| Note: Toggle plots by clicking on the legend |
Peak |
Q-type |
Chemical Shift |
Relative |
Peak Width |
Peak Shape |
Label |
(ppm) |
Peak Area |
(ppm) |
(x)L (1-x)G |
|
A | Q4(4Al) | -30.17 | 1.00 | 2.72 | 0.570 |
B | Q4(4Al) | -27.76 | 1.00 | 3.08 | 0.570 |
C | Q4(4Al) | -23.71 | 1.00 | 2.76 | 0.570 |
D | Q4(4Al) | -23.51 | 1.00 | 2.76 | 0.570 |
| Authors: | Akporiaye, D.E., Fjellvåg, H., Halvorsen, E.N., Hustveit, J., Karlsson, A. and Lillerud, K.P. | ||||
| Title: | UiO-7: A new aluminophosphate phase solved by simulated annealing and high-resolution powder diffraction | ||||
| Reference: | J. Phys. Chem., 100, 16641-16646 (1996 DOI: 10.1021/jp961046a) |
||||
| Figure: | Figure 4a | ||||
| Authors: | Fjellvag, H., Akporiaye, D.E., Halvorsen, E.N., Karlsson, A., Kongshaug, K.O., Lillerud, K.P. | |
| Title: | Crystal structure and MAS-NMR study of rehydrated UiO-7 | |
| Reference: | Solid State Sciences, 3, 603-611 (2001) DOI: 10.1016/S1293-2558(01)01175-X |
| To reference this collection of solid-state NMR spectra, we suggest: | ||
| Authors: | Brouwer, D.H. and White, A.L. | |
| Title: | A comprehensive collection of solid-state 31P NMR spectra of aluminophosphate zeolites. | |
| Reference: | Microporous Mesoporous Mat., 337, 111934 (2022) DOI: 10.1016/j.micromeso.2022.111934 | |
| Obs. freq. | 121.421 MHz (Field = 7 Tesla) | |
| Pulse sequence | single pulse | |
| MAS frequency | 4.5 kHz | |
| Spectrum | Digitized and processed by Brouwer Lab, Redeemer University | |
| Data processing | Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook |
|
| Comment | Peak assignments are not available. This spectrum from Akporiaye et al is actually of the calcined and rehydrated phase, even though the figure caption states that it is only calcined. |
| [Al - P - O]-ZON |
| Download digitized spectrum in JCAMP-DX format (This file includes also the data listed on this page) | Download all lines from the above plot in .csv format (This file contains only the plotted data) |