Note: Toggle plots by clicking on the legend |
Peak |
T site |
Q-type |
Chemical Shift |
Relative |
Peak Width |
Peak Shape |
Assigment |
(topological) | (ppm) |
Peak Area |
(ppm) |
(x)L (1-x)G |
|
Si4 | T2 | Q4(0Al) | -114.44 | 2.000 | 0.32 | 1.000 |
Si2 | T4 | Q4(0Al) | -113.17 | 1.000 | 0.32 | 1.000 |
Si1 | T3 | Q4(0Al) | -112.88 | 1.000 | 0.28 | 1.000 |
Si3 | T1 | Q4(0Al) | -110.91 | 2.000 | 0.39 | 1.000 |
Authors: | Fyfe, C.A., Strobl, H., Kokotailo, G.T., Pasztor, C.T., Barlow, G.E., Bradley, S. | ||||
Title: | Correlations between lattice structures of zeolites and their 29Si MAS n.m.r. spectra: zeolites KZ-2, ZSM-12, and Beta | ||||
Reference: | Zeolites, 8, 132-136 (1988) DOI: 10.1016/S0144-2449(88)80079-4 |
||||
Figure: | Figure 5a | ||||
Authors: | Fyfe, C.A., Feng, Y., Gies, H., Grondey, H., Kokotailo, G.T. | ||||
Title: | Natural-Abundance Two-Dimensional Solid-State 29Si NMR Investigations of Three-Dimensional Lattice Connectivities in Zeolite Structures | ||||
Reference: | J. Am. Chem. Soc., 112, 3264-3270 (1990) DOI: 10.1021/ja00165a002 | ||||
Method: | 2D correlation NMR | ||||
Figure: | Figure 7a |
Authors: | Marler, B. | |
Title: | Silica-ZSM-22: synthesis and single crystal structure refinement | |
Reference: | Zeolites, 7, 393-397 (1987) |
To reference this collection of solid-state NMR spectra, we suggest: | ||
Authors: | Brouwer, D.H., Brouwer, C.C., Mesa, S., Semelhago, C.A., Steckley, E.E., Sun, M.P.Y., Mikolajewski, J.G., and Baerlocher, Ch. | |
Title: | Solid-state 29Si NMR spectra of pure silica zeolites for the International Zeolite Association Database of Zeolite Structures | |
Reference: | Microporous Mesoporous Mat., 297, 110000 (2020) DOI: 10.1016/j.micromeso.2020.110000 |
Obs. freq. | 79.5 MHz (Field = 9.4 Tesla) | |
Pulse sequence | single pulse | |
Spectrum | Digitized and processed by Brouwer Lab, Redeemer University | |
Data processing | Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook |
[Si - O]-TON |
Download digitized spectrum in JCAMP-DX format (This file includes also the data listed on this page) | Download all lines from the above plot in .csv format (This file contains only the plotted data) |