| Note: Toggle plots by clicking on the legend |
Peak |
T site |
Q-type |
Chemical Shift |
Relative |
Peak Width |
Peak Shape |
Assigment |
(topological) | (ppm) |
Peak Area |
(ppm) |
(x)L (1-x)G |
|
P2/P1 | T2/T1 | Q4(4Al) | -32.36 | 2.00 | 5.80 | 0.490 |
P3 | T3 | Q4(4Al) | -31.96 | 1.00 | 5.80 | 0.490 |
P1/P2 | T1/T2 | Q4(4Al) | -26.71 | 2.00 | 5.80 | 0.490 |
| Authors: | Barrie, P.J., Smith, M.E., Klinowski, J. | ||||
| Title: | Double-rotation 27Al NMR studies of the aluminophosphate molecular sieve AlPO4-11 | ||||
| Reference: | Chem. Phys. Lett., 180, 6-12 (1991 DOI: 10.1016/0009-2614(91)87107-M) |
||||
| Figure: | Figure 3a | ||||
| Authors: | Barrie, P.J., Smith, M.E., Klinowski, J. | |
| Title: | Double-rotation 27Al NMR studies of the aluminophosphate molecular sieve AlPO4-11 | |
| Reference: | Chem. Phys. Lett., 180, 6-12 (1991) DOI: 10.1016/0009-2614(91)87107-M |
| Authors: | Pluth, J.J., Smith, J.V. and Richardson Jr., J.W. | |
| Title: | Crystal structure of the as-synthesized precursor (MnAl9)P10O40·C6H16N to molecular sieve MnAPO-11 | |
| Reference: | J. Phys. Chem., 92, 2734-2738 (1988) DOI: 10.1021/j100321a008 |
| To reference this collection of solid-state NMR spectra, we suggest: | ||
| Authors: | Brouwer, D.H. and White, A.L. | |
| Title: | A comprehensive collection of solid-state 31P NMR spectra of aluminophosphate zeolites. | |
| Reference: | Microporous Mesoporous Mat., 337, 111934 (2022) DOI: 10.1016/j.micromeso.2022.111934 | |
| Obs. freq. | 162 MHz (Field = 9.4 Tesla) | |
| Pulse sequence | single pulse | |
| MAS frequency | 12 kHz | |
| Spectrum | Digitized and processed by Brouwer Lab, Redeemer University | |
| Data processing | Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook |
|
| Comment | Partial peak assignments based on relative peak areas |
| [Al - P - O]-AEL |
| Download digitized spectrum in JCAMP-DX format (This file includes also the data listed on this page) | Download all lines from the above plot in .csv format (This file contains only the plotted data) |