Database of Zeolite Structures
 
Framework Type RTE
29Si CP MAS NMR spectrum of as-made pure silica RUB-3


Note: Toggle plots by clicking on the legend


Peak
Q-type
Chemical Shift
Relative
Peak Width
Peak Shape
Label
(ppm)
Peak Area
(ppm)
(x)L (1-x)G
A
Q4(0Al)
-115.82
1.00
0.60
0.744
B
Q4(0Al)
-113.14
1.00
0.56
0.744
C
Q4(0Al)
-112.57
1.00
0.56
0.744



References
Spectrum

  Authors: Marler, B., Grünewald-Lüke, A. and Gies, H.
  Title: Decasils, a new order-disorder family of microporous silicas
  Reference: Zeolites, 15, 388-399 (1995)
  Figure: Figure 7  

Crystal Structure

  Authors: Marler, B., Grünewald-Lüke, A. and Gies, H.
  Title: Structure refinement of the as-synthesized and the calcined form of zeolite RUB-3 (RTE)
  Reference: Microporous Mesoporous Mat., 26, 49-59 (1998)
Spectrum information

  Obs. freq. 59.6 MHz (Field = 7 Tesla)
  Pulse sequence cross polarization
  Spectrum Digitized and processed by Brouwer Lab, Redeemer University
  Data processing Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook
 

Chemical Formula

  |(ABH)2 | [Si24O48]-RTE
ABH = C7H13N = exo-2-aminobicyclo[2.2.1.]heptane
= bicyclo[2.2.1]heptan-2-amine    (stick drawing)

Downloads

  Download digitized spectrum in JCAMP-DX format
(This file includes also the data listed on this page)
  Download all lines from the above plot in .csv format
(This file contains only the plotted data)