Database of Zeolite Structures
 
Framework Type MSE
29Si MAS NMR spectrum of Al-MCM-68 with Si/Al = 12.2 (NMR)


Note: Toggle plots by clicking on the legend


Peak
Q-type
Chemical Shift
Relative
Peak Width
Peak Shape
Label
(ppm)
Peak Area
(ppm)
(x)L (1-x)G
A
Q4(0Al)
-113.30
47.44
3.54
0.000
B
Q4(0Al)
-109.95
20.68
4.53
0.000
C
Q4(1Al)
-106.65
31.88
9.71
0.000



References
Spectrum

  Authors: Inagaki, S., Tsuboi, Y., Nishita, Y., Syahylah, T., Wakihara, T. and Kubota, Y.
  Title: Rapid Synthesis of an Aluminum-Rich MSE-Type Zeolite by the Hydrothermal Conversion of an FAU-Type Zeolite
  Reference: Chem. Eur. J., 19, 7780-7786 (2013)
  Figure: Figure S6B  
Spectrum information

  Obs. freq. 119.2 MHz (Field = 14.1 Tesla)
  Pulse sequence single pulse
  MAS frequency 10 kHz
  Spectrum
  Data processing Spectrum digitized with WebPlotDigitizer and deconvoluted with dmfit: D. Massiot et al., Magn. Reson. Chem., 40, 70-76 (2002)
 
  Si/Al ratio12.6 (derived from the simulation above)

Chemical Formula

  [Al8.5Si103.5O224]-MSE

Downloads

  Download digitized spectrum in JCAMP-DX format
(This file includes also the data listed on this page)
  Download all lines from the above plot in .csv format
(This file contains only the plotted data)