Database of Zeolite Structures
 
Framework Type ATO
31P MAS NMR spectrum of calcined AlPO-31


Note: Toggle plots by clicking on the legend

Peak
T site
Q-type
Chemical Shift
Relative
Peak Width
Peak Shape
Assigment
(topological)
(ppm)
Peak Area
(ppm)
(x)L (1-x)G
P1
T1
Q4(4Al)
-30.59
1.000
1.22
0.003


References
Spectrum

  Authors: Mali, G., Meden, A., Ristic, A., Tusar, N.N., Kaucic, V.
  Title: Interaction of dipropylamine template molecules with the framework of as-synthesized AlPO4-31
  Reference: J. Phys. Chem. B, 106, 63-69 (2002)
  Figure: Figure 3  

Peak Assignment

  Authors: Mali, G., Meden, A., Ristic, A., Tusar, N.N., Kaucic, V.
  Title: Interaction of dipropylamine template molecules with the framework of as-synthesized AlPO4-31
  Reference: J. Phys. Chem. B, 106, 63-69 (2002)
  Method: single peak
  Figure: Figure 3  

Crystal Structure

  Authors: Bennett, J.M. and Kirchner, R.M.
  Title: The Structure of Calcined AlPO4-31 - A New Framework Topology Containing One-Dimensional 12-Ring Pores
  Reference: Zeolites, 12, 338-342 (1992)

Digitization and Modeling of Spectrum

  To reference this collection of solid-state NMR spectra, we suggest:
  Authors: Brouwer, D.H. and White, A.L.
  Title: A comprehensive collection of solid-state 31P NMR spectra of aluminophosphate zeolites.
  Reference: Microporous Mesoporous Mat., 337, 111934 (2022)
Spectrum information

  Obs. freq. 242.89 MHz (Field = 14.1 Tesla)
  Pulse sequence single pulse
  MAS frequency 11 kHz
  Spectrum Digitized and processed by Brouwer Lab, Redeemer University
  Data processing Spectrum digitized with WebPlotDigitizer and deconvoluted with Mathematica notebook
 

Chemical Formula

  [Al - P - O]-ATO

Downloads

  Download digitized spectrum in JCAMP-DX format
(This file includes also the data listed on this page)
  Download all lines from the above plot in .csv format
(This file contains only the plotted data)

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