Note: Toggle plots by clicking on the legend |
Peak |
T site |
Q-type |
Chemical Shift |
Relative |
Peak Width |
Peak Shape |
Assigment |
(topological) | (ppm) |
Peak Area |
(ppm) |
(x)L (1-x)G |
|
Si2 | T2 | Q4(0Al) | -114.72 | 1.000 | 1.76 | 0.726 |
Si1 | T1 | Q4(0Al) | -111.77 | 4.000 | 0.58 | 0.726 |
Authors: | Villaescusa, L.A., Barrett, P.A., Camblor, M.A. | ||||
Title: | Calcination of Octadecasil: Fluoride Removal and Symmetry of the Pure SiO2 Host | ||||
Reference: | Chem. Mater., 10, 3966-3973 (1998) DOI: 10.1021/cm9804113 |
||||
Figure: | Figure 4 | ||||
Authors: | Villaescusa, L.A., Barrett, P.A., Camblor, M.A. | |
Title: | Calcination of Octadecasil: Fluoride Removal and Symmetry of the Pure SiO2 Host | |
Reference: | Chem. Mater., 10, 3966-3973 (1998) DOI: 10.1021/cm9804113 | |
Method: | relative intensities |
Authors: | Villaescusa, L.A., Barrett, P.A., Camblor, M.A. | |
Title: | Calcination of Octadecasil: Fluoride Removal and Symmetry of the Pure SiO2 Host | |
Reference: | Chem. Mater., 10, 3966-3973 (1998) DOI: 10.1021/cm9804113 |
To reference this collection of solid-state NMR spectra, we suggest: | ||
Authors: | Brouwer, D.H., Brouwer, C.C., Mesa, S., Semelhago, C.A., Steckley, E.E., Sun, M.P.Y., Mikolajewski, J.G., and Baerlocher, Ch. | |
Title: | Solid-state 29Si NMR spectra of pure silica zeolites for the International Zeolite Association Database of Zeolite Structures | |
Reference: | Microporous Mesoporous Mat., 297, 110000 (2020) DOI: 10.1016/j.micromeso.2020.110000 |
Obs. freq. | 79.459 MHz (Field = 9.4 Tesla) | |
Pulse sequence | single pulse | |
MAS frequency | 5.5 kHz | |
Spectrum | Digitized and processed by Brouwer Lab, Redeemer University | |
Data processing | Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook |
[Si - O]-AST |
Download digitized spectrum in JCAMP-DX format (This file includes also the data listed on this page) | Download all lines from the above plot in .csv format (This file contains only the plotted data) |