| Note: Toggle plots by clicking on the legend |
Peak |
T site |
Q-type |
Chemical Shift |
Relative |
Peak Width |
Peak Shape |
Assigment |
(topological) | (ppm) |
Peak Area |
(ppm) |
(x)L (1-x)G |
|
P1 | T1 | Q4(4Al) | -25.81 | 1.000 | 3.08 | 0.118 |
P2 | T1 | Q4(4Al) | -18.07 | 1.000 | 2.64 | 0.118 |
| Authors: | Schreyeck, L., Stumbe, J., Caullet, P., Mougenel, J.C., Marler, B. | ||||
| Title: | The diaza-polyoxa-macrocycle 'Kryptofix222' as a new template for the synthesis of LTA-type AlPO4: Co-templating role of F- and/or (CH3)4N+ ions | ||||
| Reference: | Microporous Mesoporous Mater., 22, 87-106 (1998) DOI: 10.1016/S1387-1811(98)00082-1 |
||||
| Figure: | Figure 10a | ||||
| Authors: | Schreyeck, L., Stumbe, J., Caullet, P., Mougenel, J.C., Marler, B. | ||||
| Title: | The diaza-polyoxa-macrocycle 'Kryptofix222' as a new template for the synthesis of LTA-type AlPO4: Co-templating role of F- and/or (CH3)4N+ ions | ||||
| Reference: | Microporous Mesoporous Mater., 22, 87-106 (1998) DOI: 10.1016/S1387-1811(98)00082-1 | ||||
| Method: | 19F/31P cross polarization | ||||
| Figure: | Figure 10b | ||||
| Authors: | Schreyeck, L., Stumbe, J., Caullet, P., Mougenel, J.C., Marler, B. | |
| Title: | The diaza-polyoxa-macrocycle 'Kryptofix222' as a new template for the synthesis of LTA-type AlPO4: Co-templating role of F- and/or (CH3)4N+ ions | |
| Reference: | Microporous Mesoporous Mater., 22, 87-106 (1998) DOI: 10.1016/S1387-1811(98)00082-1 |
| To reference this collection of solid-state NMR spectra, we suggest: | ||
| Authors: | Brouwer, D.H. and White, A.L. | |
| Title: | A comprehensive collection of solid-state 31P NMR spectra of aluminophosphate zeolites. | |
| Reference: | Microporous Mesoporous Mat., 337, 111934 (2022) DOI: 10.1016/j.micromeso.2022.111934 | |
| Obs. freq. | 121.51 MHz (Field = 7 Tesla) | |
| Pulse sequence | single pulse | |
| MAS frequency | 8 kHz | |
| Spectrum | Digitized and processed by Brouwer Lab, Redeemer University | |
| Data processing | Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook |
|
| Comment | Peak assignments are based on the relative peak areas observed in a 19F/31P cross polarization experiment and the relative 19F/31P dipolar coupling constants calculated from the crystal structure |
| [Al - P - O]-LTA |
| Download digitized spectrum in JCAMP-DX format (This file includes also the data listed on this page) | Download all lines from the above plot in .csv format (This file contains only the plotted data) |