Fyfe et al. Chem. Lett., 12, 1547-1550 (1983) Figure 1B ##freq 1 ##col_ ppm Spectrum Model Si4 Si2 Si3 Si1 ----- -89.94 -0.02969 0.00095 0.00014 0.00031 0.00014 0.00035 -89.96 -0.0297 0.00095 0.00014 0.00031 0.00014 0.00035 -89.98 -0.02972 0.00095 0.00014 0.00031 0.00014 0.00035 -90. -0.02972 0.00096 0.00014 0.00031 0.00014 0.00035 -90.02 -0.02963 0.00096 0.00014 0.00031 0.00014 0.00035 -90.04 -0.02966 0.00096 0.00014 0.00031 0.00014 0.00035 -90.06 -0.03001 0.00096 0.00014 0.00031 0.00014 0.00035 -90.08 -0.02978 0.00096 0.00014 0.00031 0.00014 0.00035 -90.1 -0.02806 0.00096 0.00014 0.00031 0.00014 0.00035 -90.12 -0.02630 0.00097 0.00014 0.00031 0.00014 0.00035 -90.14 -0.02601 0.00097 0.00014 0.00032 0.00014 0.00036 -90.16 -0.02636 0.00097 0.00014 0.00032 0.00014 0.00036 -90.18 -0.02640 0.00097 0.00014 0.00032 0.00014 0.00036 -90.2 -0.02632 0.00097 0.00014 0.00032 0.00014 0.00036 -90.22 -0.02635 0.00097 0.00014 0.00032 0.00014 0.00036 -90.24 -0.02628 0.00098 0.00014 0.00032 0.00014 0.00036 -90.26 -0.02618 0.00098 0.00014 0.00032 0.00014 0.00036 -90.28 -0.02665 0.00098 0.00014 0.00032 0.00014 0.00036 -90.3 -0.02836 0.00098 0.00014 0.00032 0.00014 0.00036 -90.32 -0.03184 0.00098 0.00014 0.00032 0.00014 0.00036 -90.34 -0.03565 0.00098 0.00015 0.00032 0.00014 0.00036 -90.36 -0.03685 0.00099 0.00015 0.00032 0.00014 0.00036 -90.38 -0.03640 0.00099 0.00015 0.00032 0.00014 0.00036 -90.4 -0.03748 0.00099 0.00015 0.00032 0.00014 0.00036 -90.42 -0.03959 0.00099 0.00015 0.00032 0.00014 0.00036 -90.44 -0.04058 0.00099 0.00015 0.00032 0.00014 0.00037 -90.46 -0.03988 0.00099 0.00015 0.00032 0.00014 0.00037 -90.48 -0.03784 0.00100 0.00015 0.00032 0.00014 0.00037 -90.5 -0.03642 0.00100 0.00015 0.00032 0.00014 0.00037 -90.52 -0.03678 0.00100 0.00015 0.00033 0.00014 0.00037 -90.54 -0.03611 0.00100 0.00015 0.00033 0.00014 0.00037 -90.56 -0.03259 0.00100 0.00015 0.00033 0.00014 0.00037 -90.58 -0.02880 0.00100 0.00015 0.00033 0.00014 0.00037 -90.6 -0.02676 0.00101 0.00015 0.00033 0.00014 0.00037 -90.62 -0.02633 0.00101 0.00015 0.00033 0.00015 0.00037 -90.64 -0.02655 0.00101 0.00015 0.00033 0.00015 0.00037 -90.66 -0.02567 0.00101 0.00015 0.00033 0.00015 0.00037 -90.68 -0.02367 0.00101 0.00015 0.00033 0.00015 0.00037 -90.7 -0.02235 0.00101 0.00015 0.00033 0.00015 0.00037 -90.72 -0.02257 0.00102 0.00015 0.00033 0.00015 0.00037 -90.74 -0.02428 0.00102 0.00015 0.00033 0.00015 0.00038 -90.76 -0.02613 0.00102 0.00015 0.00033 0.00015 0.00038 -90.78 -0.02636 0.00102 0.00015 0.00033 0.00015 0.00038 -90.8 -0.02626 0.00102 0.00015 0.00033 0.00015 0.00038 -90.82 -0.02783 0.00103 0.00015 0.00033 0.00015 0.00038 -90.84 -0.02971 0.00103 0.00015 0.00033 0.00015 0.00038 -90.86 -0.03006 0.00103 0.00015 0.00033 0.00015 0.00038 -90.88 -0.02967 0.00103 0.00015 