0008,0.0015,0.0007,0.0018,0.0272 -97.1687,0.0341,0.0345,0.0008,0.0015,0.0007,0.0019,0.0296 -97.3685,0.0350,0.0358,0.0008,0.0016,0.0007,0.0020,0.0307 -97.5685,0.0351,0.0356,0.0008,0.0016,0.0007,0.0022,0.0302 -97.7684,0.0326,0.0339,0.0008,0.0017,0.0008,0.0024,0.0282 -97.9684,0.0320,0.0312,0.0009,0.0017,0.0008,0.0027,0.0251 -98.1684,0.0312,0.0280,0.0009,0.0018,0.0009,0.0030,0.0214 -98.3682,0.0264,0.0247,0.0009,0.0018,0.0009,0.0035,0.0175 -98.5682,0.0224,0.0216,0.0009,0.0019,0.0010,0.0041,0.0138 -98.7680,0.0208,0.0192,0.0010,0.0019,0.0010,0.0048,0.0105 -98.9680,0.0186,0.0176,0.0010,0.0020,0.0011,0.0058,0.0077 -99.1680,0.0143,0.0169,0.0010,0.0021,0.0011,0.0072,0.0055 -99.3679,0.0120,0.0172,0.0010,0.0022,0.0012,0.0089,0.0039 -99.5679,0.0119,0.0184,0.0011,0.0022,0.0013,0.0111,0.0027 -99.7677,0.0129,0.0207,0.0011,0.0023,0.0014,0.0140,0.0019 -99.9677,0.0176,0.0239,0.0011,0.0024,0.0015,0.0175,0.0014 -100.1677,0.0241,0.0281,0.0012,0.0025,0.0016,0.0219,0.0011 -100.3676,0.0304,0.0334,0.0012,0.0026,0.0017,0.0271,0.0009 -100.5676,0.0394,0.0397,0.0012,0.0027,0.0018,0.0332,0.0007 -100.7674,0.0493,0.0469,0.0013,0.0028,0.0020,0.0403,0.0006 -100.9674,0.0580,0.0551,0.0013,0.0029,0.0022,0.0483,0.0005 -101.1674,0.0704,0.0642,0.0013,0.0030,0.0024,0.0569,0.0005 -101.3672,0.0797,0.0738,0.0014,0.0032,0.0027,0.0661,0.0004 -101.5672,0.0900,0.0838,0.0014,0.0033,0.0031,0.0756,0.0004 -101.7671,0.0973,0.0939,0.0015,0.0034,0.0037,0.0850,0.0004 -101.9671,0.1047,0.1038,0.0015,0.0036,0.0044,0.0940,0.0003 -102.1671,0.1112,0.1130,0.0016,0.0038,0.0054,0.1020,0.0003 -102.3669,0.1187,0.1212,0.0016,0.0039,0.0068,0.1086,0.0003 -102.5669,0.1271,0.1280,0.0017,0.0041,0.0086,0.1133,0.0003 -102.7668,0.1305,0.1332,0.0017,0.0043,0.0111,0.1158,0.0002 -102.9667,0.1349,0.1367,0.0018,0.0045,0.0142,0.1159,0.0002 -103.1667,0.1367,0.1387,0.0019,0.0048,0.0183,0.1136,0.0002 -103.3666,0.1381,0.1394,0.0019,0.0050,0.0233,0.1089,0.0002 -103.5666,0.1392,0.1393,0.0020,0.0053,0.0293,0.1025,0.0002 -103.7664,0.1394,0.1388,0.0021,0.0056,0.0365,0.0945,0.0002 -103.9664,0.1398,0.1385,0.0021,0.0059,0.0446,0.0856,0.0002 -104.1664,0.1409,0.1386,0.0022,0.0063,0.0537,0.0762,0.0002 -104.3663,0.1406,0.1393,0.0023,0.0067,0.0634,0.0668,0.0001 -104.5663,0.1425,0.1406,0.0024,0.0071,0.0735,0.0575,0.0001 -104.7661,0.1460,0.1424,0.0025,0.0075,0.0834,0.0488,0.0001 -104.9661,0.1485,0.1442,0.0026,0.0081,0.0926,0.0408,0.0001 -105.1661,0.1490,0.1457,0.0027,0.0086,0.1006,0.0337,0.0001 -105.3659,0.1472,0.1463,0.0028,0.0092,0.1066,0.0275,0.0001 -105.5659,0.1425,0.1455,0.0030,0.0099,0.1103,0.0222,0.0001 -105.7658,0.1351,0.1428,0.0031,0.0107,0.1111,0.0178,0.0001 -105.9658,0.1289,0.1382,0.0033,0.0115,0.1091,0.0142,0.0001 -106.1658,0.1244,0.1318,0.0034,0.0125,0.1045,0.0113,0.0001 -106.3656,0.1202,0.1240,0.0036,0.0137,0.0976,0.0090,0.0001 -106.5656,0.1144,0.1152,0.0038,0.0151,0.0890,0.0073,0.0001 -106.7655,0.1111,0.1062,0.0040,0.0167,0.0795,0.0059,0.0001 -106.9655,0.1043,0.0976,0.0043,0.0189,0.0695,0.0049,0.0001 -107.1654,0.0992,0.0901,0.0046,0.0218,0.0595,0.0041,0.0001 -107.3653,0.0959,0.0845,0.0050,0.0259,0.0500,0.0035,0.0001 -107.5653,0.0951,0.0816,0.0054,0.0318,0.0413,0.0031,0.0001 -107.7651,0.0936,0.0825,0.0060,0.0403,0.0335,0.0027,0.0001 -107.9651,0.0958,0.0886,0.0067,0.0526,0.0268,0.0024,0.0001 -108.1651,0.0995,0.1013,0.0076,0.0703,0.0211,0.0022,0.0001 -108.3650,0.1098,0.1225,0.0087,0.0951,0.0165,0.0020,0.0001 -108.5650,0.1317,0.1541,0.0102,0.1291,0.0129,0.0019,0.0001 -108.7650,0.1574,0.1979,0.0122,0.1739,0.0100,0.0018,0.0001 -108.9648,0.2224,0.2553,0.0147,0.2311,0.0078,0.0017,0.0001 -109.1648,0.2936,0.3270,0.0179,0.3013,0.0062,0.0016,0.0001 -109.3647,0.4297,0.4122,0.0220,0.3837,0.0050,0.0015,0.0000 -109.5646,0.5214,0.5089,0.0273,0.4761,0.0041,0.0014,0.0000 -109.7646,0.6598,0.6131,0.0339,0.5744,0.0034,0.0013,0.0000 -109.9645,0.7528,0.7189,0.0420,0.6727,0.0029,0.0012,0.0000 -110.1645,0.8330,0.8191,0.0520,0.7633,0.0026,0.0012,0.0000 -110.3643,0.9230,0.9052,0.0641,0.8376,0.0023,0.0011,0.0000 -110.5643,0.9788,0.9687,0.0786,0.8870,0.0021,0.0011,0.0000 -110.7643,1.0000,1.0032,0.0956,0.9046,0.0019,0.0010,0.0000 -110.9642,0.9829,1.0060,0.1154,0.8878,0.0018,0.0010,0.0000 -111.1642,0.9468,0.9798,0.1380,0.8392,0.0016,0.0009,0.0000 -111.3640,0.9021,0.9313,0.1634,0.7655,0.0015,0.0009,0.0000 -111.5640,0.8554,0.8689,0.1915,0.6751,0.0014,0.0008,0.0000 -111.7640,0.8016,0.8011,0.2220,0.5770,0.0013,0.0008,0.0000 -111.9638,0.7541,0.7352,0.2546,0.4786,0.0012,0.0008,0.0000 -112.1638,0.7013,0.6766,0.2887,0.3859,0.0012,0.0007,0.0000 -112.3637,0.6455,0.6288,0.3237,0.3032,0.0011,0.0007,0.0000 -112.5637,0.6102,0.5932,0.3587,0.2327,0.0010,0.0007,0.0000 -112.7637,0.5790,0.5698,0.3929,0.1752,0.0010,0.0007,0.0000 -112.9635,0.5585,0.5568,0.4252,0.1301,0.0009,0.0006,0.0000 -113.1635,0.5451,0.5519,0.4545,0.0959,0.0009,0.0006,0.0000 -113.3634,0.5388,0.5522,0.4799,0.0709,0.0008,0.0006,0.0000 -113.5634,0.5390,0.5547,0.5003,0.0530,0.0008,0.0006,0.0000 -113.7633,0.5416,0.5568,0.5149,0.0406,0.0008,0.0005,0.0000 -113.9632,0.5443,0.5562,0.5230,0.0320,0.0007,0.0005,0.0000 -114.1632,0.5453,0.5516,0.5243,0.0261,0.0007,0.0005,0.0000 -114.3630,0.5379,0.5418,0.5187,0.0219,0.0007,0.0005,0.0000 -114.5630,0.5278,0.5265,0.5064,0.0190,0.0006,0.0005,0.0000 -114.7630,0.5040,0.5060,0.4881,0.0168,0.0006,0.0005,0.0000 -114.9629,0.4751,0.4806,0.4645,0.0151,0.0006,0.0004,0.0000 -115.1629,0.4448,0.4512,0.4365,0.0137,0.0006,0.0004,0.0000 -115.3627,0.4157,0.4187,0.4052,0.0126,0.0005,0.0004,0.0000 -115.5627,0.3873,0.3841,0.3716,0.0116,0.0005,0.0004,0.0000 -115.7627,0.3590,0.3484,0.3368,0.0107,0.0005,0.0004,0.0000 -115.9626,0.3279,0.3125,0.3017,0.0099,0.0005,0.0004,0.0000 -116.1625,0.2933,0.2773,0.2672,0.0092,0.0005,0.0004,0.0000 -116.3624,0.2624,0.2434,0.2339,0.0086,0.0004,0.0004,0.0000 -116.5624,0.2277,0.2114,0.2026,0.0081,0.0004,0.0003,0.0000 -116.7624,0.1973,0.1819,0.1735,0.0076,0.0004,0.0003,0.0000 -116.9622,0.1610,0.1550,0.1471,0.0071,0.0004,0.0003,0.0000 -117.1622,0.1264,0.1309,0.1235,0.0067,0.0004,0.0003,0.0000 -117.3621,0.0865,0.1097,0.1027,0.0063,0.0004,0.0003,0.0000 -117.5621,0.0675,0.0913,0.0846,0.0059,0.0004,0.0003,0.0000 -117.7621,0.0472,0.0755,0.0692,0.0056,0.0003,0.0003,0.0000 -117.9619,0.0362,0.0622,0.0563,0.0053,0.0003,0.0003,0.0000 -118.1619,0.0239,0.0512,0.0455,0.0050,0.0003,0.0003,0.0000 -118.3617,0.0149,0.0421,0.0367,0.0048,0.0003,0.0003,0.0000 -118.5617,0.0101,0.0347,0.0296,0.0046,0.0003,0.0003,0.0000 -118.7617,0.0067,0.0287,0.0238,0.0043,0.0003,0.0003,0.0000 -118.9616,0.0053,0.0240,0.0193,0.0041,0.0003,0.0003,0.0000 -119.1616,0.0053,0.0203,0.0158,0.0039,0.0003,0.0002,0.0000 -119.3614,0.0054,0.0173,0.0130,0.0038,0.0003,0.0002,0.0000 -119.5614,0.0055,0.0150,0.0109,0.0036,0.0003,0.0002,0.0000 -119.7614,0.0055,0.0132,0.0092,0.0034,0.0003,0.0002,0.0000 -119.9613,0.0060,0.0117,0.0080,0.0033,0.0003,0.0002,0.0000 -120.1613,0.0064,0.0106,0.0070,0.0032,0.0002,0.0002,0.0000 -120.3611,0.0064,0.0097,0.0062,0.0030,0.0002,0.0002,0.0000 -120.5611,0.0065,0.0090,0.0056,0.0029,0.0002,0.0002,0.0000 -120.7611,0.0055,0.0084,0.0051,0.0028,0.0002,0.0002,0.0000 -120.9609,0.0055,0.0078,0.0047,0.0027,0.0002,0.0002,0.0000 -121.1609,0.0059,0.0074,0.0044,0.0026,0.0002,0.0002,0.0000 -121.3608,0.0007,0.0070,0.0041,0.0025,0.0002,0.0002,0.0000 -121.5608,-0.0001,0.0067,0.0039,0.0024,0.0002,0.0002,0.0000 -121.7608,0.0018,0.0064,0.0037,0.0023,0.0002,0.0002,0.0000 -121.9606,0.0018,0.0061,0.0035,0.0022,0.0002,0.0002,0.0000 -122.1606,0.0028,0.0059,0.0033,0.0022,0.0002,0.0002,0.0000 -122.3605,0.0032,0.0056,0.0032,0.0021,0.0002,0.0002,0.0000 -122.5604,0.0032,0.0054,0.0030,0.0020,0.0002,0.0002,0.0000