0.00034 0.00015 0.00038 -90.9 -0.02959 0.00103 0.00015 0.00034 0.00015 0.00038 -90.92 -0.02974 0.00103 0.00015 0.00034 0.00015 0.00038 -90.94 -0.02982 0.00104 0.00015 0.00034 0.00015 0.00038 -90.96 -0.02958 0.00104 0.00015 0.00034 0.00015 0.00038 -90.98 -0.02935 0.00104 0.00015 0.00034 0.00015 0.00038 -91. -0.03033 0.00104 0.00015 0.00034 0.00015 0.00038 -91.02 -0.03235 0.00104 0.00015 0.00034 0.00015 0.00039 -91.04 -0.03342 0.00105 0.00015 0.00034 0.00015 0.00039 -91.06 -0.03321 0.00105 0.00015 0.00034 0.00015 0.00039 -91.08 -0.03298 0.00105 0.00015 0.00034 0.00015 0.00039 -91.1 -0.03305 0.00105 0.00015 0.00034 0.00015 0.00039 -91.12 -0.03309 0.00105 0.00015 0.00034 0.00015 0.00039 -91.14 -0.03307 0.00106 0.00016 0.00034 0.00015 0.00039 -91.16 -0.03314 0.00106 0.00016 0.00034 0.00015 0.00039 -91.18 -0.03309 0.00106 0.00016 0.00034 0.00015 0.00039 -91.2 -0.03281 0.00106 0.00016 0.00034 0.00015 0.00039 -91.22 -0.03312 0.00106 0.00016 0.00035 0.00015 0.00039 -91.24 -0.03471 0.00106 0.00016 0.00035 0.00015 0.00039 -91.26 -0.03673 0.00107 0.00016 0.00035 0.00015 0.00039 -91.28 -0.03847 0.00107 0.00016 0.00035 0.00015 0.00040 -91.3 -0.04034 0.00107 0.00016 0.00035 0.00015 0.00040 -91.32 -0.04235 0.00107 0.00016 0.00035 0.00015 0.00040 -91.34 -0.04338 0.00107 0.00016 0.00035 0.00016 0.00040 -91.36 -0.04326 0.00108 0.00016 0.00035 0.00016 0.00040 -91.38 -0.04333 0.00108 0.00016 0.00035 0.00016 0.00040 -91.4 -0.04352 0.00108 0.00016 0.00035 0.00016 0.00040 -91.42 -0.04222 0.00108 0.00016 0.00035 0.00016 0.00040 -91.44 -0.04018 0.00108 0.00016 0.00035 0.00016 0.00040 -91.46 -0.03990 0.00109 0.00016 0.00035 0.00016 0.00040 -91.48 -0.04010 0.00109 0.00016 0.00035 0.00016 0.00040 -91.5 -0.03758 0.00109 0.00016 0.00035 0.00016 0.00040 -91.52 -0.03352 0.00109 0.00016 0.00035 0.00016 0.00040 -91.54 -0.03084 0.00109 0.00016 0.00035 0.00016 0.00041 -91.56 -0.02972 0.00110 0.00016 0.00036 0.00016 0.00041 -91.58 -0.02946 0.00110 0.00016 0.00036 0.00016 0.00041 -91.6 -0.02974 0.00110 0.00016 0.00036 0.00016 0.00041 -91.62 -0.03011 0.00110 0.00016 0.00036 0.00016 0.00041 -91.64 -0.02945 0.00110 0.00016 0.00036 0.00016 0.00041 -91.66 -0.02748 0.00111 0.00016 0.00036 0.00016 0.00041 -91.68 -0.02611 0.00111 0.00016 0.00036 0.00016 0.00041 -91.7 -0.02619 0.00111 0.00016 0.00036 0.00016 0.00041 -91.72 -0.02626 0.00111 0.00016 0.00036 0.00016 0.00041 -91.74 -0.02605 0.00111 0.00016 0.00036 0.00016 0.00041 -91.76 -0.02708 0.00112 0.00016 0.00036 0.00016 0.00041 -91.78 -0.02910 0.00112 0.00016 0.00036 0.00016 0.00042 -91.8 -0.03007 0.00112 0.00016 0.00036 0.00016 0.00042 -91.82 -0.02981 0.00112 0.00016 0.00036 0.00016 0.00042 -91.84 -0.02960 0.00112 0.00016 0.00036 0.00016 0.00042 -91.86 -0.02968 0.00113 0.00017 0.00037 0.00016 0.00042 -91.88 -0.02975 0.00113 0.00017 0.00037 0.00016 0.00042 -91.9 -0.02971 0.00113 0.00017 0.00037 0.00016 0.00042 -91.92 -0.02961 0.00113 0.00017 0.00037 0.00016 0.00042 -91.94 -0.02971 0.00114 0.00017 0.00037 0.00016 0.00042 -91.96 -0.03006 0.00114 0.00017 0.00037 0.00016 0.00042 -91.98 -0.02955 0.00114 0.00017 0.00037 0.00016 0.00042 -92. -0.02765 0.00114 0.00017 0.00037 0.00017 0.00042 -92.02 -0.02612 0.00114 0.00017 0.00037 0.00017 0.00043 -92.04 -0.02607 0.00115 0.00017 0.00037 0.00017 0.00043 -92.06 -0.02640 0.00115 0.00017 0.00037 0.00017 0.00043 -92.08 -0.02639 0.00115 0.00017 0.00037 0.00017 0.00043 -92.1 -0.02631 0.00115 0.00017 0.00037 0.00017 0.00043 -92.12 -0.02632 0.00115 0.00017 0.00037 0.00017 0.00043 -92.14 -0.02632 0.00116 0.00017 0.00037 0.00017 0.00043 -92.16 -0.02631 0.00116 0.00017 0.00037 0.00017 0.00043 -92.18 -0.02639 0.00116 0.00017 0.00038 0.00017 0.00043 -92.2 -0.02639 0.00116 0.00017 0.00038 0.00017 0.00043 -92.22 -0.02606 0.00117 0.00017 0.00038 0.00017 0.00043 -92.24 -0.02619 0.00117 0.00017 0.00038 0.00017 0.00043 -92.26 -0.02775 0.00117 0.00017 0.00038 0.00017 0.00044 -92.28 -0.02964 0.00117 0.00017 0.00038 0.00017 0.00044 -92.3 -0.03029 0.00117 0.00017 0.00038 0.00017 0.00044 -92.32 -0.02964 0.00118 0.00017 0.00038 0.00017 0.00044 -92.34 -0.02806 0.00118 0.00017 0.00038 0.00017 0.00044 -92.36 -0.02597 0.00118 0.00017 0.00038 0.00017 0.00044 -92.38 -0.02392 0.00118 0.00017 0.00038 0.00017 0.00044 -92.4 -0.02280 0.00119 0.00017 0.00038 0.00017 0.00044 -92.42 -0.02284 0.00119 0.00017 0.00038 0.00017 0.00044 -92.44 -0.02292 0.00119 0.00017 0.00038 0.00017 0.00044 -92.46 -0.02275 0.00119 0.00017 0.00039 0.00017 0.00044 -92.48 -0.02347 0.00119 0.00017 0.00039 0.00017 0.00045 -92.5 -0.02535 0.00120 0.00018 0.00039 0.00017 0.00045 -92.52 -0.02767 0.00120 0.00018 0.00039 0.00017 0.00045 -92.54 -0.02944 0.00120 0.00018 0.00039 0.00017 0.00045 -92.56 -0.02971 0.00120 0.00018 0.00039 0.00017 0.00045 -92.58 -0.02956 0.00121 0.00018 0.00039 0.00017 0.00045 -92.6 -0.03098 0.00121 0.00018 0.00039 0.00018 0.00045 -92.62 -0.03293 0.00121 0.00018 0.00039 0.00018 0.00045 -92.64 -0.03344 0.00121 0.00018 0.00039 0.00018 0.00045 -92.66 -0.03308 0.00122 0.00018 0.00039 0.00018 0.00045 -92.68 -0.03299 0.00122 0.00018 0.00039 0.00018 0.00045 -92.7 -0.03308 0.00122 0.00018 0.00039 0.00018 0.00046 -92.72 -0.03309 0.00122 0.00018 0.00039 0.00018 0.00046 -92.74 -0.03308 0.00122 0.00018 0.00040 0.00018 0.00046 -92.76 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0.00049 -93.48 -0.02633 0.00132 0.00019 0.00042 0.00019 0.00049 -93.5 -0.02633 0.00132 0.00019 0.00042 0.00019 0.00050 -93.52 -0.02634 0.00132 0.00019 0.00042 0.00019 0.00050 -93.54 -0.02632 0.00132 0.00019 0.00043 0.00019 0.00050 -93.56 -0.02631 0.00133 0.00019 0.00043 0.00019 0.00050 -93.58 -0.02638 0.00133 0.00019 0.00043 0.00019 0.00050 -93.6 -0.02641 0.00133 0.00019 0.00043 0.00019 0.00050 -93.62 -0.02611 0.00134 0.00019 0.00043 0.00019 0.00050 -93.64 -0.02608 0.00134 0.00019 0.00043 0.00019 0.00050 -93.66 -0.02747 0.00134 0.00020 0.00043 0.00020 0.00050 -93.68 -0.02942 0.00134 0.00020 0.00043 0.00020 0.00051 -93.7 -0.03014 0.00135 0.00020 0.00043 0.00020 0.00051 -93.72 -0.02976 0.00135 0.00020 0.00043 0.00020 0.00051 -93.74 -0.02928 0.00135 0.00020 0.00043 0.00020 0.00051 -93.76 -0.02971 0.00135 0.00020 0.00043 0.00020 0.00051 -93.78 -0.03154 0.00136 0.00020 0.00044 0.00020 0.00051 -93.8 -0.03319 0.00136 0.00020 0.00044 0.00020 0.00051 -93.82 -0.03336 0.00136 0.00020 0.00044 0.00020 0.00051 -93.84 -0.03303 0.00137 0.00020 0.00044 0.00020 0.00051 -93.86 -0.03303 0.00137 0.00020 0.00044 0.00020 0.00052 -93.88 -0.03306 0.00137 0.00020 0.00044 0.00020 0.00052 -93.9 -0.03300 0.00137 0.00020 0.00044 0.00020 0.00052 -93.92 -0.03323 0.00138 0.00020 0.00044 0.00020 0.00052 -93.94 -0.03340 0.00138 0.00020 0.00044 0.00020 0.00052 -93.96 -0.03224 0.00138 0.00020 0.00044 0.00020 0.00052 -93.98 -0.03023 0.00138 0.00020 0.00044 0.00020 0.00052 -94. -0.02938 0.00139 0.00020 0.00044 0.00020 0.00052 -94.02 -0.02964 0.00139 0.00020 0.00045 0.00020 0.00053 -94.04 -0.02965 0.00139 0.00020 0.00045 0.00020 0.00053 -94.06 -0.02963 0.00140 0.00020 0.00045 0.00020 0.00053 -94.08 -0.03032 0.00140 0.00020 0.00045 0.00020 0.00053 -94.1 -0.02983 0.00140 0.00020 0.00045 0.00020 0.00053 -94.12 -0.02629 0.00141 0.00020 0.00045 0.00021 0.00053 -94.14 -0.02287 0.00141 0.00020 0.00045 0.00021 0.00053 -94.16 -0.02260 0.00141 0.00020 0.00045 0.00021 0.00053 -94.18 -0.02289 0.00141 0.00021 0.00045 0.00021 0.00053 -94.2 -0.02132 0.00142 0.00021 0.00045 0.00021 0.00054 -94.22 -0.01902 0.00142 0.00021 0.00045 0.00021 0.00054 -94.24 -0.01715 0.00142 0.00021 0.00046 0.00021 0.00054 -94.26 -0.01578 0.00143 0.00021 0.00046 0.00021 0.00054 -94.28 -0.01547 0.00143 0.00021 0.00046 0.00021 0.00054 -94.3 -0.01750 0.00143 0.00021 0.00046 0.00021 0.00054 -94.32 -0.02137 0.00143 0.00021 0.00046 0.00021 0.00054 -94.34 -0.02452 0.00144 0.00021 0.00046 0.00021 0.00054 -94.36 -0.02608 0.00144 0.00021 0.00046 0.00021 0.00055 -94.38 -0.02657 0.00144 0.00021 0.00046 0.00021 0.00055 -94.4 -0.02642 0.00145 0.00021 0.00046 0.00021 0.00055 -94.42 -0.02600 0.00145 0.00021 0.00046 0.00021 0.00055 -94.44 -0.02620 0.00145 0.00021 0.00046 0.00021 0.00055 -94.46 -0.02786 0.00146 0.00021 0.00047 0.00021 0.00055 -94.48 -0.02968 0.00146 0.00021 0.00047 0.00021 0.00055 -94.5 -0.03012 0.00146 0.00021 0.00047 0.00021 0.00055 -94.52 -0.02965 0.00146 0.00021 0.00047 0.00021 0.00056 -94.54 -0.02926 0.00147 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